• Title/Summary/Keyword: Physical characterization

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Synthesis and Characterization of Te-rich $Sb_xTe_{1-x}$ Nanowires and Nanotubes (Te이 과량 포함된 $Sb_xTe_{1-x}$ 나노와이어 및 나노튜브의 합성 및 분석)

  • Lee, Joon-Suk;No, Kwang-Soo;Jung, Soon-Won;Yoon, Sung-Min;Yu, Byoung-Gon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.423-423
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    • 2008
  • One dimensional (1D) nanostructures, including nanowires, nanorods, nanobelts, and nanotubes, have been the focus of current research on nanotechnology because of their fundamental significance in chemistry, physics, materials science and engineering, and potential applications in nanoelectronics. We have synthesized Te-rich $Sb_xTe_{1-x}$ nanowires and nanotubes via thermal evaporation method under vapor-solid mechanism. The physical morphology and chemical composition of the fabricated nanowires and nanotubes were investigated by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and energy dispersive X-ray spectroscopy (EDX).

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Fabrication and characterization of graphite nanofiber reinforced aluminum matrix composites (탄소나노섬유 강화 알루미늄 복합재료의 제조 및 특성)

  • Jang J.H.;Oh K.H.;Han K.S.
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.10a
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    • pp.35-38
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    • 2004
  • Graphite nanofiber (GNF) and carbon nanotube (CNT) are novel fiber reinforcing materials which have outstanding physical and mechanical properties. Aluminum matrix composites reinforced graphite nanofiber were fabricated by conventional powder metallurgy (PM) method. The composites were prepared through ultrasonication, ball milling, and hot isostatic pressing. A uniform distribution of GNF in aluminum matrix could be obtained. To measure the mechanical properties of GNF-Al composites testings were done in indentation and compression. The compressive strength was enhanced according to reinforcing graphite nanofiber while the hardness was decreased. This study makes the high performance composites for future applications.

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Characterization of Polyolefin Bumper Recycled by Chemical Removal Method using Electronic Speckle Pattern Interferometry (화학적 박리방법과 ESPI에 의한 재생된 폴리올레핀 범퍼수지의 물성평가)

  • 김현경;강기수;김경석;홍진후
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.10a
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    • pp.295-298
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    • 1997
  • Recycl ing of PP/EPR based bumper coated with polyester urethane paint has been per formed by chemical decoating method. Electronic Speckle Pattern Interferometry (ESP11 has been applied to characterize the deformation of polyolef in based bumper. In additon, physical properties and processability of recycled materials have been investigated by dynamic mechanical thermal analysis, impact test and melt flower index measurement. The results show that the deformation ratio of recycled material is higher than that of virgin one. The morphological change of EPR, degree of distribution and dispersion during the recycling process seem to be the most important factor for the deformation and the mechanical properties of recycled materials. The experimental results obtained show that ESPI is very powerful technique to study the thermal mechanical property of polyolefin bumper system.

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What Distinguishes Mathematical Experience from Other Kinds of Experience?

  • NORTON, Anderson
    • Research in Mathematical Education
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    • v.20 no.1
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    • pp.11-19
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    • 2016
  • Investigating students' lived mathematical experiences presents dual challenges for the researcher. On the one hand, we must respect that students' experiences are not directly accessible to us and are likely very different from our own experiences. On the other hand, we might not want to rely upon the students' own characterizations of what constitutes mathematics because these characterizations could be limited to the formal products students learn in school. I suggest a characterization of mathematics as objectified action, which would lead the researcher to focus on students' operations-mental actions organized as objects within structures so that they can be acted upon. Teachers' and researchers' models of these operations and structures can be used as a launching point for understanding students' experiences of mathematics. Teaching experiments and clinical interviews provide a means for the teacher-researcher to infer students' available operations and structures on the basis of their physical activity (including verbalizations) and to begin harmonizing with their mathematical experience.

Electrochemical Characterization of Nanosized Electrode Arrays Prepared from Nanoporous Self-Assembled Monolayers

  • Choi, Shin-Jung;Park, Su-Moon
    • Bulletin of the Korean Chemical Society
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    • v.23 no.5
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    • pp.699-704
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    • 2002
  • We characterized nanoelectrode arrays prepared from self-assembled monolayers (SAMs) by adsorption from a solution containing thiolated $\beta$-cyclodextrin ($\beta$-CD) and n-alkanethiol on the gold electrode surface, using electrochemical methods. While the framework, the n-hexadecanethiol SAM, effectively blocked electron transfer between the electrode surface and solution-phase redox probe molecules, the $\beta$-CD cavities isolated in the forests of n-hexadecanethiol molecules were shown to act as an ultramicroelectrode array. The shapes of cyclic voltammograms of probe molecules were related to the number densities of $\beta$-CD molecules within the monolayer films. Probe molecules that have the correct combination of physical and chemical characteristics were shown to effectively penetrate the framework through the $\beta$-CD pores and exchange electrons with the electrode surface.

Characterization of Synthesized WS$_2$ Solid Lubricant (합성 WS$_2$ 고체윤활제의 특성 분석)

  • 신동우;윤대현;최인혁;김인섭
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1997.10a
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    • pp.211-216
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    • 1997
  • The tungsten disulfide (WS$_2$) solid lubricant was synthesized by two different reaction processes, and the chemical and physical characteristics of synthesized WS$_2$ powder were analyzed in terms of the average particle size, morphology, crystalline phase. The solid WO$_3$ powder with the average size of 0.2 $\mu$m was reacted with CS$_2$ gas flowed with N$_2$ or 96% N$_2$ + 4% H$_2$ forming gas for 36 h and 24 h at 900$\circ$C respectively. In the case of vapour phase transport method, the 3.5 wt% iodine was added as a vapour transport reagent into the composition of tungsten and sulfur powders maintaining a constant molar ratio of W : S = 1 : 2.2. The mixture was then heat treated at 850$\circ$C for 2 weeks in vacuum The reaction product obtained showed the average size of 12 $\mu$m and the hexagonal plate shape of typical solid lubricant with 2H-WS$_2$ crystalline phase.

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Codium fragile subsp. fragile (Suringar) Hariot in Tunisia: morphological data and status of knowledge

  • Cherif, Wafa;Ktari, Leila;Bour, Monia El;Boudabous, Abdellatif;Grignon-Dubois, Micheline
    • ALGAE
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    • v.31 no.2
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    • pp.129-136
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    • 2016
  • The Mediterranean Sea is currently facing dramatic changes and threats, including change in native species and accidental introductions. The introduced green alga Codium fragile subsp. fragile (Suringar) Hariot influences diversity and community structure in some parts of the world. This paper documents the distribution of this species in Tunisia and provides a morphological description of C. fragile subsp. fragile in Northern Tunisia. Results confirm the identity of Tunisian specimens as the invasive subspecies C. fragile subsp. fragile. This is the first morphological characterization of this subspecies in Tunisia.

Synthesis of Durable Softner for Cotton Fabrics and Its Characterization (면직물용 내구성유연제의 합성과 그의 특성화)

  • Lee, Ki-Chang;Park, Hong-Soo
    • Journal of the Korean Applied Science and Technology
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    • v.7 no.1
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    • pp.87-91
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    • 1990
  • 1,3-Di(2-octadecanoyl)-2,7-dioxy-l,3,6,8-tetra aza cyclodecane [DDTC] was synthesized by reacting octadecanoic acid, 2,2'-di-aminodiethyl amine with urea. O/W type softner (STA) was prepared by blending DDTC and pentaerithritol monostearate with polyoxysthylene (20) oleyl ether, polyoxyethylene (10) castor oil, and PEG #1000-lauric acid ester. Treating STA to all cotton fabrics, the physical properties, such as tear strength, crease recovery, flexing abrasion resistance, and so on were measured. Resulting the measurements, STA was found to be durable softner with softness.

Isolation, Characterization, and Investigation of Surface and Hemolytic Activities of a Lipopeptide Biosurfactant Produced by Bacillus subtilis ATCC 6633

  • Dehghan-Noudeh Gholamreza;Housaindokht Mohammadreza;Bazzaz Bibi Sedigeh Fazly
    • Journal of Microbiology
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    • v.43 no.3
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    • pp.272-276
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    • 2005
  • Bacillus subtilis ATCC 6633 was grown in BHIB medium supplemented with $Mn^{2+}$ for 96 h at $37^{\circ}C$ in a shaker incubator. After removing the microbial biomass, a lipopeptide biosurfactant was extracted from the supernatant. Its structure was established by chemical and spectroscopy methods. The structure was confirmed by physical properties, such as Hydrophile-Lipophile Balance (HLB), surface activity and erythrocyte hemolytic capacity. The critical micelle concentration (cmc) and erythrocyte hemolytic capacity of the biosurfactant were compared to those of surfactants such as SDS, BC (benzalkonium chloride), TTAB (tetradecyltrimethylammonium bromide) and HTAB (hexadecyltrimethylammonium bromide). The maximum hemolytic effect for all surfactants mentioned was observed at concentrations above cmc. The maximum hemolytic effect of synthetic surfactants was more than that of the biosurfactant produced by B. subtilis ATCC 6633. Therefore, biosurfactant would be considered a suitable surface-active agent due to low toxicity to the membrane.

Characterization of TiO2 Synthesized in Acidic Conditions at Low Temperature by Sol-gel Method

  • Nguyen, Thanh Binh;Hwang, Moon-Jin;Lee, Seon-Sam;Choe, Dong-Eon;Ryu, Kwang-Sun
    • Journal of Powder Materials
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    • v.17 no.5
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    • pp.409-414
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    • 2010
  • Titanium dioxide ($TiO_2$), which is one of the most basic materials in our daily life, plays a key role for environment purification. We synthesized $TiO_2$ nanoparticles by the hydrolysis reactions of titanium tetraisopropoxide using $HNO_3$ as a peptizing agent or $CH_3COOH$ as a chelating agent in the sol-gel method. The powder consisted of a rod shape or a spherical shape according to the concentration and kind of acid. The physical properties of $TiO_2$ nanoparticles were investigated with X-ray diffraction, SEM, BET analysis, and UV-Vis spectrophotometer.