• Korean Journal of Materials Research
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• v.22 no.10
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• pp.499-503
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• 2012

The present study is intended to comparatively investigate the changes in microstructure and tensile properties at room and elevated temperatures in commercial AM50(Mg-5%Al-0.3%Mn) and 0.3 wt%CaO added ECO-AM50 alloys produced by permanent mould casting. The typical microstructure of AM50 alloy was distinctively characterized using two intermetallic compounds, ${\beta}(Mg_{17}Al_{12})$ and $Al_8Mn_5$, along with ${\alpha}$-(Mg) matrix in an as-cast state. The addition of a small amount of CaO played a role in reducing dendrite cell size and quantity of the ${\beta}$ phase in the AM50 alloy. It is interesting to note that the added CaO introduced a small amount of $Al_2Ca$ adjacent to the ${\beta}$ compounds, and that inhomogeneous enrichment of elemental Ca was observed within the ${\beta}$ phase. The ECO-AM50 alloy showed higher hardness and better YS and UTS at room temperature than did the AM50 alloy, which characteristics can be mainly ascribed to the finer-grained microstructure that originated from the CaO addition. At $175^{\circ}C$, higher levels of YS and UTS and higher elongation were obtained for the ECO-AM50 alloy, demonstrating that even 0.3 wt%CaO addition can be beneficial in promoting the heat resistance of the AM50 alloy. The combinational contributions of enhanced thermal stability of the Ca-containing ${\beta}$ phase and the introduction of a stable $Al_2Ca$ phase with high melting point are thought to be responsible for the improvement of the high temperature tensile properties in the ECO-AM50 alloy.

• Korean Journal of Metals and Materials
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• v.47 no.12
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• pp.834-841
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• 2009

A study on the welding of electrogalvanized TRIP (Transformation-Induced Plasticity) steels was done to compare the life of the electrode and the alloying phenomena on the electrode tip surface using singlephase AC and inverter-DC resistance welding processes. A longer life of the electrode (>200 welds) was achieved using the inverter-DC welding process. The tensile shear strength was higher in the electrode life test when welded with the inverter DC welding machine it maintained a higher value even when the welding nugget diameter was smaller than specified. When spot-welding was conducted using the single-phase AC welding process, a higher wear rate of the electrode was observed compared to that with the inverter-DC process. An alloying layer used to determine the rate of electrode growth showed differences in the metallurgical features of the surface alloying and Zn penetration depending on whether the single-phase AC process or the inverter-DC welding process was used. Moreover, changes in the dynamic resistance during the electrode life test were correlated with the electrode wear (or growth) rate.

• Journal of the Korean Society for Heat Treatment
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• v.36 no.3
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• pp.161-173
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• 2023

This study investigated the effects of K_N and process time on the formation of a compound layer at a nitriding temperature of 540℃ for SCR420H material. As a result of controlled nitriding from 3 h to 20 h at K_N 1.2 atm^-1/2, compound layers were formed up to about 10 ㎛, and an effective hardening depth of about 460 ㎛ was obtained. Initially, an ε+γ' complex phase was formed, and the phase fraction changed over time, and finally, the fraction of ε phase decreased to less than 1%. With higher K_N, the compound thickness increased, a pore layer was formed on the surface, and the surface hardness decreased. By applying the controlled nitriding process, it was possible to produce annulus gears with a compound thickness of 12.8 ㎛ and an ε phase of 5% or less. The annulus gears made through controlled nitriding were mounted on a 6-speed transmission and tested for durability. As a result, the durability test of 250,000 km was satisfied, and the transmission efficiency was also confirmed to be expected.

• Analytical Science and Technology
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• v.19 no.6
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• pp.519-528
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• 2006

An analytical method for the determination of thyroid hormones in urine samples has been studied by using solid-phase extraction and high-performance liquid chromatography/diode array detector/electro-spray mass spectrometry. Seven thyroid hormones were successfully separated by gradient elution on the reverse phase Hypersil ODS column (4.6 mm I.D., 100 mm length, particle size $5{\mu}m$) with ammonium formate buffer and acetonitrile, and UV spectra and mass fragment could be confirmed. The extraction recoveries of thyroid hormones in the urine samples (pH 3) were in the range of 89.0-113.1% with solid-phase extraction by C18, followed by elution with 4 ml of methanol/ammonium hydroxide (9 : 1). The calibration curves showed good linearity with the correlation coefficients ($r^2$) varying from 0.992 to 0.998 and the detection limits of all analytes were obtained in the range of 2-4 ng/ml (3.8-13.0 pmol/ml).

• Journal of Ocean Engineering and Technology
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• v.26 no.3
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• pp.61-65
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• 2012

Air-water flow measurements are of importance for the coastal and ocean engineering fields. Although kinematic investigations of the multi-phase flows have been conducted for long time, velocity measurements still are concerned with many researchers and engineers in coastal and ocean areas. In the present study, an imaging technique using shadowgraphy and fiber optic probe for velocity measurements of air bubbles is introduced. The shadow graphy image technique is modified from the typical image velocimetry methods, and optical fibers are used for the well-known intrusive coupled phase-detection probe system. Since the imaging technique is a non-intrusive optical method from the air, it is usually applied for 2D flows. On the other hand, the double fiber optic probes touch flows regardless of flow patterns. The results of the flow measurements by both methods are compared and discussed. The methods are also applied to the measurements of overtopping flows by a breaking wave over the structure fixed on the free surface.

• ETRI Journal
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• v.33 no.4
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• pp.528-536
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• 2011

In this paper, we analyze the location accuracy of real-time locating systems (RTLSs) in multipath environments in which the RTLSs comply with the ISO/IEC 24730-2 international standard. To analyze the location error of RTLS in multipath environments, we consider a direct path and indirect path, in which time and phase are delayed, and also white Gaussian noise is added. The location error depends strongly on both the noise level and phase difference under a low signal-to-noise ratio (SNR) regime, but only on the noise level under a high SNR regime. The phase difference effect can be minimized by matching it to the time delay difference at a ratio of 180 degrees per 1 chip time delay (Tc). At a relatively high SNR of 10 dB, a location error of less than 3 m is expected at any phase and time delay value of an indirect signal. At a low SNR regime, the location error range increases to 8.1 m at a 0.5 Tc, and to 7.3 m at a 1.5 Tc. However, if the correlation energy is accumulated for an 8-bit period, the location error can be reduced to 3.9 m and 2.5 m, respectively.

• The Transactions of the Korean Institute of Power Electronics
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• v.4 no.6
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• pp.608-615
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• 1999

In this paper, the compliance control method was propoSL'Cl and the phase-difference operating principle of an u ultrasonic motor described. The compliance control can he implementtcD with spring/damper properties of the r musculo-skeletal system of the actual limb in controlling its net configuration and movement. The proposed p phase-difference driving scheme is verifitcD through the computer simulation. Also, $textsc{k}$rformance of the proposed c control method of a two-link direct-drive manipulator are examinLD by the experimental results with resptc'Ct to s spring/ damper properties.

• Journal of the Korean Applied Science and Technology
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• v.9 no.2
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• pp.107-117
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• 1992

The synthesis and solution properties of polyglycerol alkyl ether($R_{12}Gn$) are described. The phase behavior, surface tension, cloud point and HLB value of polyglycerol dodecyl ether in aqueous solution and in mixed solution of surfactant /water /oil have been investigated and compared with values of polyoxyethylene dodecyl ether. The surface tension showed that $R_{12}Gn$ have sufficiently low values of surface tension and cmc to serve as useful polyoxyethylene alkyl ether. The mesophases appearing in the $R_{12}Gn$ systems were more stable in a high temperature range than the mesophases of polyoxyethylene alkyl ether systems. The cloud point and HLB data indicated that addition of one glycerol group was equivalent to the addition of three oxyethylene group units, as far as the hydrophilic property was concerned. The phase diagrams of the polyglycerol alkyl ether /dodecane /water systems showed that the solubilizing and emulsifying powers of $R_{12}Gn$ were greater than those of polyoxyethylene alkyl ether. It is concluded that the polyglycerol chain can be even more useful as hydrophilic group of nonionic surfactants than the polyoxyethylene chain.

• Journal of Drive and Control
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• v.15 no.1
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• pp.1-9
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• 2018

The spool displacement of directional control valve can be considered as the standard signal to measure the bandwidth frequency of a directional control valve. When the spool displacement is not available, the metering-orifice system is implemented in this research as an alternative way of measuring the 90 degrees phase bandwidth frequency of the hydraulic directional control valve. The inertia effect on the transmission line oil induces the phase lead of the valve load pressure when compared with the phase of spool displacement. The capacitance effect of the oil induces the phase lag of the valve load pressure. The phase of the load pressure can be adjusted to be the same as that of the spool displacement by controlling the opening area of the metering orifice. A series of experiments were conducted to verify the effectiveness of the metering orifice. The 90 degrees phase bandwidth frequency measured from the valve load pressure was significantly deviated in some cases from the frequency of the spool displacement. The metering orifice was hard to be applied to measure the -90 degrees phase bandwidth frequency of the high precision.

• Journal of the Korean Society for Heat Treatment
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• v.28 no.3
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• pp.126-133
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• 2015

The aim of this study is to investigate the effect of solution treatment on the corrosion behavior of Mg-8%Al-(0-1)%Zn casting alloys in 1M NaCl aqueous solution. After the solution treatment, all alloys showed single ${\alpha}$-(Mg) phase microstructure by dissolution of ${\beta}(Mg_{17}Al_{12})$ phase into the ${\alpha}$-(Mg) matrix. The $H_2$ evolution volume decreased with an increase in Zn content, which indicates that the addition of Zn plays a beneficial role in decreasing corrosion rate of the Mg-Al-Zn alloy in solution-treated state. The microstructural evaluations on the corrosion products and corroded surfaces after the immersion test in 1 M NaCl solution revealed that the incorporation of more $Al_2O_3$ and ZnO into the corrosion product, by which the penetration of $Cl^-$ ions is impeded, are thought to be responsible for the better corrosion resistance in relation with the Zn addition.