• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1990년도 제12회 학술강연회초록집
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• pp.58-62
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• 1990

The size and concentration of wear debris in lubricating oil often reveal the operating condition of the rotating machinery. To evaluate the possible application of light attenuation measurement for the estimation of wear debris concentration in the lubricating oil, the light transmittance through the lubricating oil cell contaminated with various concentrations of diatomite particles was measured, the attenuation coefficient was estimated from the transmittance measurement and the coefficients were compared with those obtained from the scattering theory. The comparision showed good agreements between them. It is also noted that the experimentally determined attenuation coefficient showed almost linear relation with particle weight concentrations for the concentrations within the range of 2000 ppm. For the case of 0 ppm weight concentration of diatomite particles in the lubricating oil cell, the thickness of the cell required to give $100 \mu W$ light attenuation is 7.75 mm. This result indicates that the light attenuation method will be one of the possible candidates of machine failure diagnostic sensors for the estimation of wear debris concentration in the lubricating oil.

• Tribology and Lubricants
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• 제6권2호
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• pp.94-98
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• 1990

The size and concentration of wear debris in lubricating oil often reveal the operating condition of the rotating machinery. To evaluate the possible application of light attenuation measurement for the estimation of wear debris concentration in the lubricating oil, the light transmittance through the lubricating oil cell contaminated with various concentrations of diatomire particles was measured, the attenuation coefficient was estimated from the transmittance measurement and the coefficients were compared with those obtained from the scattering theory. The comparision showed good agreements between them. It is also noted that the experimentally determined attenuation coefficient showed almost linear relation with particle weight coucentrations for the concentrations within the range of 2000 ppm. For the case of 0 ppm weight concentration of diatomire particles in the lubricating oil cell, the thickness of the cell required to give $100 \muW$ light attenuation is 7.75 mm. This result indicates that the light attenuation method will be one of the possible candidates of machine failure diagnostic sensors for the estimation of wear debris concentration in the lubricating oil.

• 대한기계학회논문집
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• 제11권3호
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• pp.501-508
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• 1987

본 연구에서는 입자발생 장치를 유동층(fluidized bed)을 이용하여 만들었고 이것에 의해서 고온의 연소가스속으로 입자가 공급되므로, 종래의 초음파입자 발생기 나 오리피스진동입자 발생기등에서 일어나는 호학반응 및 입자상호간의 응집(coagul- ation)현상등을 되도록 없게 하여 순수한 구형입자에 대한 입자부착 효과를 볼 수 있 게 함으로써, 부착기구의 이해와 해석등을 한층 유리하게 한다. 그리고 공급되는 입 자의 크기의 범위를 직경 0.2$\mu\textrm{m}$~30$\mu\textrm{m}$ 정도로 광범위하게 다루어 비교적 간단하고 잘 정의된 층류 유동에서, (1) 미세입자의 경우 실시간(real time) 레이져 광반사법에 의 한 입자부착률의 온도구배 및 농도에 대한 효과를 실험하고, (2) 입자의 Counting/Si- zing 법에 의하여 입자크기에 따른 열확산 효과 및 관성충돌 효과 등을 볼 수 있게 한 다.

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2008년도 춘계학술대회 논문집
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• pp.361-362
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• 2008

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2008년도 추계학술대회 논문집
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• pp.290-291
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• 2008

• Journal of Magnetics
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• 제19권4호
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• pp.323-326
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• 2014

Superparamagnetic maghemite nanoparticles were prepared by chemical co-precipitation, followed by a temperate oxidation stage, and investigated using FE-SEM, XRD, TGA, VSM, and M$\ddot{o}$ssbauer spectroscopy. Through SEM image and XRD analysis, its average particle size was found to be 13.9 nm. While VSM magnetic measurement showed typical superparamagnetic behavior at room temperature, M$\ddot{o}$ssbauer spectroscopic investigation revealed that non-vanishing magnetic hyperfine structure were retained. Cation distribution estimated from M$\ddot{o}$ssbauer spectroscopy confirmed the formation of maghemite nanophase in the sample.

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2002년도 추계학술대회 논문집
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• pp.434-435
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• 2002

에어로졸 입자의 크기 분포를 측정하는: 방법은 여러 가지가 있다. 이중 광학 입자계수기(Optical Particle Counter)는 직경 0.3-25$\mu\textrm{m}$의 입자의 산란광의 강도를 측정하여 입자의 크기별 개수를 측정하는 기기로 청정지역의 대기 중 부유하는 입자의 측정에 널리 사용되고 있다 (전영신 등, 1999). 본 연구에서는 기상청 기상연구소에서 측정한 광i부 입자계수기(HYAC/ROYCO 5230)의 측정자료를 이용하여 2001년도 1년간 서울의 대기 에어로졸의 특성과 경향을 분석하였다. 측정결과는 대기환경월보(환경부, 2001) (중략)

• 공업화학
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• 제21권6호
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• pp.670-675
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• 2010

나노실리카볼 입자를 합성하고 표면에 비닐기를 부여하는 합성 연구를 통해 다양한 크기로 조절이 된 유-무기하이브리드 입자인 비닐-나노실리카볼이 합성되었다. 다양한 크기의 비닐-나노실리카볼 입자를 상업적으로 적용되고 있는 아크릴-멜라민 클리어코트에 후첨시키고 경화시켰을 때, 클리어코트의 광택도 증가 및 유지 특성에 대해 연구하였다. 실리카볼 입자가 250 nm 정도인 경우 Matting effect에 의한 광택도 감소가 관측되었으나 20~30 nm로 작아지면 광택도 유지 효과가 약 7%까지 증가하였다. 나노실리카볼 대신 상업용 친수 실리카 Aerosil 200 (Hydrophilic fumed silica, 평균입도 12 nm, Degussa)을 사용하여 비닐- fumed 실리카 화합물을 합성하여 클리어코트에 적용하면 광택도 유지 효과가 약 2% 정도만 증가하였다.

• 한국수소및신에너지학회논문집
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• 제31권5호
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• pp.453-458
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• 2020

In this study, ethylene-propylene-diene monomer (EPDM) rubbers reinforced with various particle size of carbon black were prepared and tested. We followed recently published CSA/ANSI CHMC2 standard "the test methods for evaluating material compatibility in compressed hydrogen applications-polyemr". Measurement of change in hardness, tensile strength and volume were performed after exposure to maximum operating pressure, 87.5 MPa, for 168 hours (1 week). Once EPDM was exposed to high-pressure hydrogen, the samples experience volume increase and degradation of the physical properties. Also, after the dissolved hydrogen was fully eliminated from the specimens, the hardness and the tensile properties were not recovered. The rubber reinforced with smaller sizes of carbon black particles showed less volume expansion and decrease of physical properties. As a result, smaller particle size of carbon black filler led to more resistance to high-pressure hydrogen.

• 한국분말재료학회지
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• 제23권2호
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• pp.136-142
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• 2016

As precursors of cathode materials for lithium ion batteries, $Ni_{1/3}Co_{1/3}Mn_{1/3}(OH)_2$ powders are prepared in a continuously stirred tank reactor via a co-precipitation reaction between aqueous metal sulfates and NaOH in the presence of $NH_4OH$ in air or nitrogen ambient. Calcination of the precursors with $Li_2CO_3$ for 8 h at $1,000^{\circ}C$ in air produces dense spherical cathode materials. The precursors and final powders are characterized by X-ray diffraction (XRD), scanning electron microscopy, particle size analysis, tap density measurement, and thermal gravimetric analysis. The precursor powders obtained in air or nitrogen ambient show XRD patterns identified as $Ni_{1/3}Co_{1/3}Mn_{1/3}(OH)_2$. Regardless of the atmosphere, the final powders exhibit the XRD patterns of $LiNi_{1/3}Co_{1/3}Mn_{1/3}O_2$ (NCM). The precursor powders obtained in air have larger particle size and lower tap density than those obtained in nitrogen ambient. NCM powders show similar tendencies in terms of particle size and tap density. Electrochemical characterization is performed after fabricating a coin cell using NCM as the cathode and Li metal as the anode. The NCM powders from the precursors obtained in air and those from the precursors obtained in nitrogen have similar initial charge/discharge capacities and cycle life. In conclusion, the powders co-precipitated in air can be utilized as precursor materials, replacing those synthesized in the presence of nitrogen injection, which is the usual industrial practice.