• Proceedings of the KOSOMBE Conference
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• v.1997 no.05
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• pp.43-46
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• 1997

The interfacial bond strength and microstructural analysis of pre-heat treated porcelain-fused-metal (PFM) were investigated using a mechanical three-point bending tester and scanning electron microscope(SEM). Four kinds of heat treated samples were prepared as follows; A: heating $1200^{\circ}F\rightarrow1600^{\circ}F$, holding 1min, reheating $\rightarrow1850^{\circ}F$, hold 3min under vacuum, B: heating $1200^{\circ}F\rightarrow1600^{\circ}F$ holding 1min, reheating $\rightarrow1850^{\circ}F$ under vacuum condition, C: heating $1200^{\circ}F\rightarrow1600^{\circ}F$, holding 1min, reheating $\rightarrow1850^{\circ}F$, holding 3min in the air, repeat same heat treatment process under vacuum condition, D: heating $1200^{\circ}F\rightarrow1600^{\circ}F$, holding 1min, reheating $\rightarrow1850^{\circ}F$, holding 1min in the air. The three-point bending test results shows that the interfacial bond strength of specimen B and C were higher than that of A and B. The SEM study reveals that Specimen C shows the highest surface density.

• Journal of Technologic Dentistry
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• v.29 no.1
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• pp.35-48
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• 2007

The purpose of this study was to evaluate shade selection using conventional visual assessment in vivo natural teeth and porcelain-fused-to-metal (PFM) crown. Maxillary central incisors, lateral incisors and canines of one hundred twenty four college women were used as vivo natural teeth. Fifty one PFM crown for maxillary central incisor fabricated by dental laboratory were used as experimental materials. Using Vitapan Classical Shade Guides, shade selection of natural teeth was measured by each college woman and shade selection of PFM crown was measured by three ceramists with more than ten years career. Both natural teeth and PFM crown shade selection were measured through Shade Eye-Ex. From the shade selection comparing, following results were obtained. The results were as follows: 1. The shade matching identification of natural teeth between the shade selection using Vitapan Classical Shade Guides and the shade selection using Shade Eye-Ex was 27.4% in maxillary central incisor, 13.7% in lateral incisor and 18.5% in canine. 2. Among the shade selection of PFM crown by three ceramists, the shade evaluation of three ceramists were same only in ten cases. In twenty case, those of two ceramists were same. 3. The shade matching identification of PFM crown between the shade selection using Vitapan Classical Shade Guides and the shade selection using Shade Eye-Ex was 38.6% in average. These results suggest that the shade selection using conventional visual assessment should be dealt with care in clinic and need a credible method for shade matching color.

• Journal of Biosystems Engineering
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• v.26 no.1
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• pp.47-56
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• 2001

In order to prevent the possibility of mixing of metal powder during food grinding processing with the metal roll mill this study was conducted to develope the materials of ceramics roll as a substitute of gray cast iron mill. Since the ceramics is brittle material and can be broken easily by a crack, it was needed to develope engineering ceramics roll materials with high elastic modulus and fracture toughness. Adding 0∼50 wt% Al$_2$O$_3$as densification additives to porcelain body material and forming the ceramics an different condition, mechanical properties were evaluated. The material structure’s densification process was analyzed by SEM and XRD. The evaluation of the mechanical properties of ceramics roll materials were compared and analyzed by non-destructive test using Young’s modulus and destructive test using 3-point bending strength and fracture toughness. The results showed several correlative results. Porcelain body material with 40 wt% Al$_2$O$_3$content heated at 1,200$\^{C}$ for 5h was high bulk density of 2.77, Young’s modulus of 118.4Gpa, 3-point bending strength of 137 MPa and fracture toughness of 2.88 MPa$.$m$\^$$\sfrac{1}{2}$/ . After analyzing the relationship between non-destructive test and destructive test, the coefficient of determination was more than 0.9. Therefore, the evaluation of non-destructive test by ultrasonic was turned out to be feasible in evaluating the mechanical properties of ceramics.

• Journal of Technologic Dentistry
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• v.6 no.1
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• pp.19-26
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• 1984

This Experimental study was performed to study the effect of the heat soaking and the diameter of pattern on the casting ability of three nonprecious alloys manufactured for porcelain-metal restorations, with respect to their ability to reproduce test pieces by casting over a selected range of uniform diameters. Samples of total 60 were constructed and divided into 6 groups according to the two variables, the diameter and the heat soaking. The completed cast samples were examined visually and measured with a caliper calibrated to 0.05mm. The results obtained were as follows: 1. Length cast was significantly related to the diameter to be cast, especially in the case of the marrowest diameter of 230m. 2. Length cast not significantly related to the heat soaking. 3. The completeness of casting was significantly related to the diameter to be cast, particularly in the case of the narrowest diameter of 230m. 4. The completeness of casting was not significantly related to the heat soaking. 5. All of the three nonprecious alloys used for this experiment were significantly different from an ideal alloy in the completeness of casting.

• The Journal of Korean Academy of Prosthodontics
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• v.52 no.2
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• pp.90-96
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• 2014

Purpose: The purpose of this study is to see what impact the heat and press-on-metal technique has on the marginal fit of metal ceramic crown. Materials and methods: Prior to the experiment, 4 metal master models were prepared. Each model has margin of chamfer, margin of heavy chamfer, margin of shoulder with bevel and margin of shoulder (collarless). Additionally, 10 crowns were made for each margin, total of 40 crowns. Marginal discrepancy between the master model and crown was observed at ${\times}100$ microscopic magnification in two states; in coping state and upon completion of making metal ceramic crown. Data analysis was performed using paired t-test along with one-way ANOVA and Duncan multiple comparison test. Results: After analyzing mean and standard deviation of marginal discrepancy, it was confirmed that marginal discrepancies were within the clinical permitted range for all states; in coping state and upon completion of making metal ceramic crown. For the chamfer group, a significant increase in marginal discrepancy upon completion of making metal ceramic crown was observed compared to the heavy chamfer group. Also, a marginal discrepancy of porcelain margin in shoulder group was significantly less than the marginal discrepancy of metal margin in chamfer and shoulder group. Conclusion: From the test result, one can conclude that marginal fit of metal ceramic crown built with heat and press-on-metal technique is not significantly different from marginal fit of metal ceramic crown built with traditional technique. And along with efficiency of this system, heat and press-on-metal technique is considered in clinic.

• The Journal of Korean Academy of Prosthodontics
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• v.39 no.2
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• pp.197-207
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• 2001

Development of new ceramics and esthetic needs of patients increase the use of all ceramic restorations. Fractured teeth often need metal post and core as foundation for final restoration. When all ceramic restorations are planned, metal post and core may lead to compromised esthetics because of opacity and gray color of metal post and core. Many techniques have been proposed to solve this problem such as application of an opaque porcelain to the metal core or all ceramic post and core. This study was performed to evaluate effect on color of Empress 2 crown according to various post systems. Color was evaluated by the CIE $L^*a^*b^*$ systems and measured by spectrophotometer (Model CM-3500, Minolta, Japan). Specimens were divided into 4 groups as follows Group 1 : gold cast post specimen + Empress 2 crown specimen Group 2 : application of an opaque porcelain to gold cast post specimen + Empress 2 crown specimen Group 3 : cosmopost specimen + Empress 2 crown specimen Group 4 : In-ceram post specimen + Empress 2 crown specimen. The results obtained as follows, 1. $L^*$ Values showed that group 2, 3, 4 were higher than group 1 with significant difference and group 2, 3, 4 were not significantly different. 2. $a^*$ Values and $b^*$ values also showed that group 2. 3, 4 were higher than group 1 with significant difference and group 2, 3, 4 were not significantly different. 3. ${\Delta}E^* ab$ Values showed that ${\Delta}E^* ab$ 3 was the highest value and ${\Delta}E^* ab$ 5 was the lowest value.

• The Journal of Korean Academy of Prosthodontics
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• v.35 no.1
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• pp.118-129
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• 1997

The purpose of this study was to evaluate the shock absorbing effect of 4 restorative materials and intramobile connector. The damping effect of four restorative materials used to veneer test crown rigidly connected to IMZ implant and subjected to an impact force was measured. These materials included a gold alloy(stabilor G) : a noble metal ceramic alloy(Degudent H) : porcelain(Duceram) : composite resin(Dentacolor). In addition, this study compared damping effect of same restoretive materials after using polyoxymethylene intramobile connector(POM IMC). The result of this study suggest that : In case of using metal IMC 1. Veneered composite resin(group IV) reduced the impact force by 75%, when compared to an equivalent thickness of porcelain(group III). Group IV reduced the impact force by 87% and 89%, respectively, when compared to Stabilor G(group I) and Degudent H(group II). 2. The impact force recorded was higher for the alloy with the higher elastic modulus.(Stabilor G, group I, Young's modulus 107 Gpa, versus Degudent H, Group II, Young's modulus 95 Gpa) 3. It took the longest time for composite resin veneered group(IV) to reach to peak force when compared group I, II, III. In case of using POM IMC 4. The mean impact force recorded were reduced by 79%(group I), 78%(group II), 69%(group III), 84%(group IV), respectively, when compared to using metal IMC. 5. The time required to reach the peak force were increased by 78%(group I, II) 87%(group III), 34%(group IV), respectively, when compared to using metal IMC>.

• The Journal of Advanced Prosthodontics
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• v.6 no.2
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• pp.138-145
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• 2014

Cobalt-Chromium (Co-Cr) alloys are classified as predominantly base-metal alloys and are widely known for their biomedical applications in the orthopedic and dental fields. In dentistry, Co-Cr alloys are commonly used for the fabrication of metallic frameworks of removable partial dentures and recently have been used as metallic substructures for the fabrication of porcelain-fused-to-metal restorations and implant frameworks. The increased worldwide interest in utilizing Co-Cr alloys for dental applications is related to their low cost and adequate physico-mechanical properties. Additionally, among base-metal alloys, Co-Cr alloys are used more frequently in many countries to replace Nickel-Chromium (Ni-Cr) alloys. This is mainly due to the increased concern regarding the toxic effects of Ni on the human body when alloys containing Ni are exposed to the oral cavity. This review article describes dental applications, metallurgical characterization, and physico-mechanical properties of Co-Cr alloys and also addresses their clinical and laboratory behavior in relation to those properties.

• Journal of the Korean Ceramic Society
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• v.32 no.10
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• pp.1203-1211
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• 1995

The tests of three point bending and vickers hardness have been carried out to investigate mechanical characteristics of bioceramics for artificial dental crowns. And color and color difference test has been performed to study chromaticity changes after sintering specimens composited with glass and leucite powders. In addition, thermal dilation test has been carried out to examine bonding relations between dental porcelain and metal frame (Ni-Cr alloy). The result of three point bending test showed a maximum strength of about 68 MPa. Thermal expansion coefficient changed from 8.3$\times$10-6/$^{\circ}C$ to 13.5$\times$10-6/$^{\circ}C$ with increasing leucite content (0~30wt.%) in glass matrix. Bonding between porcelain (25% leucite-75% glass) and Ni-Cr alloy was excellent.

• Journal of Technologic Dentistry
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• v.21 no.1
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• pp.115-121
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• 1999

This investing was carried out to evaluate the alteration of stress distribution on teeth and esthetic crowns. Analyzing the stress distribution by the two-dimensional finite element methods, a model of lower 1st molar according to the porcelain fused metal crown an the porcelain fused glass ceramic core crown and the all glass ceramic crown. 1. The pattern of stress distribution showed no apparent differences. 2. The greatest von Mises values were concentrated around the central fossa of all esthetic crowns. The greatest Maximum principle value were concentrated around the interface between the base of esthetic crown and the abutment tooth. It was found that the apatite glass ceramic could be applicable for use in dental crown prosthesis.