• 제목/요약/키워드: Raw measurement

검색결과 394건 처리시간 0.021초

정량 구조 분석을 위한 Gibbsite 분말의 TEM 시편 준비법 (TEM Specimen Preparation Method of Gibbsite Powder for Quantitative Structure Analysis)

  • 김영민;정종만;이수정;김윤중
    • Applied Microscopy
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    • 제32권4호
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    • pp.311-317
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    • 2002
  • 입자 크기에 따라 상전이 경로가 달라지며 매우 큰 응집체로 존재하는 gibbsite 분말과 같은 재료의 정량적인 전이 구조 분석의 전제로서 입자 크기가 선택적인 TEM 시편의 준비가 절실히 요구된다. 입자 크기 선택성을 실현한 TEM 시편 준비의 방법론을 확립하기 위한 방안으로서 본 실험이 전개되었다. 약 1 wt%의 gibbsite 원료 분말을 에탄올 용매에 혼합 한 뒤, ball-milling에 의해 조분쇄 처리를 하고 증류수에 1 : 19의 비로 희석된 분산 조제, Darvan C, 0.25 vol%의 첨가와 함께 ultrasonic 처리를 하여 gibbsite suspension을 만들었다. 제조된 gibbsite suspension의 누적 농도 변화 관찰에 의한 침강 시간의 조정 후 정적 침강 분리에 의해 nm 크기별로 분리된 TEM 시편을 만들 수가 있었다. 시편의 전체적인 양상은 SEM으로 관찰하였고 개개 입자들의 morphology 는 TEM으로 분석하였다. 또한, 공정 과정 중의 상변화 가능성을 검토하기 위해 XRD 분석을 실시하였다.

MEASUREMENT OF THE CONCENTRATIONS OF RAW MATERIAL, SOYA OIL, AND PRODUCT, MANNOSYL ERYTHRITOL LIPID, IN THE FERMENTATION PROCESS USING NEAR-INFRARED SPECTROSCOPY

  • Kazuhiro Nakamichi;Suehara, Ken-Ichiro;Yasuhisa Nakano;Koji Kakugawa;Masahiro Tamai;Takuo Yano
    • 한국근적외분광분석학회:학술대회논문집
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    • 한국근적외분광분석학회 2001년도 NIR-2001
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    • pp.1157-1157
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    • 2001
  • Yeast, Kurtzurnanomyces sp. I-11, produces biosurfactant, mannosyl erythritol lipid (MEL), from soya oil. The properties of biosurfactant MEL include low-toxicity and high biodegradability. MEL provides new possibilities for a wide range of industrial applications, especially food, cosmetic, pharmaceutical fields and chemicals for biotechnology. In the fermentation process, techniques of measuring and controlling substrates and products are important to obtain high productivity with optimum concentrations of substrate and product in the culture broth. The measurement system for the concentrations of soya oil and MEL in the fermentation process was developed using near-infrared spectroscopy (NIRS). Soya oil and MEL in the culture broth were extracted with ethyl acetate and NIR spectra was carried out between the second derivative NIR spectral data at 1312 and 2040 nm and MEL concentrations obtained using a thin-layer chromatography with a flame-ionization detector (TLC/FID) method. A calibration equation for soya oil was results of the validation of the calibration equation, good agreement was observed between the results of the TLD/FID method and those of the NIRS method for both constituents. NIR method was applied to the measurement of the concentrations of MEL and soya oil in the practical fermentation and good results were obtained. The study indicates that NIRS is a useful method for measurement of the substrate and product in the glycolipid fermentation.

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The formation of Paper and the Measurement of Formation

  • Komppa, Olavi
    • 펄프종이기술
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    • 제29권2호
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    • pp.76-82
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    • 1997
  • In paper the evenness of planar distribution of mass in a small scale is called formation (orbetter:mass formation). Traditionally formation has been assessed visually, by looking the sheet of paper against transmitted light. Different kinds of optieal testers are being usd to obtain quantitative rankings htat would be independent of the observer but would well correspond to the visual assessment. However, various raw-material and process factors do influence light trans-mittance in paper and do impair the correspondence between basis weight and the optical formation measurement (or visual assessment). As the optical formation test methods do not incorporate an efficient calib ration routine, the formation of the sophisticated paper grades of today the is rather difficult to measure optically and may lead to erroneous results. It may be concluded that the optical measurement is not suitable for paper grades with high filler content. coating, heavy calendering or that are made of heavily beaten pulp, nordoes it apply for dyed or printed papers. For this reason, visual assessment and optical evaluation shoild be replaced with a measurement that gives reliable results independent on paper grode and manufacturing process. Formation measuremend based on beta radiation is suitable for all paper grades regardless to the material contents or process treatment. It is possible to measure even dyed or printed samples. Thonks to a sim ple and relioble calibration, the results are converted to real basis weight balues that remain reliable even with time. The only beta tester commercially available is the AMBERTEC Beta Formation Tester. Formation of paper does vary locally in the web. Typically there exists a formation profile, too similarly to other properties of paper. Therefore, formation should ? ays be expressed as a mean of a sufficient amount of parallel determinations. All formation measurements should be calibrated against basis weight.

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쌍축선 추진기 캐비테이션 소음 모형시험 연구 (A Study on the Model Test for the Twin Propeller Cavitation Noise)

  • 박철수;김건도;임근태;박영하;장현길;장영훈
    • 대한조선학회논문집
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    • 제55권1호
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    • pp.28-36
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    • 2018
  • The experimental results of the model tests for the twin propeller cavitation noise are presented. The model test was carried out by means of procedure of noise measurement followed by the signal processing and full-scale extrapolation. In order to convert the measured sound pressure level into the sound source level, transfer function measurements for three conditions were performed according to the combination of locations and number of virtual sources. White noise and LFM signal were used as a source signals to examine the influence of the input signal. For the twin propellers, 5 transfer functions were defined and the results were discussed. Cavitation noise measurement tests were performed similarly to the transfer function measurement test. Noise source localization analysis was performed to confirm the test effectiveness. It was confirmed that the source level of the twin propeller can be estimated reliably by using transfer function corrections. Finally, the model test results were converted into full-scale by applying the ITTC '87 model-ship scaling raw, and the validity of the model test was confirmed by comparison with the full-scale measurement result.

외복사근과 다열근에 대한 초음파 영상과 표면 근전도 측정방법의 신뢰도와 타당도 (Reliability and Validity of Ultrasound Imaging and sEMG Measurement to External Abdominal Oblique and Lumbar Multifidus Muscles)

  • 김창용;최종덕;김선엽;오덕원;김진경
    • 한국전문물리치료학회지
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    • 제18권1호
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    • pp.37-46
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    • 2011
  • The purpose of this study was to investigate intra-rater reliability and determine the validity of electromyography (EMG) measurements to represent muscle activity and ultrasonography (US) to represent muscle thickness during manual muscle testing (MMT) to external abdominal oblique (EO) and lumbar multifidus (MF). Twenty healthy subjects were recruited for this study and asked to perform MMT at differing levels. The subjects' muscle activity using EMG was measured by a ratio to maximum voluntary contraction (MVC) and root mean square (RMS) methods. The subjects' muscle thickness using US was measured by raw muscle thickness and change ratio of thickness to maximum (MVC) or resting condition. In three trials, measurements were performed on each subject by one examiner. The intra-rater reliability of measurements of EMG and US to EO and MF was calculated using intra-class coefficients. The intra-rater reliability of all measurements was excellent (ICC=.75~.98) in EMG and US. The conduct validity was calculated by one-way ANOVA with repeated measurements to compare whether the EMG and US measurements were different between MMT at different levels. There was only a significant difference between all grades at %MVC thickness measurement of US. These results suggest that a %MVC thickness measurement of US was a more sensitive and discriminate in all manual muscle testing grades. This information will be useful for the selection of US measurement and analysis methods in clinics.

Number of sampling leaves for reflectance measurement of Chinese cabbage and kale

  • Chung, Sun-Ok;Ngo, Viet-Duc;Kabir, Md. Shaha Nur;Hong, Soon-Jung;Park, Sang-Un;Kim, Sun-Ju;Park, Jong-Tae
    • 농업과학연구
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    • 제41권3호
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    • pp.169-175
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    • 2014
  • Objective of this study was to investigate effects of pre-processing method and number of sampling leaves on stability of the reflectance measurement for Chinese cabbage and kale leaves. Chinese cabbage and kale were transplanted and cultivated in a plant factory. Leaf samples of the kale and cabbage were collected at 4 weeks after transplanting of the seedlings. Spectra data were collected with an UV/VIS/NIR spectrometer in the wavelength region from 190 to 1130 nm. All leaves (mature and young leaves) were measured on 9 and 12 points in the blade part in the upper area for kale and cabbage leaves, respectively. To reduce the spectral noise, the raw spectral data were preprocessed by different methods: i) moving average, ii) Savitzky-Golay filter, iii) local regression using weighted linear least squares and a $1^{st}$ degree polynomial model (lowess), iv) local regression using weighted linear least squares and a $2^{nd}$ degree polynomial model (loess), v) a robust version of 'lowess', vi) a robust version of 'loess', with 7, 11, 15 smoothing points. Effects of number of sampling leaves were investigated by reflectance difference (RD) and cross-correlation (CC) methods. Results indicated that the contribution of the spectral data collected at 4 sampling leaves were good for both of the crops for reflectance measurement that does not change stability of measurement much. Furthermore, moving average method with 11 smoothing points was believed to provide reliable pre-processed data for further analysis.

경두개 자기자극 시 운동신경 유발응답 측정을 위한 근전도 측정 시스템 구축 (Establishing EMG Measurement System for Measurement of Motor Nerve Response in Transcranial Magnetic Stimulation)

  • 이근용;김수환;조재현;윤세진;이상식
    • 한국정보전자통신기술학회논문지
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    • 제12권4호
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    • pp.413-418
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    • 2019
  • 뇌와 관련된 질병(치매, 조현병, 우울증, 파킨슨병 등)을 가진 환자의 치료 및 재활 정도의 진행을 확인하고자 하는 연구가 현재 활발히 진행되고 있는 추세이다. 그 중에서 경두개 자기 자극법(Transcranial magnetic stimulation, TMS)은 뇌 질환이 있는 환자에게 비 침습적으로 뇌 신경 조절에 사용되는 기법이기 때문에 치료에 많이 사용되고 있다. 경두개 자기 자극 시 정상인의 근피로도는 증가하는 경향을 확인할 수 있다. 따라서 본 논문에서는 경두개 자기 자극 시에 운동 신경 유발 응답 측정을 위한 근전도 측정 시스템을 구축하여 피실험자의 Raw Data를 RMS 기법으로 분석하고, RMS 그래프의 경향을 통해 운동 신경 유발 응답 측정 시스템을 확인하고자 하는 것이 목표이다. 실험 방법으로는 피실험자의 위팔두갈래근의 수축과 이완 운동을 통해 피로한 상황까지 도달하게 한 후, 표면 근전도 기기를 통해 받아들인 원신호를 RMS 기법으로 분석한다. 실험 결과, RMS 그래프가 상승하는 경향을 확인 하였고, 이를 통해 구축된 근전도 측정 시스템으로 운동 신경 유발 응답을 측정한 데이터를 고려하여 개개인에 맞는 자기자극 강도 결정에 활용될 수 있을 것으로 사료된다.

A Novel Filtering Method Based on a Nonlinear Tracking Differentiator for the Speed Measurement of Direct-drive Permanent Magnet Traction Machines

  • Wang, Gaolin;Wang, Bowen;Zhao, Nannan;Xu, Dianguo
    • Journal of Power Electronics
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    • 제17권2호
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    • pp.358-367
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    • 2017
  • This paper presents a novel filtering method for speed measurements to improve the low-speed performance of the direct-drive permanent magnet traction machines for elevators. Based on the theory of nonlinear tracking differentiator (NTD), this method, which can act as a high performance filter of a raw speed signal, obtains a more accurate speed feedback signal when applying a low-resolution encoder. In addition, it can relieve the interference caused by the position derivative for speed sampling. By analyzing the frequency response of the NTD, the influence of its parameters on the performance of the speed filtering is investigated. Compared with different types of low-pass filters, the proposed method shows a shorter time delay and a stronger ability in terms of noise suppression when the parameters are selected carefully. In addition, when using the measured speed signal through a nonlinear tracking differentiator as the feedback of the system, the motor runs more steadily at low speeds. As a result, the riding comfort of a direct-drive elevator can be improved. The feasibility of the proposed strategy was verified on an 11.7kW elevator traction machine using a commercial inverter.

골프장갑의 착용실태 조사 및 기능성 향상을 위한 디자인 제안 (A Study on the Wearing Conditions of Golf Gloves and a Proposal for a Functional Glove Design)

  • 류현숙;최혜선;김은경
    • 대한가정학회지
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    • 제42권6호
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    • pp.89-101
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    • 2004
  • The aim of this study is to investigate problems with both fit and abrasion of golf gloves through a survey of golf usage among golfers over the age of 30, as well as by analyzing the golf glove industry with an emphasis on the size system and marketing situation. In addition, this study aims to suggest the basic raw materials for improving the design of golf gloves through physical properties inspections. The results of the analyses support the following suggestions. First of all, dissatisfaction arose from improper measurement in glove length. The survey showed that most problems occur in the pinky finger, while only the length of the middle finger of the glove is recorded based on Korean Standard Anthropometries Measurement. Clearly, proper measurements of every finger need to be included in the system. Secondly, the survey results clearly indicated regions 7(palm area) and 3(second finger area) as the areas requiring reinforcement. While the method of patching another layer with the same material is commonly used in the current glove market, materials other than genuine leather are unable to complement the abrasion. This study suggests that another layer of refill type genuine leather, which scored best in the physical properties inspection, needs to be patched onto regions 7 and 3.

PREPROCESSING EFFECTS ON ON-LINE SSC MEASUREMENT OF FUJI APPLE BY NIR SPECTROSCOPY

  • Ryu, D.S.;Noh, S.H.;Hwang, I.G.
    • 한국농업기계학회:학술대회논문집
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    • 한국농업기계학회 2000년도 THE THIRD INTERNATIONAL CONFERENCE ON AGRICULTURAL MACHINERY ENGINEERING. V.III
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    • pp.560-568
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    • 2000
  • The aims of this research were to investigate the preprocessing effect of spectrum data on prediction performance and to develop a robust model to predict SSC in intact apple. Spectrum data of 320 Fuji apples were measured with the on-line transmittance measurement system at the wavelength range of 550∼1100nm. Preprocess methods adopted for the tests were Savitzky Golay, MSC, SNV, first derivative and OSC. Several combinations of those methods were applied to the raw spectrum data set to investigate the relative effect of each method on the performance of the calibration model. PLS method was used to regress the preprocessed data set and the SSCs of samples, and the cross-validation was to select the optimal number of PLS factors. Smoothing and scattering corection were essential in increasing the prediction performance of PLS regression model and the OSC contributed to reduction of the number of PLS factors. The first derivative resulted in unfavorable effect on the prediction performance. MSC and SNV showed similar effect. A robust calibration model could be developed by the preprocessing combination of Savitzky Golay smoothing, MSC and OSC, which resulted in SEP= 0.507, bias=0.032 and R$^2$=0.8823.

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