• Korean Journal of Heritage: History & Science
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• v.35
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• pp.138-158
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• 2002

To compare and analyze technical system related to manufacturing of ironware during the period of the Three Kingdoms, an analysis was conducted on the minute system of metalwork, as study objects, of the remains of the Mt. Wolpyeong fortress wall in Daejeon in the period of capital during the era of the Three Kingdoms in the 5th century, the Sanwol-ri remains in the 6th century in Gunsan and the remains of ironware excavated from the great ancient tomb of Hwangnam of the Silla dynasty in the 5th century. The result of analysis shows that in the most of the casting products, the minute system of white cast iron were contained. While the iron part of decarbonization was in the system by casting as white cast iron in the central part, on the surface layer it was turned out that comparatively uniform 100% pearlite system of about 1~2mm degree was existing. The part of pearlite on the surface layer was caused by decarbonization, which appears in all the parts of blade front end and handle. Therefore, it was found that the iron part of decarbonization was manufactured by casting, and then was processed at the high temperature by decarbonization. For the products of forging, after processing the products on the basis of pure iron for materials, they manufactured the ironware that raises the strength by carbonizing that keeps carbon infiltrated on the necessary part, by the method of black smith welding that add pure iron to steel, or by varying the method of heat processing onto the part required of strength. Though limited, we could understand that the technical systems for manufacturing skill of ironware in the areas of Baekje and Silla were different each other. In the technical system for Hwangnam great ancient tomb in the Silla area, it is found that they had raised the strength on the necessary part by applying the steelmaking method of carbonizing in the last stage of production of products, in the meantime in Baekje area, it appears that they had produced steel in advance in the first stage of production of the products, and used the produced steel only to the necessary part.

• Journal of the Korean Society of Safety
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• v.35 no.5
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• pp.128-136
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• 2020

In the present experimental study, the effect of water-based iron(III) oxide nanofluid on the MFB(Minimum Film Boiling) point during quenching was investigated. As the highly heated test specimen, the cylindrical stainless steel rod was used, and as the test fluids, the water-based iron(III) oxide nanofluids of 0.001 and 0.01 vol% concentrations were prepared with the pure water. To examine the effect of location in the test specimen, the thermocouples were installed at the bottom and middle of wall, and center in the test specimen. Through a series of experiments, the experimental data about the influences of nanofluid concentrations, the number of repeated experiments, and locations in the test specimen on the reaching time to MFB point, MFBT(Minimum Film Boiling Temperature), and MHF(Minimum Heat Flux) were obtained. As a result, with increasing the concentration of nanofluid and the number of repeated experiments, the reaching time to MFB point was reduced, but the MFBT and MHF were increased. In addition, it was found that the effect of water-based iron(III) oxide nanofluid on the MFB point at the bottom of wall in the test specimen was observed to be greater than that at the middle of wall and center. In the present experimental ranges, as compared with the pure water, the water-based iron(III) oxide nanofluid showed that the maximum reduction of reaching time to MFB point was about 53.6%, and the maximum enhancements of MFBT and MHF were about 31.1% and 73.4%, respectively.

• The Bulletin of The Korean Astronomical Society
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• v.38 no.1
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• pp.49.1-49.1
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• 2013

We have been carrying out near-infrared (NIR) spectroscopy as well as [Fe II] narrow band imaging observations of Cassiopeia A supernova remnant (SNR). In this presentation, we describe the spectral classification of the iron knots around the SNR. From eight long-slit spectroscopic observations for the iron-bright shell, we identified a total of 61 iron knots making use of a clump-finding algorithm, and performed principal component analysis in an attempt to spectrally classify the iron knots. Three major components have emerged from the analysis; (1) Iron-rich, (2) Helium-rich, and (3) Sulfur-rich groups. The Helium-rich knots have low radial velocities (${\mid}v_r{\mid}$ < 100 km/s) and radiate strong He I and [Fe II] lines, that match well with Quasi-Stationary Flocculi (QSFs) of circumstellar medium, while the Sulfur-rich knots show strong lines of oxygen burning materials with large radial velocity up to +2000 km/s, which imply that they are supernova ejecta (i.e. Fast-Moving Knots). The Iron-rich knots have intermediate characteristics; large velocity with QSF-like spectra. We suggest that the Iron-rich knots are missing "pure" iron materials ejected from the inner most region of the progenitor and now encountering the reverse shock.

• Fashion & Textile Research Journal
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• v.10 no.6
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• pp.822-826
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• 2008

The data for application of mordanting is shown in this experiment by researching dying properties of iron-dye process and concentration changes using persimmon. The strength of persimmon-dying fabrics was controlled by diluting persimmon dye with water and iron mordanting showed the possibility of textile design. The experiments were performed with various conditions processed with iron mordanting liquid by adding water to persimmon-dying liquid and drying well. The most dark color of fabric is observed with the pure persimmon dying without adding water. As the adding water is increased, the color of the fabric is getting lighter with the amount of adding water. After process of iron mordanting, dark color of the fabric turns into dark grey and light color turns into light grey. The possibility of persimmon dying with fabric can be applied in the design of textile with deepened color.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.5
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• pp.379-386
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• 2008

Densification behavior of dissimilar material powder (copper and pure iron powder) under die compaction was investigated. Experimental data were obtained for copper and pure iron powder compacts with various volume ratios under die compaction. Dissimilar material powder was simultaneously compacted into a jointed cylindrical compact with different powder materials in inner and outer part, respectively. To simulate densification behavior of dissimilar material powder, elastoplastic constitutive equation proposed by Shima and Oyane was implemented into a finite element program (ABAQUS) under die compaction. Finite element results were compared with experimental data for densification, deformed geometry and density distribution of powder compacts under die compaction.

• Journal of the Korean earth science society
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• v.25 no.1
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• pp.48-51
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• 2004

The light element candidates such as S, O, Si, and K are discussed for the reasonable compositions in the earth's core since the available data show density difference from pure iron core. These candidates are favored by the some evidences such as depletion in the crust and mantle, and lower eutectic temperature of Fe-FeS melt for sulfur. FeO phase for oxygen, lighter mass than sulfur and solubility in metallic phases for silicon, and partitioning in Fe-FeS melt for potassium. However, other problems such as short experimental data, initial compositions of these elements, and oxidation state during the formation of the earth should be solved simultaneously to confirm these light elements.

• Journal of Magnetics
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• v.17 no.2
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• pp.83-85
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• 2012

Magnetic particles in a novel, wound-healing ointment were studied using M$\ddot{o}$ssbauer spectroscopy and VSM to estimate the stability of the properties of the magnetic particles. The isomer shifts of $Fe_3O_4(A)$ were found to be 0.49-0.56 mm/s relative to iron metal, this indicates that the iron ions in $Fe_3O_4(A)$ are $Fe^{3+}$. On the other hand, the isomer shifts of $Fe_3O_4(B)$ were found to be 0.91-1.13 mm/s relative to iron metal, this shows that the ion state of $Fe_3O_4(B)$ is a mixed state of $Fe^{2+}$ and $Fe^{3+}$. It is noted that this composition, as well as that of the initial pure component in the form of a highly dispersed fraction (${\sim}10\;{\AA}$), differs from the stoichiometric one. It was found that the area ratio of the M$\ddot{o}$ssbauer subspectra of $Fe_3O_4(A)$ / $Fe_3O_4(B)$ taken at 87 and 181 K linearly increased in comparison to the initial pure magnetic particles, but the rate of increase of the area ratio at 181 K was about two times that at 87 K. From the magnetic hyperfine field, despite their small size, the particles exhibit no superparamagnetism.

• Journal of Powder Materials
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• v.14 no.1 s.60
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• pp.19-25
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• 2007

This study was focused on the optimization of low-pressure ultrasonic spraying process for synthesis of pure ${\gamma}-Fe_2O_3$ nanoparticles. As process variables, pressure in the reactor, precursor concentration, and reaction temperature were changed in order to control the chemical and microstructural properties of iron oxide nanoparticles including crystal phase, mean particle size and particle size distribution. X-ray diffraction (XRD) and transmission electron microscopy (TEM) studies revealed that pure ${\gamma}-Fe_2O_3$ nanoparticles with narrow particle size distribution of 5-15 nm were successfully synthesized from iron pentacarbonyl ($Fe(CO)_{5}$) in hexane under 30 mbar with precursor concentrations of 0.1M and 0.2M, at temperatures over $800^{\circ}C$. Also magnetic properties, coercivity ($H_c$) and saturation magnetization ($M_s$) were reported in terms of the microstructure of particles based on the results from vibration sampling magnetometer (VSM).

• 한국문화재보존과학회:학술대회논문집
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• 2004.10a
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• pp.33-42
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• 2004

The forged iron axe found in the No. 2 wood-framed tomb (the middle 3rd century) of Hwangseongdong, Gyeongju is rectangular on the plane level. It shows an obtuse angle in the edge part, while the joint part has the both sides folded up and shows the traces of wood. Under the reflected light, the Iron axe shines in metal luster, which is bright light gray or light creamy colors. The result of x-ray diffraction analysis shows that the axe consists of magnetite and geothite, which can explain why the composition and structure of the original ore has been kept intact. The microtexture of the axe has the irregular network of ferrite and pearlite, and tile cementite of tiny amount in the ferrite background. The overall treatment of the texture seems to be thermal with a high ratio of carbon. There are fine-grained magnetite, wolframite, quartz, calcite, mica, hornblende and pyroxene inside the axe. Those must be the impurities that they failed to remove in the refining process. The normal ferrite is composed of pure iron whose $Fe_2O_3$ proportion is from 99.16 to $99.84\;wt.\%$. Other than them, the ferrite parts usually contain $Al_2O_3\;and\;SiO_2$. The irregular network of pearlite also contains Impurities including $Al_2O_3\;and\;SiO_2$ and shows highly diverse patterns of carbon content. It's because the axe was carburized after the material was made to resemble pure iron. The decarbonization work didn't go well along the process marks. It's estimated that the original ore was bloom produced in low-temperature reduction and formed around in $727^{\circ}C$, which is eutetic temperature.

• Proceedings of the Korean Institute of Resources Recycling Conference
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• 1993.03a
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• pp.4.2-4
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• 1993