• 한국세라믹학회지
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• 제25권2호
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• pp.184-190
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• 1988

ZrN powder was prepared from the powder mixture of ZrCl4 and Al by the halogenide process in nitrogen gas flow (100-150ml/min) at the temperatures from 200$^{\circ}$to 1050$^{\circ}C$. ZrN powder was formed about 600$^{\circ}C$ and in the slow nitriding reaction, however, an intermediate product of Al3Zr was formed. The fine powder (0.1-10$\mu\textrm{m}$) of single phase ZrN was obtained at 1050$^{\circ}C$ after 1 hour. The lattice parameter and crystallite size of ZrN were 4.5787A and 360A, respectively. According to SEM observation, the particles were apt to agglomerates. The apparent activation energy for the formation of ZrN was approximately 13.2kcal/mole(750$^{\circ}$-1000$^{\circ}C$).

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2009년도 추계 학술논문 발표대회
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• pp.121-125
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• 2009

The recycling of waste concrete is increasing for the environment protection and the shortage of aggregate according to the large scale construction project in Korea. The more manufacturing high quality recycled aggregate is produced, the more waste concrete powder generated from the manufacture process of recycled aggregate, and the consideration about the recycling of waste concrete powder is need. Waste concrete powder was used for the partial replacement of silica powder, which is a main raw material for the manufacture of autoclave foamed concrete. According to the results of research, the slurry density, flow, compressive strength mainly depend on the replacement ratio of particle size and waste concrete powder. At the SEM analysis, the more high-waste concrete powder was the less there are generated tobermorite. But we conclude that it is possible to replace WCP as silica source in the manufacture of the lightweight foamed concrete.

• 한국건축시공학회지
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• 제17권1호
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• pp.111-117
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• 2017

Stone powder sludge is a byproduct of the crushed aggregate industry, and most of it is dumped with soil in landfills. The disposal of stone powder sludge presents a major environmental problem. This paper investigates the effects of stone powder sludge on the fluidity, density, strength and micro-structure properties of AAC(autoclaved aerated concrete) samples. Stone powder sludge was obtained from a crushed aggregate factory in order to investigate its applicability as a substitute for quartz sand in AAC. To determine the properties of the AAC samples produced with stone powder sludge, specimens containing different foam ratios were produced. Flow value, density, compressive strength, tensile strength and flexural strength of the samples were tested, and X-ray diffraction (XRD) was performed. The test results indicated that the compressive strength of AAC specimens (F120) with stone powder sludge was higher than that of AAC specimens (Q120) with quartz sand for same foam ratio of 120%. For all XRD diagrams, a higher number of tobermorite peaks was shown for the F120 sample than for the Q120 sample, which may explain the slightly higher strength gain in the F120 sample.

• 한국정밀공학회지
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• 제21권6호
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• pp.28-34
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• 2004

The old technique of sandblasting which has been used for decoration of glass surface has recently been developed into a powder blasting technique for brittle materials such as glass, silicon and ceramics, capable of producing micro structures larger than 100${\mu}{\textrm}{m}$. In this study, we introduced oblique powder blasting, and investigated the effect of the impacting angle of particles, the scanning times and the stand-off distance on the surface roughness and the weight-loss rate of samples with no mask, and the wall profile and overetching of samples with different mask pattern in powder blasting of soda-lime glass. The varying parameters were the different impact angles between 50$^{\circ}$ and 90$^{\circ}$, scanning times of nozzle up to 40 and the stand-off distances 70mm and 100mm. The widths of mask pattern were 0.2mm, 0.5mm and 1mm. The powder was alumina sharp particles, WA #600. The mass flow rate of powder during the erosion test was fixed constant at 175g/min and the blasting pressure of powder at 0.2Mpa.

• 한국건축시공학회지
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• 제18권6호
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• pp.551-558
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• 2018

본 연구에서는 페로니켈슬래그 미분말의 시멘트 대체재로서의 가능성을 평가하기 위하여 페로니켈슬래그 미분말 사용 모르타르의 압축강도 및 건조수축특성을 비교 분석하였다. 연구결과 페로니켈슬래그 미분말을 사용한 배합의 경우 동일한 양의 고로슬래그 미분말 및 플라이애시를 사용한 배합에 비해 미소수화열량이 낮게 나타났으며 모르타르 플로우는 상대적으로 다소 높은 것으로 나타났다. 또한 페로니켈슬래그 미분말을 사용한 모르타르의 압축강도의 경우 초기 강도발현은 고로슬래그 미분말 및 플라이애시와 유사하게 나타났으나 재령 28일에서는 상대적으로 낮은 압축강도를 발현하였다. 건조수축의 경우 페로니켈슬래그 미분말을 사용한 배합에서 고로슬래그 미분말을 사용한 배합에 비해 낮은 건조수축값을 나타내었으며 플라이애시를 혼입한 배합의 건조수축과 유사하게 나타났다.

• 한국건축시공학회지
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• 제4권4호
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• pp.87-94
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• 2004

As the bentonite is main material to prevent from collapse of drilling hole at underground excavation works, it is increased using quantity on construction industry day by day. But, the discarded bentonite that is over using at underground excavation works is caused various enviromental trouble as soil and water pollution est. Therefore, this study aims to propose a foundamental report for pozzolan reaction of discarded Bentonite powder by heat-treatment and cooling as concrete mineral admixture. To find out pozzolan reaction ability of discarded Bentonite powder by indirect cooling & cooling using of water after heat-treatment, the experiments are excuted flow test & compressive strength on age of mortar using discarded Bentonite powder. As a result of this study, discarded Bentonite powder can be utilized as concrete mineral admixture by heat-treatment and especially, pozzolan reaction ability of discarded Bentonite powder is superior to the situation of 600℃. 60min ＆amp; cooling using of water.

• 한국재료학회지
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• 제14권10호
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• pp.719-724
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• 2004

Production of fine tantalum powder by calciothermic reduction of tantalum oxides ($Ta_{2}O_5$) pellet through an electronically mediated reaction (EMR) has been investigated. $Ta_{2}O_5$ pellet feed and reductant calcium-nickel (Ca-Ni) alloy were charged into electronically isolated locations in a molten $CaCl_2$ bath. The current flow through an external path between the feed (cathode) and reductant (anode) locations was monitored. The current approximately 4.7A was measured during the reaction in the external circuit connecting cathode and anode location. Tantalum powder with approximately 99 $mass\%$ purity was readily obtained after each experiment. Tantalum powder by EMR using $Ta_{2}O_5$ pellet feed was fine compared with that of metal powder by metallothermic reduction and EMR using $Ta_{2}O_5$ powder feed.

• 한국안전학회지
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• 제28권3호
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• pp.63-68
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• 2013

This paper is aimed to make an analysis on characteristics of the parallel arc waveform and RMS of current at the electrical tracking state by conductive powder. In order to achieve the goal in this paper, field state investigation at metal processing companies in Chung-Nam province area was conducted. With the field state investigation, conductive powder were collected from metal processing companies. By experiment on electrical connector(breaker, connector) over which the conductive powder were scattered, arc waveform and RMS of current were measured. The measured waveform and RMS(root-mean-square) of current were analyzed to describe characteristics and patterns of electrical arc by the conductive powder. It was proved that conductive powder on electrical connector can flow electrical current enough to make electrical fire with high thermal energy. Also the change of sine waveform and RMS of current can be used to find out relationship between electrical fire and fault signal by conductive powder. The results obtained in this paper will be very helpful for the prevention of electrical fires occurred at the metal processing companies.

• 한국분말재료학회지
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• 제30권1호
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• pp.41-46
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• 2023

In this study, an Al₈₂Ni₇Co₃Y₈ (at%) bulk metallic glass is fabricated using gas-atomized Al₈₂Ni₇Co₃Y₈ metallic glass powder and subsequent spark plasma sintering (SPS). The effect of powder size on the consolidation of bulk metallic glass is considered by dividing it into 5 ㎛ or less and 20-45 ㎛. The sintered Al₈₂Ni₇Co₃Y₈ bulk metallic glasses exhibit crystallization behavior and crystallization enthalpy similar to those of the Al₈₂Ni₇Co₃Y₈ powder with 5 ㎛ or less and it is confirmed that no crystallization occurred during the sintering process. From these results, we conclude that the Z-position-controlled spark plasma sintering process, using superplastic deformation by viscous flow in the supercooled liquid-phase region of amorphous powder, is an effective process for manufacturing bulk metallic glass.

• 한국진공학회지
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• 제6권S1호
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• pp.160-165
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• 1997

Yttria stabilized zirconia coating is an attractive material for several engineering applications. In order to produce coatings with consistent and reliable performance it is important to understand the influence of spraying parameters on the coating properties and optimize the spraying parameters. In this paper the low pressure plasma spray(LPPS) deposition of as-received zirconia powder has been investigated using simple one-factor-at-a-time approach. The deposition efficiency was chosen to evaluate the melting characteristics of the as-received zirconia powder. The results obtained indicated that the deposition efficiency of zirconia powder is very sensitive to the spraying parameters such as plasma gas flow rate and ranges from 24% to 57% The microstructure and the phase composition of zirconia coating deposited with the different plasma spraying parameters were also examined by SEM and XRD respectively. The relationship between deposition efficiency and the microstructure of zirconia coating was discussed.