• 제목/요약/키워드: Polarizing microscope

검색결과 116건 처리시간 0.024초

편광 현미경을 이용한 Sodium Niobate 단결정의 분역 구조 관찰 (In Situ Observation of Domain Structure of $NaNbO_3$ Using Polarizing Microscope)

  • 정선태
    • 한국세라믹학회지
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    • 제34권12호
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    • pp.1235-1239
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    • 1997
  • Sodium niobate single crystals were grown by high temperature solution growth with Na2O/B2O3 flux. The phase transitions and domain structures of sodium niobate were observed using transmission polarizing microscope from room temperature to $650^{\circ}C$. There was imperfect extinction region within as-grown crystals and this area could be removed by heat treatment. The area existed within crystal till 3$65^{\circ}C$, in which temperature the space group of sodium niobate is changed from Pbma to Pmnm. The phase transition from Pbma to Pmnm happened abruptly with changing domain structure. At 48$0^{\circ}C$, 52$0^{\circ}C$ and 572$^{\circ}C$, the colors and walls of domains were changed. All domains disappeared and the space group of sodium niobate was changed from P4/mbm to Pm3m at 64$0^{\circ}C$. When sodium niobate changed from high temperature phase to low temperature phase, the memory effect of domain structure was not observed.

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편광현미경을 이용한 전자적근관장측정기의 정확성에 관한 연구 (EVALUATION OF THE ACCURACY OF THE ELECTRONIC APEX LOCATOR USING THE POLARIZING MICROSCOPE)

  • 박한수;윤수한
    • Restorative Dentistry and Endodontics
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    • 제17권1호
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    • pp.235-243
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    • 1992
  • The purpose of this study was to evaluate the accuracy of an electronic apex locator, the Neosono - M, in determining the location of the cementodentinal junction. A total of 26 teeth with 46 canals were evaluated. The apex locator was used to locate the file and the teeth extracted. The specimen were prepared with highspeed burs and sandpaper discs to a thickness of $250{\sim}300{\mu}m$. Distances were measured from the cementodentinal junction with the use of polarizing microscope. Measurements made by the apex locator were also compared with those by the X - ray. The results were as follows. 1. The apex locator and X - ray were to measure a mean value of 0.17, 0.45mm coronal to the CDJ respectively. There was no significant difference between the accuracy of the apex locator and that of X - ray. 2. There was no significant difference between the accuracy of apex locator in vital and in nonvital teeth, and between in narrow and in wide canals. 3. The files in nonvital and narrow group were apical to the CDJ significantly than those of vital and narrow, vital and wide, and non vital and wide groups.

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아르곤 레이저 광감각법의 법랑질 우식증 조기탐지 효과에 관한 연구 (A STUDY ON THE EARLY DETECTION OF ENAMEL CARIES BY THE LUMINESCENCE EXCITED BY ARGON LASER)

  • 이난영;이창섭;이상호
    • 대한소아치과학회지
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    • 제24권1호
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    • pp.313-324
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    • 1997
  • The aim of the present study was to describe an safe and convenient method for the early detection of enamel caries using laser fluorescence. Fluorescence from natually carious lesion of human teeth illuminated by an argon laser(488nm) was observed and photographed using barrier filter. Intact enamel was found to fluorescence with a yellowish light. Whereas, incipient caries lesions in the enamel were dearly visible as dark areas in contrast to the fluorescence surroundings. For evaluation of accuracy of this method, lesion depth measured by the laser fluorescence in light microscope was compared with that polarizing microscope. The results from the present study can be summarized as follows : 1. Enamel caries of smooth surface was observed as pale white spot and undefined outline in ordinary light. Whereas, lesion was clearly visible as dark spot in laser fluorescence. 2. There was no difference between ordinary light view and laser fluorescence in occlusal surface and interproximal surface. 3. There was no significant difference between the lesion depth observed by laser fluorescence with light microscope and polarizing microscope. Apparent correlation exists between two groups.

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초기우식병소에 대한 레이저 fluorescence의 광학적 탐지감도 (OPTICAL SENSITIVITY OF LASER FLUORESCENCE FOR INCIPIENT CARIES DETECTION)

  • 김효석;김왕근;이창섭;이상호
    • 대한소아치과학회지
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    • 제26권1호
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    • pp.109-118
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    • 1999
  • The aim of this study was to evaluate the optical density of laser fluorescence for detection of incipient caries. Prepared and polished bovine enamel specimens were demineralized in a STPP solution for varying periods of time between 3 hrs. and 60 hrs. with an area of sound enamel retained on each specimen. The randomized specimens were analyzed for optical density of enamel demineralization using laser fluorescence. The specimens were sectioned and examined lesion depth by polarizing light microscope. Results were analyzed statistically with SAS program. The results from this study can be summarized as follows: 1. Optical density measured by laser fluorescence and lesion depth measured by polarizing light microscope was increased as demineralization time was increased(p<0.001). 2. Between optical density measured by laser fluorescence and lesion depth measured by polarizing light microscope was correlated highly(${\gamma}{\geq}0.74956$, p<0.001). 3. Regressive equation was obtained in this study as follows. Y=[X-0.260851]/0.000271(R-square:0.5618, p<0.001) (X:DENSITY, Y:DEPTH) In summary, optical density measured by laser fluorescence would be within the range of possibility to quantitatively presume demineralization amount of incipient caries lesion

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편광현미경을 이용한 조암광물 관찰 웹 컨텐츠 개발 (Developing Web Contents for Rock-forming Mineral Observation under Polarizing Microscope)

  • 이창진;박철모;류춘렬
    • 한국지구과학회지
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    • 제30권2호
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    • pp.176-184
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    • 2009
  • 본 연구의 목적은 조암광물의 광학적 특징에 대한 웹 컨텐츠를 개발하고 적용하는데 있다. 개발된 웹 콘텐츠는 학습 목표와 교수 학습 내용을 명료하게 보여주고 학습 내용의 접근과 항목간의 이동을 원활히 하는 시스템을 구축하는 한편 중고등 학교 교과서에서 가장 많이 인용되는 8종의 조암광물에 대한 광학적 특징을 동영상과 사진으로 제시하여 학생들의 광물에 대한 이해도를 높였다. 개발된 웹 컨텐츠를 수업에 적용한 후 MALSM를 이용한 교수-학습 자료로서의 질적 수준과 학습 효과를 분석한 결과 대부분의 학생들은 수업목표, 학습내용, 수업전략, 화면구성, 이용의 편의성, 학습자료 항목에서 긍정적인 반응을 보였다. 웹 컨텐츠를 이용한 수업을 받은 학생 중에서 약 62%의 학생들이 편광현미경으로 박편상의 조암광물을 동정할 수 있었다.

상대위상 현미경을 이용한 양파 표피세포의 상대위상 측정 (Measurement of Relative Phase Distribution of Onion Epidermal cells by using Relative Phase Microscope)

  • 신인희;김덕영
    • 한국광학회:학술대회논문집
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    • 한국광학회 2006년도 하계학술발표회 논문집
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    • pp.147-148
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    • 2006
  • Relative phase distribution of onion epidermal cells was measured by using the relative phase microscope with inverse linear polarizing method. Decrease of relative phase distribution of onion epidermal cells was also investigated as the elapse of time. In decrease of relative phase distribution, relative phase of cell membrane in onion epidermal cells decreased radically as compared with that of cytoplasm.

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전(塼)의 백화현상 규명 및 제거방안 연구 - 수원화성 백화현상을 중심으로 - (Investigation and Removal Method of Efflorescence Phenomenon of Traditional Bricks - Focusing on the Efflorescence of Hwaseong Fortress in Suwon -)

  • 정광용;차현석
    • 건축역사연구
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    • 제22권6호
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    • pp.59-66
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    • 2013
  • This study progressed an investigation on the cause of the efflorescence phenomenon of bricks in Suwon Hwaseong Fortress, which is designated as a UNESCO World Heritage by using diverse scientific analyses. The samples were taken in Hwaseong and analyzed using XRD and SEM-EDS for the material identification of efflorescence. We observed under a polarizing microscope and measured absorption factors for the basic investigation for traditional bricks. As a result of material identification, soluble salt($Na_2SO_4$, $KNO_3$) and insoluble salt($CaCO_3$) were detected. There was no big difference between original bricks and repaired bricks under the polarizing microscope. However, in terms of the water absorption rate, bricks which were used for repair nowadays showed low water absorption rate(1%). In conclusion, soluble salt and insoluble salt appeared due to an effect of an air pollution and joint mortar. Soluble salt was removed in the rainy season, but insoluble salt was not removed. As a result of the efficiency and safety tests for chemicals removing efflorescence, chemical E is likely to be the suitable chemicals for the efflorescence phenomenon of traditional bricks in Suwon Hwaseong Fortress. In the future, consideration whether the use of lime is available or not should be studied through comprehensive researches including repair work, construction work and the environment factor with lime. Also, physical, chemical identifications of repairing bricks will be required.

$BaTiO_3$의 강유전성 분역 (Ferroelectric Domans in $BaTiO_3$)

  • 박봉모;정수진
    • 한국세라믹학회지
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    • 제33권1호
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    • pp.56-64
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    • 1996
  • A large amount of papers about the cubic-to-tetragonal phase transition the ferroelectric domain structures of the BaTiO3 were already reported but there exist still some needs to observe the domain behaviors directly. In this study the domain structures of the tinned plates prepared from ta single crystal grown by the TSSG technique were observed using a polarizing microscope TE and X-ray topography. The spatial relation be-tween the orientation states of domains was investigated and the effects of external stresses and electric fields on the behaviors of ferroelectric and ferroelastic domains were studied. All the 90$^{\circ}$walls cut off in the crystal are the wedge shaped lamellar domains and all the straight boundaries in the observed domain patte군 can be interpreted as the head-to-tail 90$^{\circ}$walls. The irregular overlapped boundaries commonly observed by using a polarizing microscope and X-ray topography are complex combinations of well-known 90$^{\circ}$walls and are domain walls were predominant and were stabilized after surface polishing. In the paraelectric phase region the domain walls vanished but the residual surface strain patterns could be seen at the same positions of the stabilized 90$^{\circ}$a-a walls in the tetragonal phase region, These stabilized walls resulted from the surface strain had a memory effect in domain formation during the repeated phase transitions and could notr be affected by an external electtric field.

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광중합형 및 자가중합형 교정용 전색제의 치아우식예방 및 진행억제효과에 관한 실험적 연구 (The effects of fluoride releasing orthodontic sealants on the prevention and the progressive inhibition of enamel demiheralization in vitro)

  • 채승원;;윤영주;김광원
    • 대한치과교정학회지
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    • 제27권6호
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    • pp.979-995
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    • 1997
  • 고정성 교정장치 주변에 발생되는 백색반점은 임상적으로 쉽게 눈에 띄는 문제점을 가지고 있으므로 잔치제거 후 심니적으로 만족스럽지 못한 결과를 야기하는데, 이는 곧 교정치료의 실패를 의미한다. 이미 많은 연구를 통해 고정성 교정장치가 구강내 세균환경을 변화시켜 세균집단의 증식을 용이하게 함으로써 고정성 장치 부착 후, 법랑질 탈회의 발생빈도가 증가된다는 사실이 보고 되어 왔으며 장기간이 소요되는 교정치료의 특성으로 인해 발생되는 브라켓 또는 교정용 밴드 주변의 법랑질 탈회나 치아우식증을 예방 또는 억제시키기 위한 연구가 함께 진행되어 왔다. 이는 환자에 대한 구강위생 교육이나 치아관리 노력에도 불구하고 발생될 수 있는데 이를 예방하기 위한 방법의 하나로 불소가 유리되는 교정용 전색제를 사용할 수 있다. 본 연구는 불소가 유리되는 광중합형 및 자가중합형 교정용 전색제의 치아우식 예방 및 진행억제효과를 규명하기 위해 다음과 같이 각각 7개의 편광현미경군(A군-G군)과 주사전자현미경군(A'군-G'군)으로 분류하였고 [1. A & A'군 STPP 인공우식용액에 담그지 않은 정상치아군, 2. B & B'군 : STPP 인공우식용액에 담그고 $37^{\circ}C$의 항온용기 에 72시간 보관한 비처치군,3. C & C'군 : STPP 인공우식용액에 담그고 $37^{\circ}C$ 의 항온용기에 72시간 보관한 자가중합형 교정용 전색제군, 4. D &D'군 : STPP 인공우식용액에 담그고 $37^{\circ}C$의 항온용기에 72시간 보관한 광중합형 교정용 전색제군, 5. E & E'군 표면에 아무처리 없이 STPP 인공우식용액에 담그고 $37^{\circ}C$의 항온용기에 72시간 보관한 후, 이를 다시 아무런 처치없이 STPP 인공우식용액에 담그고 $37^{\circ}C$의 항온용기에 72시간 보관한 비처치군, 6. F & F'군 : 표면에 아무런 처치없이 STPP 인공우식용액에 담그고 $37^{\circ}C$의 항온용기에 72시간 보관한 후, 자가중합형 교정용 전색제를 도포하고 이를 다시 STPP 인공우식용액에 담그고 $37^{\circ}C$의 항온용기에 72시간 보관한 자가중합형 교정용 전색제, 7. G & G'군 :표면에 아무런 처치없이 STPP 인공우식용액에 담그고 $37^{\circ}C$ 의 항온용기에 72시간 보관한 후, 광중합형 교정용 전색제를 도포하고 이를 다시 STPP 인공우식용액에 담그고 $37^{\circ}C$ 의 항온용기에 72시간 보관한 광중합형 교정용 전색제군], 이들을 편광현미경과 주사전자현미경을 이용해 조직의 변성 여부를 검색하여 다음과 같은 결과를 얻었다. 1. 편광현미경적 연구에서 인공우식병 소의 깊이는 $A군(5.08{\mu}m),\;B군(47.82{\mu}m,\;C군(8.42{\mu}m),\;D군(7.20{\mu}m),\;E군(85.41{\mu}m),\;F군(60.38{\mu}m),\;G군(60.13{\mu}m)$,이었다. 2. 인공우식 병소의 깊이에 있어서, B군은 A군,C군,D군과 비교하여 통계학적으로 유의성 있는 차이를 보였고(p<0.05), E군은 F군,G군과 비교하여 통계학적으로 유의성 있는 차이를 보였다(p<0.05). 3. 광중합형 및 자가중합형 교정용 전색제는 법랑질탈회 예방효과가 있었다. 4. 광중합형 및 자가중합형 교정용 전색제는 법랑질탈회 진행억제효과가 있었다. 5. 광중합형 및 자가중합형 교정용 전색제 표본에 대한 주사전자현미경적 연구에서 인공우식용액의 시간 경과에 따른 영향은 없었다. 6. 광중합형 교정용 전색제 표본과 자가중합형 교정용 전색제 표본 사이의 차이는 편광현미경과 주사전자현미경으로 구별할 수 없었다.

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