• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1999.05a
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• pp.548-551
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• 1999

The cure characteristics of metal particle filled DGEBA/MDA/SN/ zeolite epoxy resin composite system for EMI shielding were investigated by dynamic DSC run method and FT-lR spectroscopy. As the heating rate increased, the peak temperature on dynamic DSC curve increased because of the rapid cure reaction. From the straight line of the Kissinger plot, the curing reaction activation energy and pre-exponential factor could be obtained. As the post-curing time at 15$0^{\circ}C$ increased, the glass increased the glass transition temperature or the thermal stability increased. When the post curing time is too long, the system filled with metallic Al particle can be thermally oxidized by the catalytic reaction of metal filler and the thermal stability of the composite for the EMI shielding application may be decreased.

• Elastomers and Composites
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• v.55 no.1
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• pp.13-19
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• 2020

4,4'-Methylenebis(2-chlorobenzenamine) (MOCA)-free fast curing polyurethanes were prepared. In this study, the processibility of a fast curing polyurethane system was characterized by assessing the pot life. The obtained pot life of the polyurethane was 6-8 s, indicating that this prepolymer-curative system is appropriate for ribbon flow casting. The influence of the NCO index on the viscosity and mechanical properties was evaluated. The viscosity, tensile strength, tear strength, and hardness of the as-prepared polyurethanes showed an increasing trend, with an increase in the NCO index, whereas the elongation at break increased initially and then decreased with an increase in the NCO index. The gel fraction and crosslink density showed a direct correlation with the NCO index, which substantiated the improved mechanical properties at the higher NCO index. The coefficients of friction and abrasion deteriorated with an increase in the NCO index.

• Journal of Korean Tunnelling and Underground Space Association
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• v.10 no.1
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• pp.17-24
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• 2008

Many problems exist in the current cast in place concrete lining used in domestic tunnel construction. Especially, the crack of tunnel lining brings about a social and economic problem. It has a lot of influence on stability of structure and the fine finish of lining. So enormous repair-work and reinforcement of tunnel lining could occur an running out of government's budget. In our country, there are domestic production enterprises which produce a special pre-cast concrete product, but the technical level of them is still far behind compared to developed countries. Also, optimum steam coring method is important for the production of high quality product. But there is no regulation of steam curing method in our country. This study is to investigate the properties of PC panel according to the variation of steam curing conditions such as presteaming time and rate of temperature rise. The result shows that the optimum presteaming time of steam curing method in PC panel is more than 1 hour and the desirable rate of temperature in curing chamber is about $20^{\circ}C/hr$.

• Composites Research
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• v.13 no.4
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• pp.42-53
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• 2000

A study has been made to establish an optimum condition in the surface treatment and curing method that is important for the fabrication of Al 7075/CFRP laminates. PAA(Phosphoric Acid Anodizing) provided a good adhesive strength and FPL(Sulfuric / Sodium Dichromate Acid Etching) had a similar adhesive strength with PAA. On the other hand, the poor adhesive strength was shown on vapor degrease and CAA(Chromic Acid Anodizing). By using the atomic force microscope(AFM), it was found that the PAA oxide surface obviously had a greater degree of microroughness as compared to vapor degrease, CAA and FPL treated surfaces. These results support the concept of a mechanical interlocking of the adhesive with-in the oxide pores as the predominant adhesion mechanism. In curing methods, the adhesive strength of co-curing method was higher than that of secondary curing method. With respect to stability of specimen shape, the secondary curing method was better than co-curing method. DMA(Dynamic Mechanical Analysis) test revealed $T_g$ in curing times over 60 min is nearly same, so it is estimated they will have similar degree of curing and joint durability in using FM300M adhesive film.

• The Research Journal of the Costume Culture
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• v.12 no.1
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• pp.1-11
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• 2004

This study was carried out on the process of natural dye substances which can flock ultraviolet rays without producing harmful substances by pollution, germs, etc. While making human body safe in contact, extracting Gardenia, Sappan wood, Radix scutellariae, Cromwell, Mugwort, Gallnut, Lac. Those are used for curing diseases, dyeing silk cloth with those extracts, and examining the color fastness, Ultraviolet protection. From this study, the following conclusion was produced. Brightness was lower in pre-mordanting than in post. And color difference showed that Radix scutellariae was the highest. Aluminum-mordanting showed a higher color difference than Fe. Colorfastness to washing was high in all samples, and the degree of color-changing by washing was the highest in the sample dyed by gardenia, pre-mordanted gallnut showed the highest degree. Colorfastness to perspiration was the highest in gardenia. UV-A test showed that all samples a high rate of 85% or higher compared with test white cloth. Especially, post-mordanted radix scutellariae, pre-mordanted gallnut and post-mordanted sappanwood showed a superior blocking rate.

• The Journal of Engineering Geology
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• v.12 no.1
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• pp.63-73
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• 2002

To evaluate reinforced region of dike by cement grouting, we investigated both the electrical resistivity and the strength of cement grout having various water-cement ratio with curing time. These investigation results showed that the electric conductivity of grout is much higher than that of water and that the apparent resistivity of grouted region is much lower than that of unoccupied region by grout. It was founded that electrical resistivity survey might be quite effective to detect grout region in dike. As the results of electrical resistivity sounding at three dikes, apparent resistivities after grouting showed several tens to several hundreds of ohm-m which were lower than those of pre-grouting and showed stabilizing trend with curing time. From these results, we could estimate that this behavior of apparent resistivity is due to increasing strength with curing time.

• Journal of Adhesion and Interface
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• v.21 no.2
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• pp.65-70
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• 2020

Epoxy adhesive was mainly used to combine different composite materials. Epoxy adhesive was a typical thermosetting resin that can be bonded by changing from a linear structure to a three-dimensional network structure by curing reaction of epoxy and hardener. The curing conditions of epoxy adhesive were different with different types of hardener such as mixing ratio, curing time, and temperature. These curing conditions affected to the adhesive property of epoxy adhesive. In industry, it was difficult to proceed the applying epoxy adhesive and combining two parts immediately. The adhesive property decreased by humidity and pre-curing of epoxy adhesive in waiting time between two processes. In this paper, the glass fiber reinforced composite (GFRC) was combined with epoxy adhesive and adhesion property between epoxy adhesive and GFRCs was evaluated using single lap shear test. The different waiting times and humidity conditions were applied to epoxy adhesive in room temperature and adhesive property decreased as the waiting time increased. In small amount of humidity, the adhesive property increased because a small amount of moisture in the surroundings accelerated the curing reaction. In certain amount of humidity, however, the adhesion property decreased.

• Proceedings of the Korea Concrete Institute Conference
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• 2002.10a
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• pp.33-38
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• 2002

Concrete placed under cold weather has some defects such as the decrease of initial strength by hydration delay, strength unrecovery at unhardened concrete freezing, and structural failure and crack by expansion pressure. So, in this study, we tried to evaluate the JIS mortar which was made under cold weather using de-icing agency. In mortar test, the do-icing agency increased compressive strength under standard curing, and the de-icing agency made by NaNO$_2$ gave the highest strength. However, as pre-curing time under 21$^{\circ}C$ was short, the de-icing agency made by NaNO$_2$ and Ca[NO$_3$]$_2$ had the highest strength.

• Proceedings of the Korea Concrete Institute Conference
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• 1998.04a
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• pp.89-93
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• 1998

In order to enlarge effection use as well as to use as a cheafut raw material for high-strength concrete admixture, we manufactured high strength admixture by using various industrial by-products and then applied to 2nd concrete pro when concrete was added MSS, strength of concrete was promoted and had a excellent property than domestic D admixture. This result could be explained that adding of MSS accelerated the famat of ettringite($C_3A$, $3CaSO_4$, $32H_2O$) like needle crystal in steam curing a also promoted to cement solidification and shorten high pre-strength display. As a result of, strength of concrete added MSS pretented, above 850kgf/$\textrm{cm}^2$ in 7 days of long-period curing.

• Proceedings of the Safety Management and Science Conference
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• 2012.04a
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• pp.117-137
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• 2012

In the ALC(Autoclaved lightweight concrete) manufacturing process, if the pre-cured semi-cake is removed after proper time is passed, it will be hard to retain the moisture and be easily cracked. Therefore, in this research, we took the research by multiple regression analysis to find relationship between variables for the prediction the hardness that is the control standard of the removal time. We study the relationship between Independent variables such as the V/T(Vibration Time), V/T movement, expansion height, curing time, placing temperature, Rising and C/S ratio and the Dependent variables, the hardness by multiple regression analysis. In this study, first, we calculated regression equation by the regression analysis, then we tried phased regression analysis, best subset regression analysis and residual analysis. At last, we could verify curing time, placing temperature, Rising and C/S ratio influence to the hardness by the estimated regression equation.