• Title/Summary/Keyword: R&D Phase

Search Result 1,422, Processing Time 0.036 seconds

Stereoselective Transformation of Phytosphingosine to Safingol

  • Kim, Na-Ri;Lee, Sun-Hee;Namgoong, Sung-Keon
    • Bulletin of the Korean Chemical Society
    • /
    • v.30 no.3
    • /
    • pp.695-699
    • /
    • 2009
  • A short and efficient synthesis of (2S,3S)-safingol from commercially available D-ribo-(2S,3S,4R)-phytosphingosine is described. The highlights of the synthesis are a stereoselective one-pot transformation of a diol into an epoxide under phase transfer catalytic conditions and a regioselective epoxide-opening reduction with a hydride reagent.

Characteristics of Undrained Shear Behavior for Nak-Dong River Sand Due to Aging Effect (Aging 효과에 따른 낙동강 모래의 비배수 전단거동 특성)

  • Kim, Young-Su;Kim, Dae-Man
    • Proceedings of the Korean Geotechical Society Conference
    • /
    • 2005.03a
    • /
    • pp.916-923
    • /
    • 2005
  • In this study, to observe aging effect of undrained shear behavior for Nak-Dong River sand, undrained static and cyclic triaxial tests were performed with changing relative density ($D_r$), consolidation stress ratio($K_c$) and consolidation time. As a result of the test, the modulus of elasticity to all samples estimated within elastic zone by the micro strain of about 0.05% in case of static shear behavior increased with the lapse of consolidation time significantly, so aging effect was shown largely. Also strength of phase transformation point(S_{PT}$) and strength of critical stress ratio point($S_{CSR}$) increased with the lapse of consolidation time. Undrained cyclic shear strength($R_f$) obtained from the failure strain 5% increased in proportion to relative density($D_r$) and initial static shear stress($q_{st}$), $R_f$ of consolidated sample for 1,000 minutes increased about 10.6% compared to that for 10 minutes at the loose sand, and $R_f$ increased about 7.0% at the medium sand. In situ application range of $R_f$ to the magnitude of earthquake for Nak-Dong River sand was proposed by using a increasing rate of $R_f$ as being aging effect shown from this test result.

  • PDF

Development of Wide-Band Planar Active Array Antenna System for Electronic Warfare (전자전용 광대역 평면형 능동위상배열 안테나 시스템 개발)

  • Kim, Jae-Duk;Cho, Sang-Wang;Choi, Sam Yeul;Kim, Doo Hwan;Park, Heui Jun;Kim, Dong Hee;Lee, Wang Yong;Kim, In Seon;Lee, Chang Hoon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
    • /
    • v.30 no.6
    • /
    • pp.467-478
    • /
    • 2019
  • This paper describes the development and measurement results of a wide-band planar active phase array antenna system for an electronic warfare jamming transmitter. The system is designed as an $8{\times}8$ triangular lattice array using a $45^{\circ}$ slant wide-band antenna. The 64-element transmission channel is composed of a wide-band gallium nitride(GaN) solid state power amplifier and a gallium arsenide(GaAs) multi-function core chip(MFC). Each GaAs MFC includes a true-time delay circuit to avoid a wide-band beam squint, a digital attenuator, and a GaAs drive amplifier to electronically steer the transmitted beam over a ${\pm}45^{\circ}$ azimuth angle and ${\pm}25^{\circ}$ elevation angle scan. Measurement of the transmitted beam pattern is conducted using a near-field measurement facility. The EIRP of the designed system, which is 9.8 dB more than the target EIRP performance(P), and the ${\pm}45^{\circ}$ azimuth and ${\pm}25^{\circ}$ elevation beam steering fulfill the desired specifications.

Electro-Thermal Characteristics of Hole-type Phase Change Memory (Hole 구조 상변화 메모리의 전기 및 열 특성)

  • Choi, Hong-Kyw;Jang, Nak-Won;Kim, Hong-Seung;Lee, Seong-Hwan;Yi, Dong-Young
    • Journal of Advanced Marine Engineering and Technology
    • /
    • v.33 no.1
    • /
    • pp.131-137
    • /
    • 2009
  • In this paper, we have manufactured hole type PRAM unit cell using phase change material $Ge_2Sb_2Te_5$. The phase change material $Ge_2Sb_2Te_5$ was deposited on hole of 500 nm size using sputtering method. Reset current of PRAM unit cell was confirmed by measuring R-V characteristic curve. Reset current of manufactured hole type PRAM unit cell is 15 mA, 100 ns. And electro and thermal characteristics of hole type PRAM unit cell were analyzed by 3-D finite element analysis. From simulation temperature of PRAM unit cell was $705^{\circ}C$.

Application of Reversed-Phase Solid Phase Extraction for the HPLC Analysis of Microcystins in Water (다량 시료중 마이크로시스틴의 농축 및 분석)

  • Kim, Myeong-Hee;Kim, Tae-Seung;Kim, Tae-Keun;Park, Sun Ku
    • Analytical Science and Technology
    • /
    • v.13 no.3
    • /
    • pp.399-402
    • /
    • 2000
  • To determine the concentrations of microcystins present in lake water or in tap water using high performance liquid chromatography, it is necessary to concentrate a large volume of water samples (about 20 L) into very small volume (0.1-0.3 mL). Concentration can be conveniently done when disc type solid phase extraction (SPE) apparatus is used. Using this apparatus we have investigated the recovery rates of three kinds of microcystins, RR, YR, LR. The recovery rates were relatively low and the reproducibilities were not good either. It is expected, however, that the appropriate selection of the disc conditioning and eluting solvents and reproducible reconcentration process after SPE will improve both the recovery rates and the reproducibilities.

  • PDF

Manufacturing Process of Translucent Microemulsion and Its Stability (Translucent Microemulsion의 제조 공정과 안정성)

  • Bae, Duck-Hwan;Shin, Jae-Sup
    • Journal of the Korean Applied Science and Technology
    • /
    • v.17 no.3
    • /
    • pp.167-173
    • /
    • 2000
  • The process variables for the manufacture of translucent microemulsion prepared with 2-octyl dodecanol, 12-hydroxy stearic acid cholesteryl , POE(40)HCO and 1,3-butandiol were examined initially (primary emulsion) and following aging for three months. The techniques empolyed in this study were particle size, turbidity, interfacial tension and microfluidizer. Particle size analysis and turbidity measurement to evaluate the emulsion stability were used. It was concluded that the process of the emulsification was an important indicator of the stability of the translucent microemulsion. From the particle size and and turbidity measurement of translucent microemulsion, adding the surfactant to the oil phase before the emulsification was found to be the most important factor for the stability of emulsions. We found that interfacial tension of the adding the surfactant to the oil phase is lower than that of the adding the surfactant to aqueous phase. In spite of hydrophilic surfactant, adding the surfactant to aqueous phase produced inferior emulsion to that to oil phase.

A Study on the Preparation of a Linear Low Density Polyethylene particles by Thermally Induced Phase Separation (열유도 상분리에 의한 선형 저밀도 폴리에틸렌 입자 제조에 관한 연구)

  • Park, Keun-Ho;Jang, Young-Min
    • Journal of the Korean Applied Science and Technology
    • /
    • v.28 no.4
    • /
    • pp.386-392
    • /
    • 2011
  • We are crystallized to the linear low density polyethylene(LLDPE) particles by a thermally induced phase separation(TIPS). TIPS process based on the phase separation mechanism was performed for the LLDPE system which undergoes liquid-solid phase separation. The linear low density polyethylene particle formation occurred by the nucleation and growth mechanism in the metastable region. Although the growth rates depended on the experimental conditions such as the polymer concentration and temperature, the particles were larger when the polymer concentration was higher or temperature was higher. The particles were observed by SEM. The LLDPE particle size distribution became broader when the polymer concentration was higher.

Novel two phase interleaved LLC series resonant converter using a phase of the resonant capacitor

  • Yi, Kang-Hyun;Moon, Gun-Woo;Heo, Tae-Won
    • Proceedings of the KIPE Conference
    • /
    • 2008.06a
    • /
    • pp.526-528
    • /
    • 2008
  • LLC series resonant converter has many unique characteristics and improvement over PWM topologies. However, many output capacitors should be needed in parallel to satisfy an output voltage ripple and a rated ripple current of the capacitors. This paper is deal with a novel two phase interleaved LLC resonant converter using a phase of the resonant capacitor. The proposed converter can satisfy output voltage ripple and a rated ripple current of capacitors with few output capacitors, relatively. The operation and features is considered in detail and a prototype with a 12V-100A output is investigated.

  • PDF

A Study on the Torque Performance to Capacitance of a Capacitor-run type Single Phase Induction Motor

  • Kim Cherl-Jin;Choi Chul-Yong;Baek Soo-Hyun
    • KIEE International Transaction on Electrical Machinery and Energy Conversion Systems
    • /
    • v.5B no.1
    • /
    • pp.20-26
    • /
    • 2005
  • Various kinds of practical machines using the single phase induction motor (SPIM) are utilized to control both speed and torque. In particular, the capacitor-run type SPIM has the characteristic that allows the motor torque to be altered by auxiliary capacitance variation. In this study, we manifest an equivalent model having a more simplified configuration, and clarify the relationship between torque and capacitance. Also, we design an experimental controller that is able to perform speed control with ease by the phase angle control of the AC input voltage. Validity of this study is confirmed through the simulation and experimental results obtained.

Developed Ability of Zero-phase Overcurrent Relay by Changed setting point value (설정치 변경에 의한 영상과전류계전기의 성능개선)

  • Kim, N.H.;Yoon, D.S.;Chang, S.I.;Choi, J.H.
    • Proceedings of the KIEE Conference
    • /
    • 1998.11a
    • /
    • pp.220-222
    • /
    • 1998
  • This paper presents a method, which develops an ability of Zero-phase Overcurrent Relay. Zero-phase current is very useful factor of Fault decision in Protect Relaying system. Actually, the setting-point value of Designed Relay, using Zero-phase current, is fixed. So in the case of deciding fault, Fixed setting-point value is not suitable for changing Load. and cause errors in Distributions system. For solving this problem, This paper proposes the Changed setting point value Algorithm, which can be adaptive for changing Distributions system using Zero-phase current r.m.s. indexes. The results of simulation under Load changing and High impedance fault show that proposed algorithm is useful for changing Distributions system and decreasing errors.

  • PDF