• Journal of the Korean Society for Heat Treatment
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• v.6 no.1
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• pp.9-16
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• 1993

To investigate the properties of diffusion bonding of 7050 Al alloy, the diffusion bonding joints have been produced in self-made diffusion bonding hot-press which admits a defined application of the bonding pressure during the heating phase and also rapid cooling after the bonding process with various bonding condition. The strength of the bond increases with increasing the bonding time and temperature. Shear test at toom temperature showed that high strength up to 70% that of parent metal (320 MPa), 220 MPa for the specimen bonded 14 hr at $560^{\circ}C$, with 3 MPa. In this case, however, there is large deformation more than 20% reduction in thickness. The results were correlated with joint characteristics found by optical microstructure and by fractography by SEM. When the strengths of the bonds are more than 50% that of parent metal, a great deal of dimples stretched along the direction of shear stress are observed over the fractured surface of the bond. On the microstructure of the bond line, initial mophology of the bond line disapeared for the grain boundary migration with increasing the bonding time.

• 전기의세계
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• v.30 no.4
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• pp.227-230
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• 1981

The variation of sheet resistance and the reduction of masking oxide thickness with the flow rate of nitrogen gas has been measured in Boron predeposition process with Planar Diffusion source, BN-975. At 900.deg. C, the sheet resistance varied as much as 75% when the nitrogen flow rate was changed from 0.4 liters/min to 2.0 liters/min. At 975.deg. C, however, only 12% of sheet resistance variation was observed under the same flow rate change. The reduction of masking oxide thickness at 975.deg. C for a 5 min predeposition was 600 nm when the nitrogen flow rate was 0.4 liters/min. When the flow rate incresased to 1.9 liters/min, however, only 100nm of masking oxide was consumed in a similar predeposition process.

• Journal of the Korean Chemical Society
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• v.31 no.3
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• pp.250-257
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• 1987

The electrical conductances for the thorium (IV) complexes with crown ethers have been measured in DMSO, and water solvents, and the oxidation-reduction reaction mechanisms, electron number and diffusion coefficients in the reversible reduction process have been examined by polarography and cyclic voltammography. The dissociation mole ratio of $Th^{4+}$ and nitrate ion are 1:1 and in aprotic solvent, and 1:4 in protic solvent like as water. The limiting molar conductances of all complexes in aprotic solvent have been found to be in the range of $92.2{\times}159$ $ohm^{-1}cm^2mol^{-1}$. In aprotic solvent, DMSO, the reduction of each complex is reversible by one electron reduction of one step, and the range of diffusion coefficients is obserbed to be $5.83\;10^{-6}{\sim}6.90{\times}10^{-6}$. The complexes which have reduction step were hydrolyzed above at 1.8volt with reference saturated calomel electrode, generating the hydrogen gas. The reaction mechanisms of thorium (IV)-crown ether complexes appear as follows. ${Th_m(IV)L_n(H_2O)_x(NO_3)_{4y}}_=^{DMSO} {\overline{{Th_m(IV)L_n(H_2O)_x(NO_3)_{4y-1}}}^+ + NO_3-$

• The Journal of the Korea Contents Association
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• v.8 no.11
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• pp.1-9
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• 2008

Thanks to the multimedia technology development, it is possible to show image representations in high quality and to process images in various ways. Anisotropic diffusion as an effective diffusion filtering among many image preprocessing methods and postprocessing methods is used in reduction of speckle noises of ultrasound images, image restoration, edge detection, and image segmentation. However, the conventional anisotropic diffusion based on a cross-kernel causes the following problems. The problem is the concentration of edges in the vertical or horizontal directions. In this paper, a new anisotropic diffusion transform based on directions of gradient is proposed. The proposed method uses the eight directional square-kernel which is an expanded form of the cross-kernel. The proposed method is to select directions of small gradient based on square-kernel. Therefore, the range of proposed diffusion is selected adaptively according to the number of the directions of gradient. Experimental results show that the proposed method can decrease the concentration of edges in the vertical or horizontal directions, remove impulse noise. The image in high quality can be obtained as a result of the proposed method.

• Journal of Electrochemical Science and Technology
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• v.4 no.3
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• pp.93-101
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• 2013

The electrodeposition of indium onto a copper electrode from an aqueous sulfate solution containing $In^{3+}$ was studied by means of cyclic voltammetry and chronoamperometry. Reduction and oxidation of indium on copper were investigated by using cyclic voltammograms at different negative limiting potentials and at different scan rates in cumulative cycles. Cyclic voltammograms indicated that reduction and oxidation processes of indium could involve various reactions. Chronoamperometry was carried out to analyze the nucleation mechanism of indium in the early stage of indium electrodeposition. The non-dimensional plot of the current transients at different potentials showed that the shape of the plot depended on the applied potential. The nucleation of indium at potential step of -0.6~-0.8 V was close to progressive nucleation limited by diffusion. However the non-dimensional plot of current transients for the indium nucleation showed different behaviors from theoretical curves at the potential step lower than -0.8 V.

• Journal of the Korean Magnetics Society
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• v.15 no.1
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• pp.42-47
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• 2005

Nanocrystalline Nd-Fe-B powder was synthesized by a new thermochemical process that combined with past reduction-diffusion process and spray-dry process. In this process, Ca reduction process is vary important due to formation of hard magnetic$Nd_{2}Fe_{14}B$ phase from various oxides by Ca powder. Therefore, the final products are essentially affected a shape, size, and composition etc. of the Ca reduced powders. Ca reduction was performed to way that raw powders just mixed with Ca powder in proper ratio unlike to compress into compact. The powders after mixture-type Ca reduction mainly composited with $Nd_{2}Fe_{14}B$ phase even relativily low reaction temperature ($800^{\circ}C$) and all particle size of powder were distributed less than 1 ${\mu}m$ except for powder after Ca oxides as magnetic properties of powders after cake-type Ca reduction, with the consequence that high magnetic properties has been expected. The magnetic properties of powders prepared by mixture-type Ca ruduction, with the conseqence that high magnatic properties has been expected. The magnetic properties of powders prepared by mixture-type Ca reduction process showed $_iH_c$ = 5.9 kOe, $B_r$ = 5.5 kG, (BH)max = $Nd_{2}Fe_{14}B{\to}Nd_{2}Fe_{17}B$ decomposition by violent exothermic reaction during washing.

• Journal of IKEEE
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• v.19 no.2
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• pp.168-175
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• 2015

In this paper, we propose FPGA design technique for rotating LED display device which is capable of displaying videos with the use of the afterimage effect. The proposed technique is made up of image data correction process based on inverse gamma correction and error diffusion, block interleaving process, and data serial output process. The data correction process based on inverse gamma correction and error diffusion is an image data correction step in which image data received are corrected by inverse gamma correction process to convert the data into linear brightness characteristics, and by error diffusion process to reduce the brightness reduction phenomenon in low-gray-level which is caused by inverse gamma correction. In the block interleaving process, the data of the frames entered transversely are first saved in accordance with entrance order, and then only the longitudinal image data are read. The data serial output process is applied to convert the parallel data in a rotating location into serial data and send them to LED Driver IC, in order to send data which will be displayed on high-speedy rotating LED Bar. To evaluate the accuracy of the proposed FPGA design technique, this paper used XC6SLX45-FG484, a Spartan 6 family of Xilinx, as FPGA, and ISE 14.5 as a design tool. According to the evaluation analysis, it was found that goal values were consistent with simulation values in terms of accurate operation of inverse gamma and error diffusion correction, block interleaving operation, and serialized operation of image data.

• Journal of the Korean Ceramic Society
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• v.36 no.2
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• pp.167-171
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• 1999

Titanium dioxide bodies sintered at 130$0^{\circ}C$ for 10 h under the oxygen flowing were reduced with hydrogen in 1200, 1250 and 130$0^{\circ}C$ for 4~20 h. Reduction kinetics were evaluated by measuring a weight loss between before and after reduction, and the thickness of reduced layer, respectively. The reduction followed the parabolic rate law, indicating that the rate-determining process is diffusion. From the Arrhenius plots, the apparent activation energies for the reduction were obtained as 210$\pm$10 kJ/mol.

• Journal of the Korean Chemical Society
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• v.35 no.4
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• pp.405-409
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• 1991

The electrochemical behaviors of copper-1-(2-thiazolylazo)-2-naphthol [Cu(II)-TAN] complex in acetonitrile (AN) solution have been investigated by the use of polarography, controlled potential coulometry and UV-Vis spectroscopy. Cu(II)-TAN complex exhibit three reduction waves at -0.91 V, -1.34 V and -1.65 V vs. S.C.E. in acetonitrile solution containing 5.0 ${\times}\;10^{-3}$M tetraethylammonium perchlorate. Every reduction wave is diffusion controlled. The first reduction wave is considerably reversible and this process is attributed to the formation of anion radical. The second reduction process to the dianion is followed by a chemical reaction producing a complex of hydrazo complex. The third reduction process produce Cu(Hg) amalgam and amine compound.

• Transactions of Materials Processing
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• v.22 no.8
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• pp.463-469
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• 2013

In the previous work, a new forging process design, which included incremental upsetting, diffusion bonding and cogging, was suggested as a method to manufacture 1.9wt%C ultrahigh carbon workrolls. The previous study showed that incremental upsetting and diffusion bonding are effective in closing voids and healing of the closed void. In addition, compression tests of the 1.9wt%C ultrahigh carbon steel revealed that new microvoids form within the blocky cementite at temperatures of less than $900^{\circ}C$ and that local melting can occur at temperatures over $1120^{\circ}C$. Thus, the forging temperature should be controlled between 900 and $1120^{\circ}C$. Based on these results, incremental upsetting and diffusion bonding were used to check whether they are effective in closing and healing voids in a 1.9wt%C ultrahigh carbon steel. The incremental upsetting and diffusion bonding were performed using sub-sized specimens of 1.9wt%C ultrahigh carbon steel. The specimen was deformed only in the radial direction during the incremental upsetting until the reduction ratio reached about 45~50%. After deformation the specimens were kept at $1100^{\circ}C$ for the 1 hour in order to obtain a high bonding strength for the closed void. Finally, microstructural observations and tensile tests were conducted to investigate void closure behavior and bonding strength.