• 제목/요약/키워드: Real-time TEM

검색결과 22건 처리시간 0.024초

TEM감쇠곡선을 이용한 해수의 지하 유동현상 파악 (Determination of an Underground Seawater Flow Using a TEM Decay Curve)

  • 황학수;문창규;이상규;이태섭
    • 자원환경지질
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    • 제34권5호
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    • pp.499-506
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    • 2001
  • 연안지역에서 해수의 지하 유동현상을 효과적이고 경제적으로 파악하기 위하여 등위치 송수신루프배열의 시간영역 전자탐사법(Time-domain Electromagnetic :TEM)을 이용한 지구물리모니터링을 적용하였다. TEM 모니터링은 전기 비저항 모니터링과 비교하여 해수유동에 대한 TEM반응의 민감도는 떨어진다. 그러나, 광범위한 조사지역에 대한 담수-해수 전이대의 공간적인 분포를 파악하는데 있어서는 측정시간을 포함한 탐사경비 그리고 현장에서 자료처리 측면에서 볼 때 매우 효율적이다.

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실시간 TEM 분석에 유용한 영상 기록 프로그램, VirtualDub (VirtualDub as a Useful Program for Video Recording in Real-time TEM Analysis)

  • 김진규;오상호;송경;유승조;김영민
    • Applied Microscopy
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    • 제40권1호
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    • pp.47-51
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    • 2010
  • The capability of real-time observation in TEM is quite useful to study dynamic phenomena of materials in a certain variable ambience. In performing the experiment, the choice of video recording program is an important factor to obtain high quality of movie streaming. Window Movie Maker (WMM) is generally recommended as a default video recording program if one uses "DV Capture" function in DigitalMicrograph$^{TM}$ (DM) software. However, the image quality does not often satisfy the condition for high-resolution microscopic analysis since the severe information loss in the final result occurs during the conversion process. As a good candidate to overcome this problem, Virtual-Dub is highly recommended since the information loss can be minimized through the streaming process. In this report, we demonstrated how useful VirtualDub works in a high-resolution movie recording. Quantitative comparison of the information quality between the images recorded by each software, WMM and VirtualDub, was carried out based on histogram analysis. As a result, the image recorded by VirtualDub was improved ~13% in brightness and ~122% in contrast compared with the image obtained by WMM at the same imaging condition. Remarkably, the gray gradation (meaning an amount of information) becomes wider up to ~115% than that of the WMM result.

SHV ESBL생성 Klebsiella pneumoniae 균주의 실시간중합효소반응분석 (Real-Time PCR Analysis of SHV Extended-Spectrum beta-Lactamases Producing Klebsiella pneumoniae)

  • 양병선;육근돌
    • 대한임상검사과학회지
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    • 제41권4호
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    • pp.153-157
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    • 2009
  • The production of extended-spectrum ${\beta}$-lactamases ($ESBL_S$) of the TEM or SHV type by bacterial pathogens is a major threat to the use of the clinically important expanded-spectrum cephalosporins. The characterization of the SHV ESBLs producing Klebsiella pneumoniae strains present in clinical isolates is time-consuming processes. We describe here in the development of a novel system, which consists of a real time PCR. We found 11 K. pneumoniae strains to be presumptive strains ESBLs producers by clinical and laboratory standards institute (CLSI) guidelines. The double disk synergy test showed 8 ESBL positive and conventional PCR showed 10 SHV ESBL positive, which were K. pneumoniae strains isolates. By real time PCR analysis, SHV gene in 11 of 11 strains were identified. When sequencing analysis was compared with real time PCR, both analysis were presented 99% similarity. In this study, we used a rapid, sensitive, and specific real-time PCR (RT-PCR) method for detection of the assay SHV ESBL producing K. pneumoniae strains in clinical isolates.

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기상합성공정을 이용한 FePt 나노입자의 실시간 L10 상변화 (Real-time Transformation of FePt Nanoparticles to L10 Phase by the Gas Phase Synthesis)

  • 이기우;이창우;김순길;이재성
    • 대한금속재료학회지
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    • 제49권1호
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    • pp.46-51
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    • 2011
  • Real-time formation of $L1_0$ phase of FePt nanoparticles in the gas phase during ultrasonic-spray pyrolysis is first discussed in the present study. Without any post heat treatment, $L1_0$ phase of FePt nanoparticles appeared at the temperature above $900^{\circ}C$ in the gas phase synthesis. X-ray diffractometry (XRD) and transmission electron microscopy (TEM) studies revealed that FePt nanoparticles less than 10 nm in size contained small volume of $L1_0$ fct phase. However, in other samples obtained at the temperature below $900^{\circ}C$, iron oxide phase co-existed and no evidence of phase transformation was found. Thus, it is anticipated that the time of flight of particles required for crystallization and phase transformation was extended according to the increase of the collision rate. Finally, magnetic properties represented by coercivity and saturation magnetization and functional groups on the particle surface were discussed based on VSM and FT-IR results.

실시간 XRD와 TEM을 이용한 MAPbI3의 온도 변화에 따른 구조 분석 (Investigation of Electron Thermally Induced Phase Transition in MAPbI3 Perovskite Solar Cells Using In-Situ XRD and TEM)

  • 최진석;엄지호;윤순길
    • 한국전기전자재료학회논문지
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    • 제32권1호
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    • pp.64-69
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    • 2019
  • Methylammonium lead triiodide ($MAPbI_3$)-based perovskite solar cells potentially have potential advantages such as high efficiency and low-cost manufacturing procedures. However, $MAPbI_3$ is structurally unstable and has low phase-change temperatures ($30^{\circ}C$ and $130^{\circ}C$); it is necessary to solve these problems. We investigated the crystal structure and phase separation using real-time temperature-change X-ray diffraction, transmission electron microscopy, and electron energy loss spectroscopy. $MAPbI_3$ has a tetragonal structure, and at about $35^{\circ}C$ the c-axis contracts, transforming $MAPbI_3$ into the related cubic crystal structure. In addition, at $130^{\circ}C$, phase separation occurs in which $CH_3NH_2$ and HI at the center of the unit cell of the perovskite structure are extracted by gas, leavingand only $PbI_2$ of the three-component structure, is produced as the final solid product.

TEM 관련 이론해설 (5): 원자집합체의 산란 (Scattering from Assemblies of Atoms)

  • 이확주
    • Applied Microscopy
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    • 제34권4호
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    • pp.211-221
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    • 2004
  • 물질을 이루고 있는 원자의 집합체에서 단 한번의 회절이 일어나는 경우의 회절이론의 개발을 소개하였다. Fourier transform으로 이루어지는 역 격자 공간에서의 역격자 공간 분포와 실 공간에서의 패터슨 함수와의 관계를 유도하고 이어 여러 가지 물질을 예로 들어 고찰하였다.

In-situ HRTEM Studies of Alumina-Aluminum Solid-Liquid Interfaces

  • Oh, Sang-Ho;Scheu, Christina;Ruhle, Manfred
    • Applied Microscopy
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    • 제36권spc1호
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    • pp.19-24
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    • 2006
  • The alumina-aluminum solid-liquid interfaces were directly observed at atomic scale by heating the alumina single crystal in high-voltage electron microscope (HVEM) owing to the electron beam damage processes, Atomic ordering in the first several layers of the liquid was clearly resolved adjacent to the alumina surface and its relevance to the single crystal growth was examined with the real-time observations.

In situ UHV TEM studies on nanobubbles in graphene liquid cells

  • Shin, Dongha;Park, Jong Bo;Kim, Yong-Jin;Kim, Sang Jin;Kang, Jin Hyoun;Lee, Bora;Cho, Sung-Pyo;Novoselov, Konstantin S.;Hong, Byung Hee
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.102-102
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    • 2016
  • Water, which is most abundant in Earth surface and very closely related to all forms of living organisms, has a simple molecular structure but exhibits very unique physical and chemical properties. Even though tremendous effort has been paid to understand this nature's core substance, there amazingly still lefts much room for scientist to explore its novel behaviors. Especially, as the scale goes down to nano-regime, water shows extraordinary properties that are not observable in bulk state. One of such interesting features is the formation of nanoscale bubbles showing unusual long-term stability. Nanobubbles can be spontaneously formed in water on hydrophobic surface or by decompression of gas-saturated liquid. In addition, the nanobubbles can be generated during electrochemical reaction at normal hydrogen electrode (NHE), which possibly distorts the standard reduction potential at NHE as the surface nanobubble screens the reaction with electrolyte solution. However, the real-time evolution of these nanobubbles has been hardly studied owing to the lack of proper imaging tools in liquid phase at nanoscale. Here we demonstrate, for the first time, that the behaviors of nanobubbles can be visualized by in situ transmission electron microscope (TEM), utilizing graphene as liquid cell membrane. The results indicate that there is a critical radius that determines the long-term stability of nanobubbles. In addition, we find two different pathways of nanobubble growth: i) Ostwald ripening of large and small nanobubbles and ii) coalescence of similar-sized nanobubbles. We also observe that the nucleation and growth of nanoparticles and the self-assembly of biomolecules are catalyzed at the nanobubble interface. Our finding is expected to provide a deeper insight to understand unusual chemical, biological and environmental phenomena where nanoscale gas-state is involved.

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항공 TEM 을 이용한 천해지역에서의 퇴적층 두께 및 기반암 심도 원격탐사에 관하여 (Towards remote sensing of sediment thickness and depth to bedrock in shallow seawater using airborne TEM)

  • Vrbancich, Julian;Fullagar, Peter K.
    • 지구물리와물리탐사
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    • 제10권1호
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    • pp.77-88
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    • 2007
  • 선행된 연구에서의 성공적인 수심도 작성 예에 뒤이어, 항공전자탐사를 이용한 해저면 특성파악 가능성이 고찰되었다. 헬리콥터에 탑재된 시간영역전자탐사 (TEM) 장비에서 얻어진 자료의 1D 역산으로부터 추정된 퇴적층의 두께가 해양 탄성파 연구에 기초하여 얻어진 추정치와 비교되었다. 일반적으로, 해수의 깊이가 대략 20 m이고 퇴적층의 두께가 40 m 미만이면 퇴적층의 두께 즉 비전도성 기반암까지의 깊이는 두 경우에 있어서 타당한 범위 내에서 일치됨을 보였다. 잡음이 섞인 합성자료의 역산은 초기 모형이 실제모형과 차이가 나는 경우에도 수직 전자탐사 유일성 이론과 일치하게 역산 후 실제모형과 매우 닮은 결과를 보여주었다. 잡음이 섞인 합성자료로부터 얻어진 천해 해수 깊이에 관한 표준편차는 대략 깊이의 ${\Box}5\;%$ 정도였으며, 이는 실제자료의 역산 시 대략 ${\pm}1\;m$ 정도의 오차를 우발할 수 있다. 이에 상응하는 기반암 깊이 추정의 불확실성은 대략 ${\pm}10\;%$에 이른다. 잡음이 포함된 합성자료로부터 얻어진 해수와 퇴적층의 평균 역산 두께는 대략 1 m 정도의 정밀도를 나타냈고, 중합에 의해 정밀도가 향상되었다. 주의 깊게 보정된 항공 TEM 자료를 이용하면 퇴적층의 두께와 기반암의 지형을 조사할 수 있다는 가능성을 알 수 있었으며, 천해에서의 해저면 저항치를 알아내기 위한 방법으로서의 가능성도 보여 주었다.

동촌유원지의 이용실태 및 변동분석 (Analysis on the Use Behavioral Patterns and Use Fluctuation over the Tong-Ch′on Amusement Park)

  • 김용수;임원현
    • 한국조경학회지
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    • 제15권1호
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    • pp.17-37
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    • 1987
  • The purpose of this study is to establish more rational and practical planning theory for amusement park. It analyze and consider the fluctuation of people who come and use the Tong-Ch'on amusement park. The results drawn from this reserch work are as follows; 1. The main visitors of the Tong-Ch'on amusement park are students in their twenties and thirties, and people whose incomes are below 300,000 Won a month. The purpose of visit is for a rest rather than for amusement and user prefer summer, while the user is so rare in wintertime. Those phenomena observed are somewhat different from the real purpose of a amusement park which is on purpose to make profits by offering entertainments to the users. So planner should pay attention to the three points. They are varieties, seasonable diversification and fantastic character of facilties, in the amusement park. 2. The access time of the Tong-Ch'on amusement park was 41 minutes, the use frequency was 4 times a year and resident time was 164 minutes. The relationship of the three factors are as follows; log Y(F) =1.7832-0.0277(A.T) R$^2$=0.75 Y(R. F)=31.8885+3.3217(A.T) R$^2$=0.53 Y(R. T)=224.8959-87.8309 1og(F) R$^2$=0.38 F;Use frequency(time/year) A.T;Access Time(minute) R.T;Resident Time(minute) 3. In the choice of space, there were much differences according to tole user's age, job, degree of education, companion type and purpose of use. 4. There are considerable correlation between use fluctuation and some factors. The factors are season(summer, winter) as a time, temperature, cloud amount, duration of sunshine, weather(rainy-day) as a climate and a day of the week(weekday, holiday) as a social system. The important variables are temperature, cloud amount, duration of sunshine and a day of the week(weekday, holiday) to estimate the user of amusementpark. 5. 1 can reduce the following two types of regression models. 1) log$\sub$e/ Y1 = 6.9114 + 0.l135 TEM + 0.00002 SUN -0.4068W1 + 0.4316 W3 (R$^2$= 0.94) 2) log$\sub$e/ Y2 = 7.2069 + 0.l177 TEM - 0.0990 CLO + 0.4880 W3 (R$^2$=0.95) Y; Number of User TEM; Temperature CLO; Amount of cloud SUN; Duration of Sunshine W1; Weekday W3; Holiday Those model is in order to estimate the user for management of Tong-Ch'on amusement park and use on the computation of facility sloe for reconstruction. Besides the amusement park, city park and outdoor recreation area could estimate of user through this method. But, I am not sure about the regression models because I did not apply the regression models to the other amusement park, city Park or outdoor recreation area. Therefore, I think that this problem needs to be studied on in the future.

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