• Journal of Korea Foundry Society
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• v.31 no.1
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• pp.26-30
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• 2011

For the fabrication of bulk near-net-shape Ti-Ni-Cu shape memory alloys, consolidation of Ti-Ni-Cu alloy powders are useful because of their brittle property. In the present study, $Ti_{50}Ni_{30}Cu_{20}$ shape memory alloy powders were prepared by gas atomization and martensitic transformation temperatures and microstructures of those powders were investigated as a function of powder size. The size distribution of the powders was measured by conventional sieving, and sieved powders with the specific size range of 25 to $150\;{\mu}m$ were chosen for this examination. XRD analysis showed that the B2-B19 martensitic transformation occurred in the powders. In DSC curves of the as-atomized $Ti_{50}Ni_{30}Cu_{20}$ powders as a function of powder size, only one clear peak was found on each cooling and heating curve. The martensitic transformation start temperature($M_s$) of the $25-50\;{\mu}m$ powders was $31.5^{\circ}C$. The $M_s$ increased with increasing powder size and the difference of $M_s$ between $25-50\;{\mu}m$ powders and $100-150\;{\mu}m$ powders is only $1^{\circ}C$. The typical microstructure of the rapidly solidified powders showed cellular morphology and very small pores were observed in intercellular regions.

• Transactions of Materials Processing
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• v.31 no.3
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• pp.124-128
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• 2022

NdFeB magnets have been positioned as the core materials in advanced technologies such as MRI (magnetic resonance imaging), FA (factory automation system), robot, motors, and so on based on the highest magnetic properties. To effectively improve the refined microstructure, the plastic deformation has been known as the good alternatives by the recrystallization. However, it has been regarded as being impossible because of the few slip systems in the RE-Fe-B magnets at room temperature. The purpose of this study was to investigate the possibility of control of grain refinement and magnetic anisotropy of NdFeB alloy powder by the severe plastic deformation. The NdFeB magnet powder was fabricated by gas atomization process, and the powder was pre-compacted at high temperature. The pre-compacted billets were deformed by HPT (high pressure torsion), and then the deformed billets were observed microstructure and magnetic properties. After the HPT process at room temperature, the grain size decreased with increasing because of the melted Nd-rich phase, and the anisotropy of Nd₂Fe₁₄B phase was formed after the HPT process.

• Journal of Powder Materials
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• v.15 no.4
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• pp.285-291
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• 2008

Fe based ($Fe_{68.2}C_{5.9}Si_{3.5}B_{6.7}P_{9.6}Cr_{2.1}Mo_{2.0}Al_{2.0}$) amorphous powder were produced by a gas atomization process, and then ductile Cu powder fabricated by the electric explosion of wire(EEW) were mixed in the liquid (methanol) consecutively. The Fe-based amorphous - nanometallic Cu composite powders were compacted by a spark plasma sintering (SPS) processes. The nano-sized Cu powders of ${\sim}\;nm$200 produced by EEW in the methanol were mixed and well coated with the atomized Fe amorphous powders through the simple drying process on the hot plate. The relative density of the compacts obtained by the SPS showed over 98% and its hardness was also found to reach over 1100 Hv.

• Journal of ILASS-Korea
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• v.2 no.2
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• pp.35-42
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• 1997

An innovating technique of atomizer has been proposed to supply and to atomise molten materials. Both of a simple geometry of nozzle and an improved nozzle have been fabricated in the present study. With these nozzles, characteristics of the suction and disintegration have been empirically investigated. The important conclusions are as follows; In the case of a simple nozzle: 1) Although the sucking up and supplying of molten materials are available, the applications of powder metallurgy are limited. 2) It is concluded that the more air flow rate, $W_A$ or the shorter the height of air nozzle from the surface of supplied water, $L_h$, the more the atomizing mass of liquids, $W_L$. In the case of an improved nozzle: 3) The stable liquids can be supplied due to cut off the passage of surrounding air entrainment by air jets. 4) The atomizing mass of liquids, $W_L$ has affected not so much on the height of nozzle from the surface of supplied water, $L_h$ as that from the orifice, hc.

• Journal of Powder Materials
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• v.13 no.6 s.59
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• pp.421-426
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• 2006

The microstructural and mechanical properties of Al-Si alloyed powder, prepared by gas atomization fallowed by hot extrusion, were studied by optical and scanning electron microscopies, hardness and wear testing. The gas atomized Al-Si alloy powder exhibited uniformly dispersed Si particles with particle size ranging from 5 to $8{\mu}m$. The hot extruded Al-Si alloy shows the average Si particle size of less than $1{\mu}m$. After heat-treatment, the average particle size was increased from 2 to $5{\mu}m$. Also, mechanical properties of extruded Al-Si alloy powder were analyzed before and after heat-treatment. As expected from the microstructural analysis, the heat-treated samples resulted in a decrease in the hardness and wear resistance due to Si particle growth. The friction coefficient of heat-treated Al-Si alloyed powder showed higher value tough all sliding speed. This behavior would be due to abrasive wear mechanism. As sliding speed increases, friction coefficient and depth and width of wear track increase. No significant changes occurred in the wear track shape with increased sliding speed.

• Journal of Powder Materials
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• v.6 no.2
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• pp.171-177
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• 1999

Ti-45.2at.%Ni-5at.%Cu and Ti-40.2at.%Ni-10atat.%Cu alloy powders were fabricated by gas atomization process. The microstructures, Shape, hardness and phase transformation behaviors of the powders were investigated by means of optical microscopy, scanning electron microscopy, micro-hardness measurement, x-ray diffraction analyses and differential scanning calorimetry. The hardness of the Ti-Ni-XCu alloy powders decreased as Cu-content increased. The x-ray diffraction analyses were carried out for powders without heat treatment, and those that treated at 85$0^{\circ}C$ for an hour in a vaccum state($10^5$ torr) and then quenched into ice water. The intensity of B$19^t$ phase increased with heat treating. The monoclinic B$19^t$ martensite was formed in the Ti-Ni-XCu alloy powders during cooling.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.771-772
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• 2006

Mechanical properties of metal injection molded titanium and titanium alloy parts were investigated in this study. Material powders with low oxygen content and spherical shape were obtained by electrode induction-melting gas atomization which could melt and atomize titanium and titanium alloy bars with no touch on crucible or tundish. Tensile specimens were fabricated from obtained powders by metal injection molding process. Tensile strength of the specimens increases with increasing oxygen content. This result corresponds to a tendency of wrought metal.

• Journal of Biosystems Engineering
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• v.28 no.4
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• pp.351-360
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• 2003

This study was carried out to settle the plugging problem which occurs frequently when agricultural wettable powder is used in pest control work using the crushing and the dispersing effects caused by irradiation of ultrasonic wave. Sonication was applied to the wettable powder suspension in a beaker for 30 seconds using a 28 kHz, 200 W PZT BLT, and the image of suspension before and after sonication was observed using a microscope and a SEM. The image of tow commercial wettable powder suspensions in water observed using an optics microscope showed that the agglomerated particles were irregularly distributed over the whole observed region when stirred mechanically, while showing more uniform distribution composed of comparatively single particles in the whole observed region after sonication. Concerning the above, the projected areas of particles in the four suspensions after sonication were decreased distinctively in the observed range of the microscope and the atomization of crystals was much developed. Over the measured range of 5.6∼4,157 ${\mu}$m particle size, the overall projected area of particles was decreased to 58.3∼89.6% on the average after sonication. When the SEM images of sonicated wettable powder suspensions dissolved in water and CH$_3$OH were compared to the suspensions before sonication, such phenomena as the atomization of particles, the expansion of voids between particles, the reduction and the decrease of agglomerated particle groups, and the progress of crack developments on the surface of flake-shaped particles were observed. It seemed possible that the plugging problem that occurs frequently in pest control machine when using wettable powder would be settled by the use of sonication.

• Proceedings of the Materials Research Society of Korea Conference
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• 1999.11a
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• pp.106-106
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• 1999

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.769-770
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• 2006

The MIM industry is currently focusing on parts that are used in automobiles and medical instruments. Many of the parts in these categories are very small and often not easy to machine because of its complex geometry. Therefore MIM is well suited for the production of these parts. We tested the sinterability of SUS316L ultra fine powders (3,4, 6, 8micron) produced by ATMIX high-pressure water-atomization, and it showed excellent results. A density of 97% theoretical was obtained by sintering at 1373K when using the ultra fine powder (3micron). Specifically, the finer the powder size, higher was the sintered density. The surface roughness and accuracy are also greatly improved with ATMIX ultra fine powder.