• Title/Summary/Keyword: Physical characterization

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Characterization of Cone Index and Tillage Draft Data to Define Design Parameters for an On-the-go Soil Strength Profile Sensor

  • Chung S. O.;Sudduth Kenneth A.
    • Agricultural and Biosystems Engineering
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    • v.5 no.1
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    • pp.10-20
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    • 2004
  • Precision agriculture aims to minimize costs and environmental damage caused by agriculture and to maximize crop yield and profitability, based on information collected at within-field locations. In this process, quantification of soil physical properties, including soil strength, would be useful. To quantify and manage variability in soil strength, there is need for a strength sensor that can take measurements continuously while traveling across the field. In this paper, preliminary analyses were conducted using two datasets available with current technology, (1) cone penetrometer readings collected at different compaction levels and for different soil textures and (2) tillage draft (TD) collected from an entire field. The objective was to provide information useful for design of an on-the-go soil strength profile sensor and for interpretation of sensor test results. Analysis of cone index (CI) profiles led to the selection of a 0.5-m design sensing depth, 10-MPa maximum expected soil strength, and 0.1-MPa sensing resolution. Compaction level, depth, texture, and water content of the soil all affected CI. The effects of these interacting factors on data obtained with the soil strength sensor should be investigated through experiments. Spatial analyses of CI and TD indicated that the on-the-go soil strength sensor should acquire high spatial-resolution, high-frequency ($\ge$ 4 Hz) measurements to capture within-field spatial variability.

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Structural and Field-emissive Properties of Carbon Nanotubes Produced by ICP-CVD: Effects of Substrate-Biasing (ICP-CVD 방법으로 성장된 탄소 나노튜브의 구조적 특성 및 전계방출 특성: 기판전압 인가 효과)

  • Park, C.K.;Kim, J.P.;Yun, S.J.;Park, J.S.
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.56 no.1
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    • pp.132-138
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    • 2007
  • Carbon nanotubes (CNTs) arc grown on Ni catalysts employing an inductively-coupled plasma chemical vapor deposition (ICP-CVD) method. The structural and field-emissive properties of the CNTs grown are characterized in terms of the substrate-bias applied. Characterization using the various techniques, such as field-omission scanning electron microscopy (FESEM), high-resolution transmission electron microscopy (HRTEM), Auger spectroscopy (AES), and Raman spectroscopy, shows that the structural properties of the CNTs, including their physical dimensions and crystal qualities, as well as the nature of vertical growth, are strongly dependent upon the application of substrate bias during CNT growth. It is for the first time observed that the provailing growth mechanism of CNTs, which is either due to tip-driven growth or based-on-catalyst growth, may be influenced by substrate biasing. It is also seen that negatively substrate-biasing would promote the vertical-alignment of the CNTs grown, compared to positively substrate-biasing. However, the CNTs grown under the positively-biased condition display a higher electron-emission capability than those grown under the negatively-biased condition or without any bias applied.

Physical Properties of High-Solid Coatings with Acrylic Resins Containing Acetoacetoxy Group and HDI-Trimer (Acetoacetoxy기 함유 아크릴수지와 HDI-Trimer에 의한 하이솔리드 도료의 도막물성)

  • You, Hyuk-Jae;Chung, Dong-Jin;Hahm, Hyun-Sik;Park, Hong-Soo;Kim, Seong-Kil
    • Journal of the Korean Applied Science and Technology
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    • v.20 no.3
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    • pp.237-242
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    • 2003
  • The high-solid coatings were prepared by blending the synthesized acrylic resin in the previous paper and hexamethylene diisocyanate-trimer and curing it at room temperature. The characterization of the films of the prepared coatings was performed. The impact resistance, $60^{\circ}C$ specular gloss, cross-hatch adhension, and heat resistance of the films proved to be good, and the pencil hardness and drying time proved to be slightly poor. Especially, there was a remarkable improvement in the heat resistance. This improvement may stem from the regular arrangement of ethyl groups introduced into the acrylic resin. From a viscoelastic measurement using a rigid-body pendulum, curing was accelerated with the $T_g$ value. With the increase in $T_g$, log damp value was lowered and dynamic viscoelasic $T_g$ of a cured film was increased.

Characterization of Soldering Property on Heating Condition by Infrared Lamp Soldering Process for C-Si Photovoltaic Modules (적외선 램프 가열방식을 이용한 태양전지 셀의 솔더링 공정 및 열처리 조건 별 특성 평가)

  • Son, Hyoun Jin;Lee, Jung Jin;Kim, Sung Hyun
    • Current Photovoltaic Research
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    • v.4 no.2
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    • pp.59-63
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    • 2016
  • A key point of a soldering process for photovoltaic (PV) modules is to increase an adhesive strength leading a low resistivity between ribbon and cell. In this study, we intended to optimize a heating condition for the soldering process and characterize the soldered joint via physical and chemical analysis methods. For the purpose, the heating conditions were adjusted by IR lamp power, heating time and hot plate temperature for preheating a cell. Since then the peel test for the ribbon and cell was conducted, consequently the peel strength data shows that there is some optimum soldering condition. In here, we observed that the peel strength was modified by increasing the heating condition. Such a soldering property is affected by a various factors of which the soldered joint, flux and bus bar of the cell are changed on the heating condition. Therefore, we tried to reveal causes determining the soldering property through analyzing the soldered interface.

NMR Microimaging for Noninvasive Investigation of Polymers (고분자의 비파괴 연구를 위한 핵자기 공명 현미영상법)

  • Lee, D.H.;Ko, R.K.;Moon, C.H.;Cho, Z.H.
    • Proceedings of the KOSOMBE Conference
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    • v.1995 no.11
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    • pp.253-256
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    • 1995
  • Polymers have been one of the emerging biomedical materials in the area of biomedical research which are applicable to the human body. For human applications, noninvasive characterization of the biomedical polymers has been one of the important topics, and is valuable information. Among others, the swelling rate is one of the important measurements needed for the hydrophilic polymers. NMR imaging has been a suitable method for the noninvasive study of such a material since it is sensitive to many physical and biochemical changes of the specimens. In addition, NMR techniques possess many useful intrinsic properties such as the relaxation and diffusion effects. The present study has provided a noble and noninvasive method of measuring the process of swelling as well as volumetric changes occurred in polymers and drug delivery processes in a drug delivery system (DDS) together with changes of released drug. This gives information, relating with both water ingress process, volumetric changes of polymer specimens and the visualization of sequential drug delivery process. Also, this study provides more reliable method to ascertain the time dependent swelling process compared to the conventional method. The important aspects is that the proposed method is truly noninvasive and is able to ascertain time dependent processes.

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Physical Properties of High-Solid Coatings with 80% Solid Contents Acrylic Resins Containing Caprolactone Group and HMDI-Trimer (카프로락톤기 함유 80% 고형분인 아크릴수지와 HMDI-Trimer에 의한 하이솔리드 도료의 도막물성)

  • Park, Hong-Soo;Jung, Choong-Ho;Jo, Hye-Jin;Shim, Il-Woo;Kim, Seung-Jin;Kim, Seong-Kil
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.2
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    • pp.110-114
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    • 2006
  • The high-solid coatings were prepared by blending the synthesized acrylic resin in the previous paper, and hexamethylene diisocyanate-trimer and curing it at room temperature. The characterization of the films of the prepared coatings was performed. The $60^{\circ}$ specular gloss, impact resistance, cross-hatch adhesion, and heat resistance of the films proved to be good, and the pencil hardness, drying time, and pot-life proved to be slightly poor. From a viscoelastic measurement using a rigid-body pendulum, curing was accelerated with the Tg value.

Characterization of the Yellow Croaker Larimichthys polyactis muscle Oil Extracted with Supercritical Carbon Dioxide and an Organic Solvent

  • Lee, Joo-Hee;Asaduzzaman, A.K.M.;Yun, Jun-Ho;Yun, Jun-Hyun;Chun, Byung-Soo
    • Fisheries and Aquatic Sciences
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    • v.15 no.4
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    • pp.275-281
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    • 2012
  • Yellow croaker Larimichthys polyactis muscle oil was extracted using an environmental friendly solvent, supercritical carbon dioxide (SC-$CO_2$), in a semi-batch flow extraction process. SC-$CO_2$ was applied at temperature $35^{\circ}C$ to $45^{\circ}C$ and $150^{\circ}C$ to $250^{\circ}C$ bar of pressure. The flow rate of $CO_2$ (27.79 g/min) was constant throughout the entire 1.5 h extraction period. The oil extraction yield was influenced by the physical properties of SC-$CO_2$ at different temperatures and pressures. The extracted oil was analyzed by gas chromatography to determine the fatty acid composition. According to our results, the SC-$CO_2$ extracted oil was high in eicosapentaenoic acid and docosahexaenoic acid. In addition, the SC-$CO_2$ extracted oil showed greater stability than n-hexane extracted oil based on the peroxide value and acid value. Thus, the quality of yellow croaker oil obtained by SC-$CO_2$ extraction was slightly higher than that of oil obtained by n-hexane extraction.

Characterization for $AgGaS_2$ single crystal thin film grown by hot wall epitaxy (Hot Wall Epitaxy(HWE)법에 의해 성장된 $AgGaS_2$ 단결정 박막의 특성)

  • Lee, Gyoun-Gyo;Hong, Kwang-Joon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.11a
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    • pp.101-102
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    • 2006
  • A stoichiometric mixture of evaporating materials for $AgGaS_2$ single crystal thin films was prepared from horizontal electric furnace. To obtain the single crystal thin films. $AgGaS_2$ mixed crystal was deposited on thoroughly etched semi-Insulating GaAs(100) substrate by the hot wall epitaxy (HWE) system. The source and substrate temperatures were $590^{\circ}C$ and $440^{\circ}C$, respectively. The temperature dependence of the energy band gap of the $AgGaS_2$ obtained from the absorption spectra was well described by the Varshni's relation, $E_g(T)=2.7284 eV-(8.695{\times}10^{-4} eV/K)T^2/(T+332 K)$. After the as-grown $AgGaS_2$ single crystal thin films was annealed in Ag-, S-, and Ga-atmospheres, the origin of point defects of $AgGaS_2$ single crystal thin films has been investigated by the photoluminescence(PL) at 10 K.

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Characterization of NR Vulcanizates Cured by Both Sulfur and Resole (황과 레졸로 가교된 천연고무 가교물의 특성)

  • Choi, Sung-Seen
    • Elastomers and Composites
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    • v.35 no.4
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    • pp.261-271
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    • 2000
  • Physical properties of NR vulcanizates cured by both sulfur and resole were studied. Cure characteristics of the compounds were also investigated. Two types of resoles with different molecular weight distributions were employed. The scorch time of the NR compound containing the resole with a low molecular weight distribution was shorter than that of the compound containing the resole with a high one. Crosslink densities of the NR vulcanizates with a high resole content after the thermal aging at $95^{\circ}C$ decreased, while that of the vulcanizate without resole after the thermal aging at $95^{\circ}C$ increased. Though crosslink densities of the NR vulcanizates with a high resole content decreased with increasing the aging time, the moduli increased while the tensile strength and tear strength decreased.

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Fabrication and Characterization of Electrospun PLGA/Gelatin Nanofiber Tube for Potential Intestinal Stent Application

  • Son, So-Ra;Franco, Rose-Ann;Bao, Trinh-Quang;Bae, Sang-Ho;Min, Young-Ki;Lee, Byong-Taek
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.05a
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    • pp.51.1-51.1
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    • 2011
  • An electrospun Poly (lactice-co-glycolide acid) (PLGA) and Gelatin nanofiber tube was fabricated for potential intestinal stent application. Mechanical properties of tube were evaluated by tensile strength and burst strength tests. Physical and chemical properties were evaluated by contact angle measurement, swelling rates and porosity measurements. Biodegradability was investigated by immersion in simulated body fluid (SBF). Biocompatibility was investigated in vitro by cytotoxicity and proliferation studies by MTT assay, confocal microscopy and western blot using IEC-18 (Rat intestinal epithelial cell). After intestinal stent was implanted into rat bowel for periods from 7 to 10days, it was then analyzed using micro-computed tomography (Micro CT) and X-ray techniques. Futhermore, histological analysis was performed by hematoxylin-eosin (H&E) stain.

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