• Title/Summary/Keyword: Pulling Rate

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LiF 단결정 성장에서 고체-액체의 계면형상 (Solid-liquid Interface Shape in LiF Single Crystal Growth)

  • 정대식;오근호
    • 한국세라믹학회지
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    • 제21권3호
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    • pp.271-277
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    • 1984
  • To study interface between crystals grown and molten state in the crusible. Pulling and rotating rate of the shaft were varied in LiF crystal growth by Czochralski method. Lower speed of the pulling and rotating rate increased the degree of convexity in solid-liquid interface and higher speed of the pulling and rotating rate decreased it. Optimum condition of LiF crystal growth obtained as pulling rate was 6.5cm/h when it rotated as 46rpm.

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초크랄스키 실리콘 단결정에서 인상 속도의 거시적 변동이 OSF-링 형성에 미치는 영향 (Effect of a Macroscopic Fluctuation in Pulling Rate on the Formation of OSF-ring Cz-Si SIngle Crystal)

  • 박봉모;서경호;김건
    • 한국결정학회지
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    • 제11권3호
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    • pp.157-161
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    • 2000
  • In a 200nm Cz-Si crystal, a macroscopic fluctuation in pulling rate was intentionally introduced an then the variations of the pulling rate and the position of OSF-ring were compared each other. The formation behavior of OSF-ring in the effective volume, defined as the region between the growth interface position -α and the growth interface position +α, is most affected by the pulling rate fluctuation. To understand the correct effect of a macroscopic pulling rate fluctuation, its cumulative effect in the effective volume should be considered. A new concept of modeling for it was proposed here.

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$Bi_{12}GeO_{20}$단결정 육성 및 표면탄성파 소자 제조 (Growth of Optical Quality $Bi_{12}GeO_{20}$ Crystals and Preparation of SAW-Filter)

  • 이태근;정수진
    • 한국결정학회지
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    • 제2권2호
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    • pp.32-40
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    • 1991
  • The effects of compositional variation, rotation speel and pulling rate on the growth of optical quality Bi120e02(1 crystals were examined. It was found to flatten the shape of crystal-melt interface for yowing a single crystals less than about 30mm in diameter at the rotation speed of 50rpm. Diameter of crystals with flat interface was increased as the pulling rate. The precipitation of Bi40e3012 phase set limits to pulling rate of BGO crystals. Precipitate-free BGO crystals were grown under pulling rate of 2mm l hr which released the stress resulted from too hi어 Pulling rate, and from 6. IBi203·GeO2 batch composition obtained by addition of 0.1 mole Bi203 into Bi-deficient melts to fill up the deficiency resulted from gradual volatilization of Bi2O). The pale-yellow colored crystals had good quality in that dislocation density was less than 103pits/cm, and it also exhibited transmittance of 70% and optical activity of 23°/mm. and SAW velosity was measured 1700m/sec on 111 cut 110 propagating BGO crystals. The SAW filter with electrode thickness of 9.8um was fabricated by using the electron beam and dry etching technique, it makes Bi12GeO20 devices intersting for color TV IF with half device size.

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초크랄스키 실리콘 단결정에서 인상 속도의 거시적 변동이 성장 결함 형성에 미치는 영향 (Effects of a Macroscopic Fluctuation in Pulling Rate on the Formation of Grown-in Defects in Cz-Si Single Crystal)

  • 박봉모;서경호;김건
    • 한국결정학회지
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    • 제11권4호
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    • pp.200-206
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    • 2000
  • In a 200 mm Cz-Si crystal, a macroscopic fluctuation in pulling rate was intentionally introduced then the variations of the pulling rate and the formation behaviors of grow-in defects were compared. The diameters of the OSF-ring and the FPD area were affected by the fluctuation in the region above 1100℃. The COP density depended on the diameter of the OSF-ring. ΔOi and BMD were affected by the fluctuation in the region near 1000Δ. As the result, when a macroscopic fluctuation in pulling rate is introduced, the quality of crystal in the region of 150 mm from the growth interface should be reviewed carefully because it can be affected by the fluctuation.

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Micro-pulling down법을 이용한 $Al_2$O$_3$/ZrO$_2$eutectic fiber의 제조 및 기계적 특성 (Growth $Al_2$O$_3$/ZrO$_2$eutectic fibers by the micro-pulling down method and its mechanical properties)

  • 이종호;;;윤대호
    • 한국결정성장학회지
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    • 제10권5호
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    • pp.345-349
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    • 2000
  • Micro-pulling down법을 이용하여 $Al_2O_3/ZrO_2$eutectic fiber를 제조하여 그 미세구조 및 기계적 특성과 성장속도의 관계를 조사하였다. 성장속도는 0.1~15 mm/min였으며, 직경 0.2~2 mm, 길이 500 mm의 eutectic fiber를 제조하였다. $Al_2O_3/ZrO_2$eutectic fiber의 미세구조는 성장속도에 따라 rod-shape structure에서 lameller structure를 거쳐 lamellar pattern을 갖는 cellular structure로 변화하였다. lamellar thickness는 성장속도가 1 mm/min에서 15 mm/min로 증가함에 따라 380 nm에서 110 nm로 감소하였다. 이와 같은 성장속도에 따른 lamellar thickness의 감소경향은 inverse-square-root로 나타내면, = 1 -l/2와 같이 표현할 수 있다. 여기서 는 m, 는 m/s의 단위를 갖는다. 13.1 Gpa의 hardness, 900 Mpa의 상온인장강도를 나타냈으며, 성장속도의 증가 즉, interlamellar spacing이 감소함에 따라 증가하는 경향을 나타냈다.

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오일 풀링 중재에 따른 치주질환 임상 지표 비교 -일반화추정 방정식 모형의 적용 (Comparative evaluation of the effects of oil pulling on periodontal indices - Using generalized estimating equation model)

  • 김윤정;양진주;이미라;김미혜;윤금채;이가연
    • 한국치위생학회지
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    • 제20권6호
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    • pp.973-980
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    • 2020
  • Objectives: This study was to analyz the effects of comparative evaluation of the effects of oil pulling on periodontal indices. Methods: A total subjects were 38; control group (19 subjects) and experimental group (19 subjects). In the experimental group, coconut oil was provided and rinsed the mouth for about 10 minutes once a day. We evaluated possession rate of pocket depth (≥4 mm), possession rate of bleeding on exploring and possession rate of gingival recession (≥1 mm). Results: The possession rate of pocket depth (≥4 mm), bleeding on exploring and gingival recession (≥1 mm) significant difference in interaction between the group and measurement time. Conclusions: The findings of this study indicate that dental hygiene process and oil pulling specialists in care of periodontal diseases were effective mediation.

초크랄스키법에 의한 실리콘 단결정성장에서 회전효과가 미치는 영향에 대한 연구 (Effects of Rotation on the Czochralski Silicon Single Crystal Growth)

  • 김무근
    • 대한기계학회논문집
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    • 제19권5호
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    • pp.1308-1318
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    • 1995
  • The influence of varying rotation speed of both crystal and crucible was numerically investigated for the Czochralski silicon-crystal growth. Based on a simplified model assuming flatness of free surfrae, the Navier-Stokes Boussinesq equations were employed to identify the flow pattern, temperature distribution as well as the shape of the melt/crystal interface. The present results showed that the interface shape was relatively convex with respect to the melt at lower pulling rate and tended to be concave as the pulling rate increased. In particular, the experimentally observed gull-winged shape of the interface was qualitatively in agreement with the predicted shape. The rotation of crystal alone little affected the growth system. When the rotation speed of the crucible was increased, there occurred inversion of the interface shape from convex to concave pattern. At rapid rotation of the crucible, an interesting channel formation was predictied primarily due to the assumption of laminar flow.

Pulling rate, rotation speed 및 melt charge level 최적화에 의한 쵸크랄스키 공정 실리콘 단결정의 O2 불순물 최소화 설계 (A Czochralski Process Design for Si-single Crystal O2 Impurity Minimization with Pulling Rate, Rotation Speed and Melt Charge Level Optimization)

  • 전혜준;박주홍;블라디미르 아르테미예프;황선희;송수진;김나영;정재학
    • Korean Chemical Engineering Research
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    • 제58권3호
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    • pp.369-380
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    • 2020
  • 대부분의 단결정 실리콘 잉곳은 초크랄스키(Czochralski(Cz)) 공정으로 제조된다. 그러나 단결정 실리콘 잉곳을 제품화 및 태양 전지 기판으로 가공하였을 때 산소 불순물이 있는 경우 낮은 효율성을 나타내는 경향이 있다. 단결정 Si-잉곳의 생산을 위해서는 용융 Si를 녹인 다음 단결정 Si의 시드(Seed)로 결정화하는 초크랄스키(Cz) 공정을 도입한다. 용융된 다결정 Si-덩어리를 단결정 Si-잉곳으로 결정성장 될 때, 열 전달은 Cz-공정의 구조에서 중요한 역할을 한다. 본 연구에서 고품질 단결정 실리콘 잉곳을 얻기 위해 Cz-공정의 최적화된 설계를 구성하였다. 결정 성장 시뮬레이션로부터 결정성장을 위한 Pulling rate 및 Rotation speed에 최적의 변수값을 형성하기 위해 사용되었으며, 변형된 Cz-공정에 대한 연구 및 해당 결과가 논의되며 결정 성장 시뮬레이션을 사용하여 Cz-공정의 Pulling rate, Rotation speed 및 Melt charge level의 최적화된 설계로 인한 결정성장시 단결정 실리콘으로 유입되는 산소 농도 최소화를 설계하였다.

$LiNbO_3$단결정성장 및 특성 연구 (Growth And Characterization of $LiNbO_3$ Single Crystals)

  • 손진영;노광수;이진형
    • 한국결정성장학회지
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    • 제2권1호
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    • pp.43-50
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    • 1992
  • 인상속도를 변수로 Czochralski법을 이용하여 $ LiNbO_3$결정들을 성장시켰다. 성장된 단결정에 균열, 기포, 셀 구조 등의 결함들이 관찰되었다. 균열들은 인상속도와 냉각속도에 매우 민감하였는데 6~7mm/h의 인상속도와 20^{circ}C/h의 냉각속도가 직경 15mm정도의 결정성장에 적당한 조건임을 알 수 있었다. 소자응용에 필요한 유전적 성질 및 광학적 성질 등을 알아보기 위하여 a축, c축방향에 따라 절삭된 시편을 온도를 변화시켜가며 측정하였다.

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치은염 환자에게 적용한 오일풀링과 전문가 칫솔질법의 효과 (Effects of coconut oil pulling and professional toothbrushing on gingivitis)

  • 이미라;문상은;김윤정;김선영;조혜은;강현주
    • 한국치위생학회지
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    • 제19권3호
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    • pp.375-385
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    • 2019
  • Objectives: The purpose of this study was to provide basic data for gingivitis management programs by dental hygienists by evaluating the effect of oral health education, oil pulling, and professional toothbrushing on gingivitis. Methods: A total of 38 subjects were divided into three groups: control group (12 subjects), experimental group 1 (13 subjects), and experimental group 2 (13 subjects). The control and experimental groups were instructed to brush using the rotating method. Distilled water was provided to the control group after training. Coconut oil was provided every morning for about 10 minutes. In the experimental group 2, a professional brushing method was used at each visit. Results: There were no significant differences in oral health among the three groups, and there was homology between patient hygiene performance (PHP) index (p=0.144) and bleeding rate (p=0.213). The PHP index showed a significant interaction between the group and measurement time. The control and experimental groups showed changes in the PHP index with time (F=3.711; p=0.013). The bleeding rate showed a significant interaction between the group and measurement period. The control and experimental groups showed changes in the bleeding rate with time (F=6.707; p<0.001). Conclusions: Oral health education, professional toothbrushing, and oil pulling specialists in oral care of gingivitis were effective in managing gingivitis. It is necessary to educate people on self-management methods for oral health promotion using gingivitis management programs by dental hygienists.