• Bulletin of the Korean Chemical Society
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• v.31 no.8
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• pp.2322-2328
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• 2010

A multiple solid-phase extraction (SPE) method was used with liquid chromatography, coupled with mass spectrometry (LC/MS), for the analysis of heterocyclic amines (HCAs) in human urine. Separation efficiencies based on the pH of the mobile phase and the types of columns were compared. An amide column showed better baseline separation and narrower HCA peak widths at pH 5.0 for the mobile phase than a $C_8$ column. Each SPE step, HLB, MCX, and HybridSPE, was optimized by controlling the pH conditions. The combined method with the three SPEs effectively removed interfering species that cause ion-suppression during HCA detection. Validation of the method, performed with SIM and SRM detection, showed correlation coefficients above 0.991 in the range 0.3 - 16.7 ng/mL. Recovery rates were 45.4 - 97.3% on the $C_8$ column and 71.8 - 101.4% on the amide column, and method detection limits were 0.11 - 0.65 ng/mL on the $C_8$ column and 0.12 - 0.48 ng/mL on the amide column. This method using multiple SPEs offers significant benefits for high-throughput determination of HCAs in urine.

• ETRI Journal
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• v.42 no.3
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• pp.324-332
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• 2020

In this paper, a blind symbol timing offset (STO) estimation method is proposed for offset quadrature phase-shift keying (OQPSK) modulated signals, which also works for other linearly modulated signals (LMS) such as binary-PSK, QPSK, 𝜋/4-QPSK, and minimum-shift keying. There are various methods available for blind STO estimation of LMS; however, none work in the case of OQPSK modulated signals. The popular cyclic correlation method fails to estimate STO for OQPSK signals, as the offset present between the in-phase (I) and quadrature (Q) components causes the cyclic peak to disappear at the symbol rate frequency. In the proposed method, a set of close and approximate offsets is used to compensate the offset between the I and Q components of the received OQPSK signal. The STO in the time domain is represented as a phase in the cyclic frequency domain. The STO is therefore calculated by obtaining the phase of the cyclic peak at the symbol rate frequency. The method is validated through extensive theoretical study, simulation, and testbed implementation. The proposed estimation method exhibits robust performance in the presence of unknown carrier phase offset and frequency offset.

• Journal of computational fluids engineering
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• v.12 no.2
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• pp.21-25
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• 2007

A general purpose program NUFLEX has been extended for two-phase flows with topologically complex interface and cavitation flows with liquid-vapor phase change caused by large pressure drop. In analysis of two-phase flow, the phase interfaces are tracked by employing a LS(Level Set) method. Compared with the VOF(Volume-of-Fluid) method based on a non-smooth volume-fraction function, the LS method can calculate an interfacial curvature more accurately by using a smooth distance function. Also, it is quite straightforward to implement for 3-D irregular meshes compared with the VOF method requiring much more complicated geometric calculations. Also, the cavitation process is computed by including the effects of evaporation and condensation for bubble formation and collapse as well as turbulence in flows. The volume-faction and continuity equations are adapted for cavitation models with phase change. The LS and cavitation formulation are implemented into a general purpose program for 3-D flows and verified through several test problems.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.9 s.180
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• pp.2313-2318
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• 2000

The method of photoelasticity allows one to obtain principal stress differences and principal stress directions in a photoelastic model. In the classical approach, the photoelastic parameters are measured manually point by point. This is time consuming and requires skill in the identification and measurement of photoelastic data. Fringe phase shifting method has been recently developed and widely used to measure and analyze fringe data in photo-mechanics. This paper presents the test results of photoelastic fringe phase shifting method for the stress analysis of a curved beam plate. The technique used here requires four phase stepped photoelastic images obtained from a circular polariscope by rotating the analyzer at 0˚, 45˚, 90˚ and 135˚. Experimental results are compared with those of ANSYS and calculated by the simple beam theory. Good agreement among the results can be observed.

• Journal of Power Electronics
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• v.17 no.5
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• pp.1203-1210
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• 2017

This paper presents an improved switching selection method for the direct torque control (DTC) of five-phase induction motors (IMs). The proposed method is conducted using optimal switching selection. A five-phase inverter has 32 voltage vectors which are divided into 30 nonzero voltage vectors and two zero voltage vectors. The magnitudes of the voltage vectors consist of large, medium, and small voltage vectors. In addition, these vectors are related to the torque response and torque ripple. When a large voltage vector is selected in a drive system, the torque response time decreases with an increased torque ripple. On the other hand, when a small voltage vector is selected, the torque response time and torque ripple increase. As a result, this paper proposes an optimal voltage vector selection method for improved DTC of a five-phase induction machine depending on the situation. Simulation and experimental results verify the effectiveness of the proposed control algorithm.

• The Journal of Korean Institute of Communications and Information Sciences
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• v.32 no.12C
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• pp.1149-1155
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• 2007

In this paper, we propose a new overlap and add speech synthesis method which demonstrates improved continuity performance. The proposed method uses a weighted phase error function and minimizes the wave discontinuity of the synthesis signal, rather than the phase discontinuity, to estimate the mid-point phase. Experimental results show that the proposed method improves the continuity between the synthesized signals relative to the existing method.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2003.05a
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• pp.833-838
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• 2003

The problem of elastic wave resonance scattering from elastic targets is studied in this paper. A new resonance formalism to extract the elastic resonance information of the target from scattered elastic waves is introduced. The proposed resonance formalism is an extension of the works developed for acoustic wave scattering problems by the author. The classical resonance scattering theory computes reasonable magnitude information of the resonances in each partial wave, but the phase behaves in somewhat irregular way, therefore, is not clearly explainable. The proposed method is developed to obtain physically meaningful magnitude and phase of the resonances. As an example problem, elastic wave scattering from an infinitely-long elastic cylinder was analyzed by the proposed method and compared to the results by RST. In case of no mode conversion, both methods generate identical magnitude. However, the new method computes exact $\pi$ radian phase shills through resonances and anti-resonances while RST produces physically unexplainable phases. In case of mode conversion, in addition to the phase even magnitudes are different. The phase shifts through resonances and antiresonances obtained by the proposed method are not exactly $\pi$ radians due to energy leak by mode conversion. But, the phases by the proposed method show reasonable and intuitively correct behavior compared to those by RST.

• Proceedings of the KIPE Conference
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• 2019.11a
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• pp.96-97
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• 2019

Pulse Width Modulation (PWM) is a widely adopted technique to drive the motor using the voltage source inverters. Since they generate high frequency Common Mode (CM) Voltage, a high shaft voltage in induction motor is induced which leads to parasitic capacitive currents causing adverse effects such as premature deterioration of ball bearings and high levels of electromagnetic emissions. This paper presents an Active Cancellation Circuit (ACC) which can significantly reduce the CM voltage hence the common mode current in the three phase induction motor drives. In the proposed method the CM voltage is detected by the capacitors and applied to the frame of the motor to cancel the CM voltage hence the CM current. Unlike the conventional methods the proposed method does not insert the transformer in between the inverter and motor, a high power rating three phase transformer is not required and no losses associated with it. In addition the proposed method is applicable to any kind of PWM motor drives regardless of their PWM methods. The effectiveness of the proposed method is proved by the experiments with a three phase induction motor (1.1kW 415V/60Hz) combined with a three phase voltage source inverter modulated by the Space Vector Modulation (SVM).

• Journal of the Korean Institute of Navigation
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• v.18 no.4
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• pp.137-146
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• 1994

In this paper, a new algorithm to measure the ultrasonic travel time is proposed, which is fundamental to estimate distance depth and volume in several media. Pulse wave has been used to measure travel time of transmitted signal. However, due to the characteristic of transducer and propagation, the received signal is so distorted that it is difficult to measure travel time, which is propagation, the received signal is so distorted that it is difficult to measure travel time, which is to be time difference between transmitted and received signals. In this proposed method, transmitted and received signal are transformed respectively into norm phase newly designed by this paper and displayed on phase-time curve. And travel time is simply determined by the arithmetic numerical mean of time difference at the identical norm phase on the phase-time curves of transmitted and received signals. This method has several features; firstly, travel time is calculated analytically with high accuracy by least square error method, secondly, it is useful to compare the difference of signal magnitude for time information, thirdly, noise and discrete errors are relatively small, finally, the measurement accuracy is not influenced by D.C. bias. In particular, this method is useful and applicable to measuring very short distance and sound speed with high accuracy.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.20 no.4
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• pp.375-380
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• 2009

Bit error rate(BER) performance of each bit for hierarchical M-ary phase shift keying(H-MPSK) modulation scheme is changed according to the phase parameters. Thus, a method to find the phase parameters appropriate to the requests of the system is needed. In this paper, we propose a method to obtain the phase parameters from an approximate approach of BER for H-MPSK and verify a validity of the proposed method through the previously provided expression for analyzing an exact error probability of H-MPSK.