• Title/Summary/Keyword: Phase VI

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Solvent Extraction of Trace Mo(VI) in Natural Water Samples by Chelation and Ion-pairing (킬레이트 및 이온쌍 형성을 이용한 자연수 중 극미량 Mo(VI)의 용매추출)

  • Kim, Young-Sang;Nho, Seung-Gu;Choi, Jong-Moon;Choi, Hee-Seon
    • Analytical Science and Technology
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    • v.6 no.3
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    • pp.289-296
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    • 1993
  • The formation of Mo(VI)-alizarin red S chelate ion and its extraction into an organic solvent by ion-pairing were studied for the separative determination of trace Mo(VI) in natural water samples. Natural water 100mL was sampled in 250mL separatory funnel. After Mo(VI)-ARS chelate ion was formed by adding 0.01M alizarin red S solution 0.5mL to the water sample of pH 4.0, 0.2% aliquat-336 chloroform solution 10mL was added and the solution was vigorously shaked for about 30 seconds to from the ion-pair between Mo(VI)-ARS and aliquat-336, completely. The solution was stood for about 90 minutes. And the organic phase was taken for the absorbance measurement of the ion-pair at 520 nm. The content of Mo(VI) in sample was obtained from the standard calibration curve. Several extraction conditions such as pH, adding amounts of alizarin red S and aliquat-336, and shaking and standing times were optimized. This procedure was applied to the analysis of river and tap waters. It could be confirmed from the recoveries of over 99% in samples spiked with a given amount of Mo(VI) that this method was quantitiative in the determination of trace Mo(VI) in a natural water.

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Isolation and Identification of Nonpolar Taxane Derivatives from the Plant Cell Culture of Taxus chinensis

  • Gi, Un-Sook;Min, Bumchan;Hong, Seung-Suh;Lee, Hyun-Soo;Kim, Jin-Hyun
    • Journal of Applied Biological Chemistry
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    • v.43 no.3
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    • pp.176-179
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    • 2000
  • Nonpolar taxoides extracted from a large-scale cell culture of Taxus chinensis were isolated through the normal and reverse phase column chromatographies, and their compounds were identified via NMR spectroscopy. The complete separation method was systematically established and described. In dichloromethane, dissolved paclitaxel and other taxoids with hexane were precipitated during the purification of paclitaxel from the plant cell culture of T. chinensis through a large-scale process while the relatively nonpolar taxane derivatives remained dissolved in the hexane phase. 13-Deoxy baccatin III (I), baccatin VI (II), taxchinin I (III), $2{\alpha}$, $5{\alpha}$, $10{\beta}$, $14{\beta}$-tetraacetoxy-4(20), 11-taxadiene(IV), 1-deoxy baccatinVI(V), and taxayuntin C (VI) were isolated through column chromatography and identified via NMR spectroscopy. Compounds I and IV were found to the major components, aside from paclitaxel, in the plant cell culture of T. chinensis. The concentrations of I and IV were compared with the that concentration of the paclitaxel in each of plant cell culture. The possible applications of compounds I, II, IV, and V were discussed.

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Harmonic Analysis of TCSC Power Transmission System considering Load Characteristics (부하 특성을 고려한 TCSC 전력송전 시스템의 고조파 해석)

  • 정교범
    • Proceedings of the KIPE Conference
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    • 2000.07a
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    • pp.468-471
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    • 2000
  • This paper investigates the harmonics of TCSC power transmission system having nonlinear VI characteristic loads. Nonlinear VI characteristic components are modelled with Nortons harmonic current sources. The system parameters such as line impedances admittances and node voltages and the thyristor switching action are described in complex Fourier series. EMTP simulation studies with a detailed three-phase TCSC power transmission system are also performed in order to verify the harmonic analysis at the steady state.

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A Study on the Calculation of Evapotranspiration Crop Coefficient in the Cheongmi-cheon Paddy Field (청미천 논지에서의 증발산량 작물계수 산정에 관한 연구)

  • Kim, Kiyoung;Lee, Yongjun;Jung, Sungwon;Lee, Yeongil
    • Korean Journal of Remote Sensing
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    • v.35 no.6_1
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    • pp.883-893
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    • 2019
  • In this study, crop coefficients were calculated in two different methods and the results were evaluated. In the first method, appropriateness of GLDAS-based evapotranspiration was evaluated by comparing it with observed data of Cheongmi-cheon (CMC) Flux tower. Then, crop coefficient was calculated by dividing actual evapotranspiration with potential evapotranspiration that derived from GLDAS. In the second method, crop coefficient was determined by using MLR (Multiple Linear Regression) analysis with vegetation index (NDVI, EVI, LAI and SAVI) derived from MODIS and in-situ soil moisture data observed in CMC, In comparison of two crop coefficients over the entire period, for each crop coefficient GLDAS Kc and SM&VI Kc, shows the mean value of 0.412 and 0.378, the bias of 0.031 and -0.004, the RMSE of 0.092 and 0.069, and the Index of Agree (IOA) of 0.944 and 0.958. Overall, both methods showed similar patterns with observed evapotranspiration, but the SM&VI-based method showed better results. One step further, the statistical evaluation of GLDAS Kc and SM&VI Kc in specific period was performed according to the growth phase of the crop. The result shows that GLDAS Kc was better in the early and mid-phase of the crop growth, and SM&VI Kc was better in the latter phase. This result seems to be because of reduced accuracy of MODIS sensors due to yellow dust in spring and rain clouds in summer. If the observational accuracy of the MODIS sensor is improved in subsequent study, the accuracy of the SM&VI-based method will also be improved and this method will be applicable in determining the crop coefficient of unmeasured basin or predicting the crop coefficient of a certain area.

Wind Tunnel Test for Scaled Wind Turbine Model (Scale effect correction) (축소형 풍력터빈 풍동시험-축소효과 보상기법)

  • Cho, Tae-Hwan;Kim, Yang-Won;Park, Young-Min;Chang, Byeong-Hee
    • New & Renewable Energy
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    • v.4 no.2
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    • pp.87-93
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    • 2008
  • Wind tunnel test for the 12% scaled model of NREL Phase VI wind turbine was conducted in KARI low speed wind tunnel for $2006{\sim}2007$. The 1st and 2nd test was designed to find out the wind tunnel test method for the blade manufacturing accuracy and surface treatment method by using the composite and aluminum blades. And the 3rd test was designed to study the scale effect. The chord extension method which was used for Bo-105 40% scaled model was adapted for scale effect correction. Test results shows that the chord extension method works well for the torque slope but the maximum torque for scaled model is about 8% below than the real scale model. New correction method to correct this offset was proposed.

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A Study on the Propriety of Substitute Fuel of Gasoline Engine(VI) (가솔린 엔진용 대체연료의 타당성에 관한 연구(VI))

  • 유정인;양옥용
    • Journal of the korean Society of Automotive Engineers
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    • v.7 no.4
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    • pp.49-56
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    • 1985
  • This study consists of instrumenting and running tests on variable compression engines and measuring the following combustion characterics: (a)flame speed, (b) emission and (c)performance parameter such as power and economy. The results were as follows: 1) The phase separation diagram of substitute fuels were obtained from phase separation experiment. 2) The flame propagation speed of substitute fuels were higher than gasoline and increased with increasing methanol weight percent of substitute fuels. 3) BEMP of substitute fuels was slightly less than that of gasoline but in the range of small weight percent, BEMP was compatible to gasoline. 4) Concentration of NOx decreased significantly with delaying spark advancing time. Also, it decreased for rich equivalence ratio but increased with high compression ratio. In general, NOx concentration was much lower than that of gasoline. 5) Concentration of HC and CO increased for rich equivalence ratio. Also it was lower than that of gasoline.

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Wind Tunnel Test for Scaled Wind Turbine Model (Scale effect correction) (풍력터빈 축소모델 풍동시험 : 축소효과 보상기법)

  • Cho, Tae-Hwan;Kim, Yang-Won;Park, Young-Min;Chang, Byeong-Hee
    • 한국신재생에너지학회:학술대회논문집
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    • 2008.05a
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    • pp.282-285
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    • 2008
  • NREL Phase VI 12% 축소모델을 사용한 표준풍력터빈 풍동시험은 2006$\sim$2007년에 수행되었다. 1,2차 풍동시험은 복합재 및 알루미늄 블레이드를 사용하여 블레이드 제작정밀도 및 표면상태에 의한 영향을 파악하기 위해 수행되었다. 3차 풍동시험은 축소효과보상기법 개발을 위해 수행되었다. Bo-105 40% 모델에 사용된 코드확장기법을 적용하여 15% 코드확장 블레이드를 사용하여 풍동시험을 수행하였다. 시험결과 코드확장기법을 적용할 경우 풍속에 대한 토크 기울기는 실물모델과 잘 일치하나, 최대토크 대비 8%정도 간극을 나타내고 있다. 풍력터빈 블레이드와 같이 캠버가 큰 익형을 사용하는 회전체에 대한 수정된 보상기법을 적용할 경우 이러한 간극은 보상될 수 있다.

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Scaled effect correction method for the wind turbine blade with multi airfoils (다수의 익형이 적용된 풍력터빈 블레이드에 대한 축소효과 보상기법)

  • Jo, Tae-Hwan;Kim, Cheol-Wan
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.494-497
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    • 2009
  • 풍력터빈 블레이드 풍동시험의 경우 사용가능한 시험설비의 크기제한으로 인해 축소모델 사용이 불가피하며, 이로 인해 풍동시험에서는 실물 블레이드에 비해 10% 미만의 낮은 Re수에서 시험이 수행된다. 축소모델 블레이드 풍동시험 결과를 활용하여 실물 블레이드의 성능(토크)를 추정하기 위한 축소효과 보정기법을 2008년 제시하였으며, NREL Phase VI 모델 시험결과에 적용하였다. 당시 제시된 보정기법은 단일익형을 전체 블레이드에 사용한 사례이며 축소효과 보정을 위해 Re수에 따른 익형의 양력계수 변화만을 적용하였다. 본 논문에서는 당시 제안된 축소효과 보정기법을 익형의 양력계수 및 항력계수를 포함한 형태로 수정하였으며, 블레이드에 다수의 익형이 사용되었을 경우에 대해 확장하였다. NREL Phase VI 12% 시험모델의 경우 익형의 양력계수 기울기에 의한 보정량은 약 15% 정도이며, 항력계수 변화에 의한 보정량은 약 5% 정도로 나타났다. 블레이드에 다수의 익형이 사용되었을 경우 설계 또는 전산해석을 통해 구한 반경별 토크 함수를 적용하여 블레이드 축소효과를 보정할 수 있다.

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Wind turbine test results by blade surface condition in wind tunnel test (풍동시험에서 블레이드 표면상태에 따른 풍력터빈 성능변화)

  • Cho, Tae-Hwan;Kim, Yang-Won;Lee, Deok-Ho;Chang, Byeong-Hee
    • New & Renewable Energy
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    • v.3 no.2 s.10
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    • pp.53-59
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    • 2007
  • NREL Phase VI 12% 축소모델을 사용한 표준풍력터빈 풍동시험은 2006년에 1차 시험이 수행되었다. 1차 풍동시험은 복합재블레이드를 사용하여 표준조건(설치각 3도)에 대해 수행되었으며 블레이드 표면상태에 따라 측정값이 영향을 받는 것을 파악하였다. 2007년 4월에 수행된 2차 풍동시험은 표면상태의 영향을 보다 정확히 파악하기 위해 알루미늄 블레이드를 사용하여 시험을 수행하였으며, 블레이드 제작 정밀도에 따른 영향을 파악하였다. 낮은 레이놀즈 수 영역(저속영역)에서는 블레이드 표면상태 따라 토크 값 다르게 나타나며, 블레이드 끝단 부근의 제작 정밀도는 최대 토크 이후의 영역에 영향을 미치는 것으로 나타났다. 0.1mm 이내의 정밀도로 제작된 모델의 경우 NREL 시험결과와 전체적인 형상이 유사하게 나타나며, 축소효과에 의한 영향으로 최대토크는 약 25% 정도 감소현상을 보이고 있다.

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