• 제목/요약/키워드: Reduced atmosphere

검색결과 474건 처리시간 0.029초

문화재의 생물열화 방제-훈증처리를 중심으로 (Biodeterioration of Cultural Property and Fumigation)

  • 이호봉
    • 보존과학연구
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    • 통권13호
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    • pp.69-80
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    • 1992
  • A great numbers of cultural properties destroyed though attack by insect pests and microorganisms. Biodeterioration damage is particularly serious in this country because many cultural propertiese are made of organic materials. Recently, there are various countermeasures of biodeterioration or alternative methods are reported, such as Gamma Radiation, Micro-wave Irridation, Freezing, Inert Atmosphere (Oxygen-less atmosphere), and Environmental Control. However its practical application are limited and some difficulties for treatment of large objects. Fumigation is one of the most useful and effective methods of control biodeterioration because it gives less damage of cultural properties but rapidly eradicate infesting organisms at one action. This paper evaluated selected fumigants and fumigation methods with emphasis on the following paragraph:1) Effectiveness of selected fumigants on insects and microbes involved inbiodeterioration.2) Physical and chemical characters of selected fumigants.3) Less toxic new alternative fumigant and its mixtures.4) Inert atmosphere (Oxygen-less atmosphere)5) Methods of fumigation : Sealed fumigation, Covered fumigation and Vacuum fumigation (Reduced-pressure fumigation)

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Effects of the Decomposition Residue of Compound Additive on Resintering Behavior

  • Kim, H.S.;C.Y. Joung;Kim, S.H.;S.H. Na;Lee, Y.W.;D.S. Sohn
    • Nuclear Engineering and Technology
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    • 제34권4호
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    • pp.323-330
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    • 2002
  • Various types of compounds were tested with the aspects of decomposition and formation of residue in a $CO_2$ or 7H$_2$+93$N_2$ atmosphere. The evaporation temperature range of each compound was determined from thermogravimetric curve. Decomposition of dicarbon amide, stearic acid, acrowax and zinc stearate was studied by thermogravimetry in $CO_2$ or in 7H$_2$+93$N_2$ atmosphere. All compounds were decomposed in $CO_2$ atmosphere at lower than 40$0^{\circ}C$, but the residue, ZnO remained for zinc stearate. ZnO did not decompose in $CO_2$ atmosphere up to 130$0^{\circ}C$, but reduced into Zn metal and disappeared in the temperature range of $600^{\circ}C$ to 120$0^{\circ}C$ in 7H$_2$+93$N_2$ atmosphere. The effect of residue, which trapped in closed pores of sintered pellet, on the thermal stability was studied using the resintering test at 1$700^{\circ}C$ in 7H$_2$+93$N_2$ atmosphere. In the case of oxidative sintered pellet with admixing zinc stearate, the cavity formation accompanied with a density drop after resintering is due to the pressure of the Zn gases trapped in the isolated pores.

$WS_2$ 고체윤활제의 마찰.마모 거동 (Tribological Behaviour of $WS_2$Solid Lubricant)

  • 신동우;김인섭;윤대현;김경도;김성진;정진수
    • Tribology and Lubricants
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    • 제14권2호
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    • pp.35-41
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    • 1998
  • The $WS_2$ solid lubricant synthesized through the vapour phase transport method was coated on the commercial bearing steel (SUJ 2) substrate, and the tribological behaviour of the lubricant was investigated using a ball-on-disk type tester. The $WS_2$ powder was spray-coated at room temperature using compressed air, and the change of friction coefficient was examined in various conditions, i.e., specimen configuration, atmosphere (air and nitrogen), applied load and rotating speed. $WS_2$ coated ball and disk showed the optimum friction coefficient of 0.07 and wear life of 45,000 cycles in the nitrogen atmosphere under 0.3 kgf and 100 rpm, whereas relatively high coefficient of 0.13 and reduced wear life of 4,000 cycles were observed in air atmosphere. The effect of rotating speed on the friction coefficient was not observed both in nitrogen and in air atmospheres. This confirmed that the spray-coated $WS_2$ solid lubricant was effective in reducing the friction coefficient and improving wear life in nitrogen atmosphere, and the oxygen and moisture existing in air could seriously deteriorate the lubrication effect of $WS_2$ coating layer.

Effect of Annealed Oxides on the Formation of Inhibition Layer During Hot-Dip Galvanizing of 590Mpa Trip Steel

  • Kim, Seong-Hwan;Huh, Joo-Youl;Lee, Suk-Kyu;Park, Rho-Bum;Kim, Jong-Sang
    • Corrosion Science and Technology
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    • 제10권1호
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    • pp.6-12
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    • 2011
  • The selective surface oxidation of a transformation-induced-plasticity (TRIP) steel containing 1.6 wt.% Mn and 1.5 wt.% Si during annealing at $800^{\circ}C$ was investigated for its influence on the formation of an inhibition layer during hot-dip galvanizing. The selective oxidation of the alloying elements and the oxide morphology were significantly influenced by the annealing atmosphere. The pure $N_{2}$ atmosphere with a dew point $-40^{\circ}C$ promoted the selective oxidation of Mn as a crystalline $Mn_{2}SiO_{4}$ phase, whereas the $N_{2}$ + 10% $H_{2}$ atmosphere with the same dew point $-40^{\circ}C$ promoted the selective oxidation of Si as an amorphous Si-rich oxide phase. During hot-dip galvanizing, the $Mn_{2}SiO_{4}$ phase was reduced more readily by Al in the Zn bath than the Si-rich oxide phase. Consequently, the pure $N_{2}$ atmosphere resulted in a higher formation rate of $Fe_{2}Al_{5}$ particles at the Zn/steel interface and better galvanizability than the $N_{2}$ + 10% $H_{2}$ atmosphere.

소성 분위기에 따른 인공골재의 미세구조 관찰 (Microstructural observation of artificial aggregates at various sintering atmospheres)

  • 박지윤;김유택
    • 한국결정성장학회지
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    • 제16권2호
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    • pp.71-75
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    • 2006
  • 소성 분위기를 변화시켜 골재를 제조할 때 골재의 중앙에 만들어지는 블랙코어(black core) 형성정도의 차이와 골재 물성의 차이점을 알아보기 위해 적점토, 탄소(carbon), 산화철($Fe_2O_3$)이 혼합된 직경 10mm 구형골재를 조성별로 산화분위기, 중성분위기, 환원분위기에서 각각 소성시키고 각각의 비중, 흡수율, 블랙코어 면적비(%)를 측정하고 비교하였다. 산화분위기에서 소성시킨 골재는 껍질(shell)과 블랙코어가 뚜렷하게 구분되는 반면 중성 및 환원분위기에서 소성한 시편에서는 시편의 단면전체에 블랙코어가 형성되었다. 산화분위기와 중성분위기와는 달리 환원분위기에서 소성된 시편에서는 탄소첨가량이 증가할수록 비중이 증가했으며, 전반적인 비중은 가장 낮았다. 흡수율은 모든 분위기에서 탄소첨가량이 증가할수록 증가하는 경향을 보였다.

분사조건에 따른 LPG 인젝터의 분무특성에 관한 연구 (A Study on the spray characteristics according to injection conditions for LPG injector)

  • 류재덕;윤용원;이기형;이창식
    • 한국분무공학회지
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    • 제6권3호
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    • pp.17-22
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    • 2001
  • Recently LPG engine is developed to fulfill such new requirements as improved fuel efficiency in additional to further reduced exhaust emission. This experimental study is conducted to analyze spray characteristics for pintle type injector used in a LPLi (Liquid Phase LPG injection) engine. Since spray parameters including penetration length and spray angle make a role to design injector and engine intake system, spray visualization experiment is performed under atmosphere ambient and charging condition using Mie scattering method. From the experimental result under various LPG formation, the increased propane component decreases penetration length because boiling point of propane is lower than butane. To simulate intake charging condition in MPI engine, spray visualization is performed under high pressure condition. As a result, as ambient pressure is increased from atmosphere to 3.0 bar, penetration length is decreased. However, as ambient pressure is increased from atmosphere to 3.0 bar, spray angle is increased.

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쾌속 금형 제작을 위한 텅스텐 카바이드와 코발트 혼합물의 선택적 레이저 소결 (Selective Laser Sintering of WC-Co Mixture for Rapid Tooling)

  • 김광희;조셉비만
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2002년도 금형가공 심포지엄
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    • pp.187-194
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    • 2002
  • This paper describes the experimental results on direct selective laser sintering of WC-Co mixture for rapid tooling. The experiments were carried out within an air, argon and nitrogen atmosphere. Coupons of single layer were sintered at various laser powers, scanning speeds and scan spacings. As the energy density (energy per unit scanned area) is increased, the thickness of coupons is increased. The main problem took place during sintering within an air atmosphere was severe oxidation of WC-Co mixture. As the laser power is increased and/or scanning speed is decreased, more severe oxidation occurred. Within an argon and nitrogen atmosphere the oxidation is reduced significantly. Experiments on multi-layer sintering were also carried out.

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접합모형을 이용한 경년 및 계절안 진동 모사실험 연구 (On the Study of Intraseasonal and Interannual Oscillations Simulation by using Coupled Model)

  • 안중배
    • 한국환경과학회지
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    • 제8권6호
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    • pp.645-652
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    • 1999
  • In order to simulate and investigate the major characteristics of El Nino/Southern Oscillation(ENSO) and Madden Jullian Oscillation(MJO), an intermediate type atmosphere-ocean coupled model is developed and their results are examined. The atmosphere model is a time-dependent non-linear perturbation moist model which can determine the internal heating for itself. The counterpart of the atmosphere model is GCM-type tropical ocean model which has fine horizontal and vertical grid resolutions. In the coupled experiment, warm SST anomaly and increased precipitation and eastward wind and current anomalies associated with ENSO and MJO are properly simulated in Pacific and Indian Oceans. In spite of some discrepancies in simulation MJO, the observed atmospheric and oceanic low-frequency characteristics in the tropics are successfully identified. Among them, positive SST anomalies centered at the 100m-depth of tropical eastern-central Pacific due to the eastward advection of warm water and reduced equatorial upwelling, and negative anomalies in the Indian and western Pacific seem to be the fundamental features of tropical low-frequency oscillations.

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$H_2/Ar$분위기에서 제조한 투명전극용 ZnO:Al 박막의 특성 (Characteristics of ZnO:Al Thin Films for TCO Prepared by RE Magnetron Sputtering in $H_2/Ar$ Atmosphere)

  • 탁성주;이정섭;김원목;김동환
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2006년도 춘계학술대회
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    • pp.162-165
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    • 2006
  • AZO (ZnO:Al) were fabricated by RF magnetron sputtering In $H_2/Ar(5%\;H_2)$ atmosphere, and structural, electrical and optical properties were investigated. The substrate temperatures were varied at RT, $100^{\circ}C,\;150^{\circ}C$ and$200^{\circ}C$. The resistivity of the films grown in $H_2/Ar(5%\;H_2)$ were reduced from $7.67{\times}10^{-4}{\Omega}\;cm$ to $5.95{\times}10^{-4}{\Omega}\;cm$ comparing that Ar (100%) and the transmittance of the ZnO:Al films in the visible range was 85%.

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AUC(Ammonium Uranyl Carbonate)의 하소 및 환원 반응 -분말의 특성 및 상변화- (A Study on Calcination and Reduction of AUC (Ammonium Uranyl Carbonate) -Characteristics and Phase Change of Powder-)

  • 김응호;최청송;박진호;장인순
    • 한국세라믹학회지
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    • 제30권4호
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    • pp.279-288
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    • 1993
  • A study on calcination and reduction of AUC(ammonium uranyl carbonate, (NH4)4UO2(CO3)3) has been carried out by using TG-DTA in N2, air and H2 atmospheres, respectively. Phases of various intermediate obtained during thermal analysis of AUC in different atmospheres were confirmed by XRD. Powder characteristics of each intermediate were investigated by measuring particle size and specific surface area, and also observed by SEM. As a results, regardless of applied atmosphere AUC was calcined into amorphous UO3, which was converted to $\alpha$-U3O8 Via $\alpha$-UO3 in both H2 and N2 atmosphere, but directly into $\alpha$-UO3 in air atmosphere. Further reduction of U3O8 was only detectable in hydrogen atmosphere. During calcination and reduction, average particle size was reduced to less than 30% of original value without morphology change. Specific surface area was dramatically increased with release of NH3, CO2 and H2O from AUC powder and reached maximum value around 25$0^{\circ}C$, and then gradually decreased with the increase of temperature due to sintering effect of uranium oxides such as UO3 and U3O8. It was also found that the change of average crystallite size and pore size were closely related to the changes of specific surface area of uranium oxides.

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