• Title/Summary/Keyword: Reduced Pressure Evaporation

Search Result 51, Processing Time 0.03 seconds

Optimum design of the Characteristics of Double Stage Evaporator/Absorber for Large temperature Difference Absorption System (냉수 대온도차 흡수식 냉동기용 2단 증발기/ 흡수기 최적 설계)

  • Park, Chan-Woo;Im, Ick-Tae;Kang, Yong-Tae
    • Proceedings of the SAREK Conference
    • /
    • 2008.11a
    • /
    • pp.203-211
    • /
    • 2008
  • The optimal design of two stage evaporation & absorption system which is related to the large temperature difference system was investigated numerically in the absorption refrigeration system. The concentrations at inlet & oulet of absorber are 62.9% and 56.9%, but in two stage absorption system the values are 62.2% and 56.2%. Therefore strong solution & weak solution became diluted than the standard value. The amount of weak solution circulation can be reduced in absorption refrigeration system, and the sensible heat load is more reduced to enhance the COP of system. As UAR is increased, COP becomes larger, and this means the role of top section is more important than bottom section in two stage evaporation & absorption system. But the increase of COP becomes slower at 0.7 of UAR ratio. The performance of Type2 is higher than Type1 in COP with the flow direction of cooling waters. This phenomena is due to the active absorption of vapor -absorption & lower temp. cooling water is more effective. The pressure at bottom section becomes higher & that at top section becomes lower and therefore the circulation rate can be diminished more.

  • PDF

Studies on the Synthesis of High Purity and Fine Mullite Powder (I) (고순도 초미립자 물라이트 분말 합성에 대한 연구 (I))

  • 김경용;김윤호;김병호;이동주
    • Journal of the Korean Ceramic Society
    • /
    • v.26 no.5
    • /
    • pp.682-690
    • /
    • 1989
  • Fine mullite powder was prepared by colloidal sol-gel route. Boehmite as a starting material of Al2O3 and silica sol or fumed silica as a starting material of SiO2 were used. $\alpha$-Al2O3, TiO2 and ZrO2 were used as seeding materials. The combination of boehmite and silica was found to be the stoichiometric mullite powder. Techniques for drying used were spray drying, freeze drying, reduced pressure evaporation and drying in a oven. The gelled powder was heated at 130$0^{\circ}C$ for 100min and was attrition-milled for 1~3hrs. The mullite powder obtained was composed of submicrometer, uniform and spherical particles with a narrow size distribution. The mullite powder was characterized by BET, SEM, XRD and IR spectroscopy.

  • PDF

Removal of Residual Solvents in Paclitaxel by Supercritical Carbon Dioxide (초임계 이산화탄소를 이용한 Paclitaxel의 잔류용매 제거)

  • 김진현;박흥복;기은숙;강인선;최형균;홍승서
    • KSBB Journal
    • /
    • v.16 no.3
    • /
    • pp.233-236
    • /
    • 2001
  • Because of casehardenign effect of amorphous paclitaxel, residual solvents, methylene chloride and emthanol could not be reduced to the maximum value allowed, 600 ppm and 3,000 ppm, in accord with the guidelines issued by the International Conference on Harmonization (ICH, 1997), using rotary evaporation and successive drying in a vacuum oven. However, methylene chloride and methanol were reduced to 486 ppm and 403 ppm, respectively using supercritical $CO_2$ on purified paclitaxel. The optimum pressure and operating time were 80 bar and 30 min at fixed operating temperature ($40^{circ}C$). This approach serves as a novel application of supercritical fluid extraction to remove residual solvents from active pharmaceutical ingredients.

  • PDF

A Design Process for Reduction of Pressure Drop of Air-cooled Condenser for Waste Heat Recovery System (폐열 회수 시스템용 공랭식 응축기의 압력 손실 저감 설계)

  • Bae, Sukjung;Heo, Hyungseok;Park, Jeongsang;Lee, Hongyeol;Kim, Charnjung
    • Transactions of the Korean Society of Automotive Engineers
    • /
    • v.21 no.6
    • /
    • pp.81-91
    • /
    • 2013
  • A novel design process of a parallel multi-flow type air-cooled condenser of a dual-loop waste heat recovery system with Rankine steam cycles for improving the fuel efficiency of gasoline automobiles has been investigated focusing on reduction of the pressure drop inside the micro-tubes. The low temperature condenser plays a role to dissipate heat from the system by condensing the low temperature loop working fluid sufficiently. However, the refrigerant has low evaporation temperature enough to recover the waste from engine coolant of about $100^{\circ}C$ but has small saturation enthalpy so that excessive mass flow rate of the LT working fluid, e.g., over 150 g/s, causes enormously large pressure drop of the working fluid to maintain the heat dissipation performance of more than 20 kW. This paper has dealt with the scheme to design the low temperature condenser that has reduced pressure drop while ensuring the required thermal performance. The number of pass, the arrangement of the tubes of each pass, and the positions of the inlet and outlet ports on the header are most critical parameters affecting the flow uniformity through all the tubes of the condenser. For the purpose of the performance predictions and the parametric study for the LT condenser, we have developed a 1-dimensional user-friendly performance prediction program that calculates feasibly the phase change of the working fluid in the tubes. An example is presented through the proposed design process and compared with an experiment.

Effect of M2O3 on the Sinterbility and Electrical Conductivity of ZrO2(Y2O3) System(III) : Ceramics of the ZrO2-Y2O3-Ln2O3 System (ZrO2(Y2O3)계 세라믹스의 소결성과 전기전도도에 대한 M2O3의 영향(III) : ZrO2-Y2O3-Ln2O3계 세라믹스)

  • 오영제;정형진;이희수
    • Journal of the Korean Ceramic Society
    • /
    • v.24 no.2
    • /
    • pp.123-132
    • /
    • 1987
  • Yttria-stabilized zirconia with erbia-lanthana were investigated with respect to the amount of Ln2O3 (Ln; Er, La) addition in the range of 0.5∼5 mol% to the base composition of 8 mol% yttriazirconia. Following analysis and measurement were adopted for the characterization of synthesizes of solid electrolyte; phase transformation, lattice parameter, crystallite size, relative density, chemical composition and SEM/EDS. Electrical conductivity by two-probe method versus temperature from 350$^{\circ}C$ to 800$^{\circ}C$ and frequency in the range of 5Hz∼13MHz by complex impedance method was also conducted together with the determination of oxygen ion transference number by EMF method for the evaluation of their electrical properties. The results were as followsing; Electrical conductivity were decreased with increase in Ln2O3 content, but their activation energies increased. In the case of La2O3 addition, espicially, its electrical conductivity was decreased owing to the segregation of second phases at the grain-boundary. Grain-boundary conductivity of the specimen contained 0.5 mol% Er2O3 exhibited a maximum conductivity among thecompositions experimented. However, their bulk conductivities decreased in both case. Oxygen ion transference number was also reduced with decrease in oxygen partial pressure. For example, in the case of Er2O3 addition it retained value in the range of 0.97∼0.94 abvove 4.74${\times}$10-2in oxygen partial pressure. With the increase in the quantities of the evaporation of additive components, the crystallite size of stabilized zirconia decreased, and their relative density also reduced owing to the formation of porosity in their matrices. In the case of La2O3 the sinterbility was improved in the limited amount of addition up to 0.5 mol%, in the same range of addition the strength of sintered bodies were improved perhaps owing to the precipitation of metastable tetragonal phase in the fully stabilized zirconia.

  • PDF

Purification of Band 3 from the Human Erythrocyte Membrane and its Incorporation into Liposome (사람 적혈구막 Band 3의 정제 및 Liposome으로의 도입)

  • Kim, Jae-Ryong;Kim, Jung-Hye;Lee, Ki-Yung
    • Journal of Yeungnam Medical Science
    • /
    • v.3 no.1
    • /
    • pp.41-48
    • /
    • 1986
  • Band 3, the predominent 95,000 dalton anion transport protein, is the major intrinsic glycoprotein of the human erythrocyte membrane. This anion carrier exists as a dimer and binds the cytoskeletons such as spectrin, ankyrin and actin. And the liposomes are vesicular structures which form spontaneouly upon hydration of phospholipids. These artificial lipid vesicles have been investigated as model of the biological membranes and as a mean of improving the delivery of nucleic acids, drugs, proteins and biological substances to specific target tissues and cells. In this study, we were purified Band 3 from the human erythrocyte membrane(ghost) was prepared by hemolysis of intact human erythrocyte with weak alkali-hypotonic solution. Band 6 was removed from ghost by extracting with solution of an ionic strength of 0.15. Band 3 and Band 4 were solubilized selectively by extracting Band 6-depleted ghosts with Triton X-100 under nondenaturing conditions. Band 3 was then purified from Triton X-100 extract treated with p-chloromercuribenzoate by sucrose density gradient ultracentrifugation. This purified Band 3 was incorporated into liposomes prepared by reverse-phase evaporation. Phosphatidyl L-serine and cholesterol(1 : 1 molar ratio) were dissolved in chloroform and then chloroform was removed by rotatory evaporation under reduced pressure. Band 3 solution without Triton X-100 was introduced into a mixture of lipids and diethylether. Diethylether was subsequently removed by evaporation. This purified Band 3 and its incorporation into liposomes were confirmed by sodium dodecyl sulfate-polyacrylamide gel electrophoresis.

  • PDF

Preparation and Characterization of Solid Dispersions of Eprosartan with Hydrophilic Polymers (친수성 고분자를 이용한 에프로살탄 고체분산체의 제조 및 특성 분석)

  • Hwang, Jun-Seok;Ko, Ji-Eun;Kim, So-Hee;Huh, Kang-Moo
    • Polymer(Korea)
    • /
    • v.36 no.4
    • /
    • pp.500-506
    • /
    • 2012
  • In this study, we developed and optimized hydrophilic polymer based solid dispersion formulations (SDs) for enhancing the aqueous solubility of eprosartan, one of poorly soluble drugs, that has been broadly used for the treatment of high blood pressure. Poly(ethylene glycol) (PEG) and poly(vinyl pyrrolidone) (PVP) based SDs were prepared by hot melting and solvent evaporation methods and the drug/polymer composition varied in the range of 1:1~1:5 with or without poloxamer 407 (P407) as a polymeric surfactant. The SDs prepared by solvent evaporation showed more reduced crystallinity than ones by hot melting, and PVP based SDs showed more enhanced solubility and lower crystallinity than PEG based SDs. Furthermore, it was observed from DSC and PXRD analysis that the SDs with P407 (drug:polymer: P407 = 1:5:1) demonstrated no crystallinity and the most enhanced solubility (more than 3~4 times).

A Study of Injection and Combustion Characteristics on Gasoline Direct Injection in Constant Volume Chamber (정적 연소기 내 가솔린 직접 분사 시 분무 및 연소특성에 관한 연구)

  • Kim, Kyung-Bae;Kang, Seok-Ho;Park, Gi-Young;Seo, Jun-Hyeop;Lee, Young-Hoon;Kim, Dae-Yeol;Lee, Seong-Wock
    • Journal of ILASS-Korea
    • /
    • v.17 no.3
    • /
    • pp.113-120
    • /
    • 2012
  • It is being more serious problems that the pollutant and the greenhouse gas emitted from the internal combustion engines due to the increasing demand of automobiles. To counteract this, as one of the ways has been studied, GDI type engine, which is directly injected into the combustion chamber and burns by a spark ignition that chose the merits of both gasoline engine and diesel engine, was appeared. The combustion phenomena in this GDI engine is known to contribute to combustion stability, fuel consumption reduction and reductions of harmful substances of exhaust gas emission, when the fuel spray of atomization being favorable and the mixture formation being promoted. Accordingly, this study analyzed the affection of ambient temperature and fuel injection pressure to the fuel by investigate the visualization of combustion, combustion pressure and the characteristic of emission, by applying GDI system on the constant combustion chamber. As a result, as the fuel injection pressure increases, the fuel distribution in the combustion chamber becomes uniform due to the increase of penetration and atomization. And when ambient temperatures in the combustion chamber become increase, the fuel evaporation rate being high but the penetration was reduced due to the reduction of volume flux, and confirmed that the optimized fuel injection strategy is highly needed.

Engineering Approach to Crop Production in Space (우주에서 작물 생산을 위한 공학적 접근)

  • Kim Yong-Hyeon
    • Journal of Bio-Environment Control
    • /
    • v.14 no.3
    • /
    • pp.218-231
    • /
    • 2005
  • This paper reviews the engineering approach needed to support humans during their long-term missions in space. This approach includes closed plant production systems under microgravity or low pressure, mass recycling, air revitalization, water purification, waste management, elimination of trace contaminants, lighting, and nutrient delivery systems in controlled ecological life support system (CELSS). Requirements of crops f3r space use are high production, edibility, digestibility, many culinary uses, capability of automation, short stems, and high transpiration. Low pressure on Mars is considered to be a major obstacle for the design of greenhouses fer crop production. However interest in Mars inflatable greenhouse applicable to planetary surface has increased. Structure, internal pressure, material, method of lighting, and shielding are principal design parameters for the inflatable greenhouse. The inflatable greenhouse operating at low pressure can reduce the structural mass and atmosphere leakage rate. Plants growing at reduced pressure show an increasing transpiration rates and a high water loss. Vapor pressure increases as moisture is added to the air through transpiration or evaporation from leaks in the hydroponic system. Fluctuations in vapor pressure will significantly influence total pressure in a closed system. Thus hydroponic systems should be as tight as possible to reduce the quantity of water that evaporates from leaks. And the environmental control system to maintain high relative humidity at low pressure should be developed. The essence of technologies associated with CELSS can support human lift even at extremely harsh conditions such as in deserts, polar regions, and under the ocean on Earth as well as in space.

Purification and Single Crystal Growth of Molybdenum by Electron Beam Floating Zone Melting (Electron Beam Floating Zone Melting에 의한 몰리브덴의 정련 및 단결정 성장에 관한 연구)

  • 최용삼;지응준
    • Korean Journal of Crystallography
    • /
    • v.3 no.2
    • /
    • pp.85-97
    • /
    • 1992
  • EBFZM( Electron Beam Floating Zone Melting) 법을 이용하여 몰리브덴에서의 금속계 불순물과 침입형 불순물의 정련기구 및 단결정 성장기구를 연구하 였다. Fe, Cr, Co등의 금속계 불순물은 몰리브덴과의 평형증기압의 차이에 따른 불순물의 선택적 증발에 의하여 우수한 정련효과를 나타내며, 몰리브덴보다 응점이 높은 Ta, W는 잘 제거되지 않았다. 한편 대역 정제에 의한 정련효과는 미약함을 확인하였다. EBF ZM은 C,0,N등의 침입형 불순물의 정련에도 효과적 이었다. 본 연구의 모든 조건에서 몰리브덴은 단결정으로 성장하였으며 2차 재결정 epitaxy에 의한 단결 정 성장기구가 제시되었다. 몰리브덴 단결정 내의 전 위밀도는 strain-anneal법에 의한 단결정의 경우보다 높았으며,본 실험의 열처리 조건에서는 변화하지 않았다. The purification and single crystal growth mechanisms of molybdenum were analysed in EBFZM ( electron beam floating zone melting). Metallic impurities of Fe, Cr, Co were purified efficiently but Ta and W were not removed well in this study. It was due to a preferential evaporation of the elements caused by the difference in equillibrium vapor pressure between the elements and molybdenum. The pu- rification effect by zone refining was not significant. The EBFZM also refined the interstitial impurities of C, 0 and N, effectively. The single crystals of molybdenum were grown regardless of the experimental conditions and the secondary recrystallization epitaxy was surge sled as a growth mechanism. The dislocation density in single crystal was higher than that by strain-anneal method, and was not reduced by heat treatments.

  • PDF