• Title/Summary/Keyword: Pure Co

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Extraction Efficiencies of Organophosphorus Pesticides Spiked in Fish Tissues by Supercritical Carbon Dioxide (초임계 이산화탄소에 의한 어류조직 중 유기인계 농약의 첨가회수율)

  • Lim, Sang-Bin;Jwa, Mi-Kyung
    • Korean Journal of Food Science and Technology
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    • v.30 no.5
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    • pp.1163-1168
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    • 1998
  • Fish tissues were spiked with organophosphorus pesticides (OPPs), mixed with a celite as a drying agent, and dynamically extracted with pure $CO_2$ or modified $CO_2$ for 10 min at different extraction temperatures, pressures and $CO_2$ flow rates. Recoveries of OPPs spiked in jacopever increased with the decrease of extraction temperature and pressure, and decreased with the increase of $CO_2$ flow rates. Modified $CO_2$ extractions with 10% methylene chloride showed a slight increase in the recoveries over pure $CO_2$ extraction. Quantity of fish tissues had great effect on their extraction efficiencies. Recoveries of OPPs were $66.7{\sim}86.3%$ for jacopever, $56.2{\sim}79.2%$ for yellow tail, $57.6{\sim}77.8%$ for blanquillo, $84.2{\sim}96.3%$ for sardine, $74.6{\sim}83.6%$ for mackerel. Application of supercritical carbon dioxide extraction offers an attractive alternative to the use of organic solvents for extraction of pesticide residues from fish tissues.

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Extraction of Glabridin from Licorice Using Supercritical Carbon Dioxide (초임계 이산화탄소를 이용한 감초 중의 glabridin 추출)

  • Cho Yun-Kyoung;Kim Hyun-Seok;Kim Ju-Won;Lee Sang-Yun;Kim Woo-Sik;Ryu Jong-Hoon;Lim Gio-Bin
    • KSBB Journal
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    • v.19 no.6 s.89
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    • pp.427-432
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    • 2004
  • The purpose of this study is to investigate the feasibility of a cosolvent-modified supercritical $CO_2\;(scCO_2)$ extraction technique for the production of licorice extracts with high levels of glabridin. The effects of various parameters such as the type and amount of modifiers, extraction temperature ($40{\sim}80^{\circ}C$) and pressure ($10{\sim}50.0\;MPa$) on the extraction efficiency were examined at a fixed flow rate of 1 mL/min. The organic solvent extraction with pure methanol was also conducted for a quantitative comparison with the $scCO_2$ extraction. The recovery of glabridin from licorice was found to be extremely small for pure $scCO_2$. However, the addition of modifiers such as ethanol and acetone to $scCO_2$ resulted in a significant improvement in the recovery of glabridin. The recovery of glabridin was observed to increase with pressure at a constant temperature. Furthermore, the purity of the glabridin obtained from the $scCO_2$ extraction was higher compared with the organic solvent extraction.

Synthesis and Magnetic Properties of Body-centered-tetragonal Fe-Co Alloy (체심정방정 구조 Fe-Co계 합금상의 합성 및 그 자기적 특성)

  • Kim, K.M.;Kwon, H.W.;Lee, J.G.;Yu, J.H.
    • Journal of the Korean Magnetics Society
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    • v.27 no.4
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    • pp.129-134
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    • 2017
  • Bulk-type body-centered-tetragonal Fe-Co alloy was synthesised by utilising a conventional alloy preparation technologies, such as melting, solidification, and homogenising treatments, and its magnetic properties were investigated. In the $(Fe_{100-x}Co_x)_{1-y}C_y$ alloy, the composition range, from which single phase body-centered-tetragonal alloy (martensite phase) was obtained, was severely limited: Co content x = 2.5, and C content y = 0.062. Tetragonality(c/a) of the synthesised body-centered-tetragonal $(Fe_{97.5}Co_{2.5})_{0.938}C_{0.062}$ alloy was 1.05. Magnetocrystalline anisotropy constant ($K_1$) of the body-centered-tetragonal $(Fe_{97.5}Co_{2.5})_{0.938}C_{0.062}$ alloy was measured to be $9.8{\times}10^5J/m^3$), which was 3.1 time as high as the pure iron (${\alpha}-Fe$).

THE CURVATURE OF HALF LIGHTLIKE SUBMANIFOLDS OF A SEMI-RIEMANNIAN MANIFOLD OF QUASI-CONSTANT CURVATURE

  • Jin, Dae Ho
    • The Pure and Applied Mathematics
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    • v.19 no.4
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    • pp.327-335
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    • 2012
  • We study half lightlike submanifolds M of semi-Riemannian manifolds $\widetilde{M}$ of quasi-constant curvatures. The main result is a characterization theorem for screen homothetic Einstein half lightlike submanifolds of a Lorentzian manifold of quasi-constant curvature subject to the conditions; (1) the curvature vector field of $\widetilde{M}$ is tangent to M, and (2) the co-screen distribution is a conformal Killing one.

TWO CHARACTERIZATION THEOREMS FOR HALF LIGHTLIKE SUBMANIFOLDS OF AN INDEFINITE KENMOTSU MANIFOLD

  • Jin, Dae Ho
    • The Pure and Applied Mathematics
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    • v.21 no.1
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    • pp.1-10
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    • 2014
  • In this paper, we study the curvature of locally symmetric or semi-symmetric half lightlike submanifolds M of an indefinite Kenmotsu manifold $\bar{M}$, whose structure vector field is tangent to M. After that, we study the existence of the totally geodesic screen distribution of half lightlike submanifolds of indefinite Kenmotsu manifolds with parallel co-screen distribution subject to the conditions: (1) M is locally symmetric, or (2) the lightlike transversal connection is flat.

A Study on the Preparation and Properties of Cellulose-EVOH Fibers (Cellulose-EVOH 섬유의 제조와 물성에 관한 연구)

  • 문병화;임상규;손태원;김삼수
    • Textile Coloration and Finishing
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    • v.10 no.5
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    • pp.19-23
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    • 1998
  • In this study, Cellulose-Poly(Ethylene-Co-Vinyl Alcohol) (EVOH) fibers from MMNO(N-me-thylmorpholine-N-oxide) /water/cellulose/EVOH were prepared according to changes of EVOH content(wt%), which is main factors to dry-jet wet spinning. The mechanical properties and morphology of produced fibers were investigated. The resultant fibers had tensile strength of 3.7∼4.5g/d, elongation of 3.3∼7.5% and exhibited lower density than the density of pure cellulose fiber.

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The Effect of Alloy Microstructure on the Behavior of Pd and Pd-based Alloy towards H2

  • Lee, Hyun Kyu;Noh, Hak
    • Transactions of the Korean hydrogen and new energy society
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    • v.11 no.3
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    • pp.97-105
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    • 2000
  • The influence of different microstructures and compositional variations on hydrogen absorption by pure Pd, and $Pd_{0.9}Rh_{0.1}$ alloy has been examined from changes in the hydrogen isotherms. The dilute phase solubilities and the plateau pressures are affected by differences in microstructures and compositional variations but the hydrogen capacities at relatively high hydrogen pressures are not affected except for the alloy form which has some phase separation.

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ISOTOPIC-SPECTRAL DETERMINATION OF CARBON IN HIGH PURITY INORGANIC MATERIALS

  • Lee, V.N.;Nemets, V.M.
    • Analytical Science and Technology
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    • v.8 no.4
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    • pp.477-480
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    • 1995
  • Isotopic-spectral method [I] was applicated for determination of carbon in silicate materials (pure silica, guartz glasses, geological probs etc.). Isotopic heterogeneous balancing of carbon in gaseous phase and solid samples was carried out at the temperature of $1500-1900^{\circ}K$. Spectroscopic measuring of isotope concentration in a balanced gas was made using the electron-vibrational band heads of CO molecules excited in HF discharge. Limits of detection of carbon concentrations appear to be $n^*10^{-6}$.

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