• Title/Summary/Keyword: Pulsed current activated combustion synthesis

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Mechanical Properties and Fabrication of Nanostructured 2MoSi2-SiC by Pulsed Current Activated Combustion Synthesis (펄스 전류 활성 연소합성에 의한 나노구조의 2MoSi2-SIC제조 및 기계적 성질)

  • Shon, In-Jin;Kim, Dong-Ki;Jeong, In-Kyoon;Doh, Jung-Mann;Yoon, Jin-Kook;Ko, In-Yong
    • Journal of Powder Materials
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    • v.14 no.4
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    • pp.245-250
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    • 2007
  • Dense nanostructured $2MoSi_{2}-SiC$ composites were synthesized by the pulsed current activated combustion synthesis (PCACS) method within 3 minutes in one step from mechanically activated powders of $Mo_{2}C$ and 5Si. Simultaneous combustion synthesis and densification were accomplished under the combined effects of a pulsed current and mechanical pressure. Highly dense $2MoSi_{2}-SiC$ with relative density of up to 96% was produced under simultaneous application of a 60 MPa pressure and the pulsed current. The average grain size of $MoSi_{2}$ and SiC were about 120 nm and 90 nm, respectively. The hardness and fracture toughness values obtained were 1350 $kg/mm^{2}$ and 4 $MPa{\cdot}m^{1/2}$, respectively.

Fabrication of 4.25 Co0.53Fe0.47-Al2O3 Composite by High FrequencyInduction Heated Combustion Synthesis and Sintering (펄스 전류 활성 연소합성과 소결에 의한 4.25 Co0.53Fe0.47-Al2O3 복합재료제조)

  • Lee, Dong-Mok;Jo, Kwang-Myoung;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.47 no.6
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    • pp.344-348
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    • 2009
  • Dense $4.25Co_{0.53}Fe_{0.47}-Al_{2}O_{3}$ composite was simultaneously synthesized and consolidated by pulsed current activated combustion method within 2 min from mechanically activated powders. Consolidation was accomplished under the combined effects of a pulsed current and mechanical pressure. Dense $4.25Co_{0.53}Fe_{0.47}-Al_{2}O_{3}$ with relative density of up to 96% was produced under simultaneous application of 80 MPa pressure and the pulsed current. Fracture toughness and hardness of the composite are $6MPa{\cdot}m^{1/2}$ and $570kg/mm^{2}$ respectively.

The Effect of Rapid Consolidation of Nanostructured MoSi2-SiC Composite on its Mechanical Properties (나노구조 몰리브덴늄실리사이드-실리콘카바이드 복합재료의 급속소결과 기계적 성질)

  • Ko, In-Yong;Chae, Seung-Myoung;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.48 no.5
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    • pp.417-423
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    • 2010
  • A dense nanostructured MoSi$_{2}$-SiC composite was synthesized by a pulsed current activated combustion synthesis method within 2 min of one step from mechanically activated powders of Mo$_{2}$C and Si. Simultaneous combustion synthesis and consolidation were accomplished under the combined effects of a pulsed current and mechanical pressure. Highly dense MoSi$_{2}$-SiC with a relative density of up to 98% was produced under simultaneous application of an 80 MPa pressure and pulsed current. The average grain size and mechanical properties of the composite were investigated.