• Title/Summary/Keyword: Physical characterization

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Recent Developments in Magnetic Measurements: from Technical Method to Physical Knowledge

  • Basso, V.;Fiorillo, F.;Beatrice, C.;Caprile, A.;Kuepferling, M.;Magni, A.;Sasso, C.P.
    • Journal of Magnetics
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    • v.18 no.3
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    • pp.331-338
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    • 2013
  • We present a few significant advances in methods and concepts of magnetic measurements, aimed both at providing novel routes in the characterization of hard and soft magnetic materials and at improving our basic knowledge of the magnetization process. We discuss, in particular, investigation methods and experimental arrangements that have been developed in recent times for: 1) Hysteresis loop determination in extra-hard magnets by means of Pulsed Field Magnetometry; 2) Broadband observation of domain wall dynamics by highspeed stroboscopical Kerr techniques; 3) Entropy measurements in magnetocaloric materials by calorimetry in magnetic field. While pertaining to somewhat independent fields of investigation, all these measuring techniques have in common a solid approach to the underlying physical phenomenology and have a potential for further developments.

Design of the Fuzzy-based Mobile Model for Energy Efficiency within a Wireless Sensor Network

  • Yun, Dai Yeol;Lee, Daesung
    • Journal of information and communication convergence engineering
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    • v.19 no.3
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    • pp.136-141
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    • 2021
  • Research on wireless sensor networks has focused on the monitoring and characterization of large-scale physical environments and the tracking of various environmental or physical conditions, such as temperature, pressure, and wind speed. We propose a stochastic mobility model that can be applied to a MANET (Mobile Ad-hoc NETwork). environment, and apply this mobility model to a newly proposed clustering-based routing protocol. To verify its stability and durability, we compared the proposed stochastic mobility model with a random model in terms of energy efficiency. The FND (First Node Dead) was measured and compared to verify the performance of the newly designed protocol. In this paper, we describe the proposed mobility model, quantify the changes to the mobile environment, and detail the selection of cluster heads and clusters formed using a fuzzy inference system. After the clusters are configured, the collected data are sent to a base station. Studies on clustering-based routing protocols and stochastic mobility models for MANET applications have shown that these strategies improve the energy efficiency of a network.

Nickel Doping on Cobalt Oxide Thin Film Using by Sputtering Process-a Route for Surface Modification for p-type Metal Oxide Gas Sensors

  • Kang, Jun-gu;Park, Joon-Shik;An, Byeong-Seon;Yang, Cheol-Woong;Lee, Hoo-Jeong
    • Journal of the Korean Physical Society
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    • v.73 no.12
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    • pp.1867-1872
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    • 2018
  • This study proposes a route for surface modification for p-type cobalt oxide-based gas sensors. We deposit a thin layer of Ni on the Co oxide film by sputtering process and annealed at $350^{\circ}C$ for 15 min in air, which changes a typical sputtered film surface into one interlaced with a high density of hemispherical nanoparticles. Our in-depth materials characterization using transmission electron microscopy discloses that the microstructure evolution is the result of an extensive inter-diffusion of Co and Ni, and that the nanoparticles are nickel oxide dissolving some Co. Sensor performance measurement unfolds that the surface modification results in a significant sensitivity enhancement, nearly 200% increase for toluene (at $250^{\circ}C$) and CO (at $200^{\circ}C$) gases in comparison with the undoped samples.

Synthesis and spectroscopic characterization of zinc ferrite nanoparticles

  • Arora, Shefali;Nandy, Subhajit;Latwal, Mamta;Pandey, Ganesh;Singh, Jitendra P.;Chae, Keun H.
    • Advances in nano research
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    • v.13 no.5
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    • pp.437-451
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    • 2022
  • Synthesis approaches usually affect the physical and chemical properties of ferrites. This helps ferrite materials to design them for desired applications. Some of these methods are mechanical milling, ultrasonic method, micro-emulsion, co-precipitation, thermal decomposition, hydrothermal, microwave-assisted, sol-gel, etc. These methods are extensively reviewed by taking example of ZnFe2O4. These methods also affect the microstructure and local structure of ferrite which ultimately affect the physical and chemical properties of ferrites. Various spectroscopic techniques such as Raman spectroscopy, Fourier Transform Infrared spectroscopy, Ultra Violet-Visible spectroscopy, Mossbauer spectroscopy, extended x-ray absorption fine structure, and electron paramagnetic resonance are found helpful to reveal this information. Hence, the basic principle and the usefulness of these techniques to find out appropriate information in ZnFe2O4 nanoparticles is elaborated in this review.

A Survey Study on Needs for the Construction of the CSFT (Cluster with a Strongpoint for Field Training) (CSFT-구축 수요도에 관한 조사 연구)

  • Lee, Jae-Hong;Kang, Kyu-Hun;Kwon, Won-An;Kim, Gi-Chul;Kim, Chang-Tae;Min, Dong-Gi;Lee, Jin-Hwan
    • PNF and Movement
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    • v.11 no.1
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    • pp.27-33
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    • 2013
  • Purpose : The purpose of this research was to research on Needs for the Construction of the CSFT(Cluster with a Strongpoint for Field Training) on students and professors of health-related majors. Methods : We investigated 164 students and professors using a self-reporting method with experience of Field Training. A statistical analysis was performed using SPSS 17.0 for window version. Results : It showed that educational satisfaction had scored 4.05 in curriculum, 4.00 in environment, 3.52 in schedule, 3.71 in evaluation and 3.71 in teaching and 3.84 in industrial-college systems for Field Training. Needs for the Construction of the CSFT had scored 4.17 in $mean{\pm}standard$ deviation. Conclusion : Characterization of Nursing, Department of Health and local health care environment and conditions, if you think the quality of education for the Department of Health Nursing, gradually, the acquisition and improvement of the base hospital is necessary. Therefore, it is considered to be institutionalized by installing the strongpoint hospital at least one in each region, so that they can contribute to the improvement of people's health.

Physical Characterization and Contact Lens Application of Polymer Produced with Propylene Glycol Additive (프로필렌 글리콜을 첨가제로 사용한 고분자재료의 물성 및 콘택트렌즈 응용)

  • Kim, Tae-Hun;Sung, A-Young
    • Journal of the Korean Chemical Society
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    • v.54 no.1
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    • pp.105-109
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    • 2010
  • HEMA (2-hydroxyethyl methacrylate), EGDMA (ethylene glycol dimethacrylate) and propylene glycol was copolymerized in the presence of AIBN (azobisisobutyronitrile) initiator in a mould. The physical properties of the contact lens were measured. The water content of 37.06~38.71%, refractive index of 1.492~1.432, visible transmittance of 89.4~91.5%, tensile strength of 0.1416~0.2302 kgf, and contact angle of $38.60{\sim}53.53^{\circ}$ were obtained. Therefore, the contact lens material produced using propylene glycol as an additive satisfied the basic physical properties required for contact lenses application. It is interesting to note that an increase in wettability and tensile strength while having no significant changes in water content.

Isolation and Characterization of an Extremely Thermophilic Sulfur-metabolizing Bacterium from a Deep-sea Hydrothermal Vent System

  • Kwak, Yi-Seong;Kobayashi, Tetsuo;Akiba, Teruhiko;Horikoshi, Koki;Kim, Young-Bae
    • Journal of Microbiology and Biotechnology
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    • v.4 no.1
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    • pp.36-40
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    • 1994
  • A water sample was taken from a black smoker chimney of a deep-sea hydrothermal vent by using an unmanned submersible "Dolphin 3K". The temperature of the hydrothermal fluid from the black smoker was $276^{\circ}C$. After isolation by repeated serial dilutions, An extremely thermophilic bacterial strain was selected. The strain designated as DT1331, was an anaerobic, non-motile, coccoid shaped bacterium with about 0.5 to $1.0\;\mu\textrm{m}$ in diameter. The strain DT1331 could grow up to $93^{\circ}C$, but the optimum temperature of this strain was $80^{\circ}C$. The growth occurred in the pH range of 4.5 to 8.5 and the optimum pH was 6.0. The strain DT1331 required 1% to 5% NaCl for growth and cell lysis was observed below 1% NaCl concentration. The bacterium could grow on polypeptides such as tryptone, peptone, soytone and on proteins such as casein or gelatin. However, no growth was observed on single amino acids, sugar and organic acids. Hydrogen gas was detected slightly during growth. This bacterium obligately required elemental sulfur and hydrogen sulfide gas was produced during growth.

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AN INVESTIGATION ON THE CHARACTERIZATION OF COMPOSITE RESIN POLYMERIZED BY THE USE OF AN ARGON ION LASER (Argon 이온 레이저 중합에 의한 Composite resin의 물성에 관한 연구)

  • Cho, Hyung-Kyung;Lee, Chung-Suck
    • Restorative Dentistry and Endodontics
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    • v.17 no.1
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    • pp.69-82
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    • 1992
  • An experimental investigation of the physical properties of light curing composite resin P-50 was performed, in which an argon ion laser beam was irradiated. The physical and mechanical properties of laser polymerized composite resin were determined by measuring the compressive strength, diametral tensile strength, curing depth and microhardness depending upon the experimental conditions such as the laser irradiation time(10sec, 20sec, 30sec) and laser power(300mW, 500mW, 1000mW). These observations were compared with a conventional visible light curing technique. In addition, to evaluate the marginal adaptation, Class V cavity was prepared on the buccal or lingual surface of the extracted premolar and filled with P-50 light curing resin. The test samples were irradiated with both light sources so that the interface between the restoration and the tooth structure were observed under scanning electron microscope. The most of physical and mechanical properties of the laser cured resin showed a remarkable improvement than those treated with the conventional light source, while the observations with the scanning electron microscope provided no significant difference for two polymerized sources. From the results in the experiment it appears that the potential of an argon ion laser is of important value of the use in the polymerization of composite resin.

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Photocurrent Characteristics of Zinc-Oxide Films Prepared by Using Sputtering and Spin-Coating Methods

  • Park, Sungho;Kim, Byung Jun;Kang, Seong Jun;Cho, Nam-Kwang
    • Journal of the Korean Physical Society
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    • v.73 no.9
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    • pp.1351-1355
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    • 2018
  • The photocurrent characteristics of zinc-oxide (ZnO) thin-film transistors (TFTs) prepared using radio-frequency sputtering and spin-coating methods were investigated. Various characterization methods were used to compare the physical and the chemical properties of the sputtered and the spin-coated ZnO films. X-ray photoelectron spectroscopy was used to investigate the chemical composition and state of the ZnO films. The transmittance and the optical band gap were measured by using UV-vis spectrometry. The crystal structures of the prepared ZnO films were examined by using an X-ray diffractometer, and the surfaces of the films were investigated by using scanning electron microscopy. ZnO TFTs were prepared using both sputter and solution processes, both of which showed photocurrent characteristics when illuminated by light. The sputtered ZnO TFTs had a photoresponsivity of 3.08 mA/W under illumination with 405-nm light while the solution-processed ZnO TFTs had a photoresponsivity of 5.56 mA/W. This study provides useful information for the development of optoelectronics based on ZnO.

Structural and component characterization of the B4C neutron conversion layer deposited by magnetron sputtering

  • Jingtao Zhu;Yang Liu;Jianrong Zhou;Zehua Yang;Hangyu Zhu;Xiaojuan Zhou;Jinhao Tan;Mingqi Cui;Zhijia Sun
    • Nuclear Engineering and Technology
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    • v.55 no.9
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    • pp.3121-3125
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    • 2023
  • Neutron conversion detectors that use 10B-enriched boron carbide are feasible alternatives to 3He-based detectors. We prepared boron carbide films at micron-scale thickness using direct-current magnetron sputtering. The structural characteristics of natural B4C films, including density, roughness, crystallization, and purity, were analyzed using grazing incidence X-ray reflectivity, X-ray diffraction, X-ray photoelectron spectroscopy, time-of-flight secondary ion mass spectrometry, and scanning electron microscopy. A beam profile test was conducted to verify the practicality of the 10B-enriched B4C neutron conversion layer. A clear profile indicated the high quality of the neutron conversion of the boron carbide layer.