• Title/Summary/Keyword: Particle Sedimentation

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TEM Specimen Preparation Method of Gibbsite Powder for Quantitative Structure Analysis (정량 구조 분석을 위한 Gibbsite 분말의 TEM 시편 준비법)

  • Kim, Young-Min;Jeung, Jong-Man;Lee, Su-Jeong;Kim, Youn-Joong
    • Applied Microscopy
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    • v.32 no.4
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    • pp.311-317
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    • 2002
  • There is great requirement on the TEM specimen preparation method with particle size selectivity as a prerequisite for the quantitative structure analysis on the materials such as gibbsite powder, which generally forms a large agglomerate and shows a variation of transition process depending on their sizes. In this experiment, we made an attempt to give a methodology for the TEM specimen preparation of powder with the size selectivity. After mixing 1 wt% gibbsite powder with ethanol solvent, gibbsite suspension was prepared by application of ball-milling and ultrasonification with addition of 0.25 vol% dispersion agent, Darvan C, which was diluted into distilled water by the ratio 1:19. Appling the static sedimentation method to gibbsite suspension after estimation of the sedimentation time by the measurement of accumulative concentration variation, we acquired TEM specimens with well-dispersed and size selected gibbsite particles in nm scale. Overall picture of each sample was taken by SEM and morphology of each dispersed particle was imaged by TEM. Raw and processed gibbsite powders were also examined by XRD to investigate whether they were suffered from phase change during the process or not.

Preparation of Kyungohkgo Suspension Beverage Containing Cultivated Wild Ginseng (산양삼경옥고 현탁음료의 제조)

  • Kwon, Se Uk;Lee, Hoon Yeon;Xin, Mingjie;Il, Ji Young;Cha, Ji Yun;Kim, Hyo Jin;Kwak, Woo Ri;Go, Chun Kyu;Kim, Dae Ki;Lee, Young Mi
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.27 no.2
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    • pp.233-238
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    • 2013
  • The development of healthy beverages are increasing by big concerns for well-being. The aim of this study is to develop cultivated wild ginseng-Kyungohkgo (CKOG) beverage using cultivated wild ginseng instead of natural wild ginseng for Kyungohkgo. To examine physiochemical properties of CKOG beverage, pH, degree Brix, acidity, Huntor color, particle size and sedimentation volume were measured. When compared with commercial KOG beverage, CKOG beverage was lower in pH, acidity, particle size and higher in sedimentation volume. In the sensory evaluation of CKOG beverage, the best recipe of healthy CKOG beverage was 20% CKOG, 5.7% honey, 0.2% citric acid and 74.1% of water. In stability testing, pH, degree Brix, acidity, Huntor color of CKOG beverage was not changed, microbes in CKOG beverage was not detected for 60 days. These results suggest that CKOG may have a possibility of development as healthy beverage.

The Evaluation of the Thick Polycrystalline HgO and PbO Films Derived by Particle Sedimentation Method for the Mammographic Application (입자침전법을 이용한 다결정 산화수은과 산화납 필름의 방사선 유방촬영 장치 적용성 평가)

  • Noh, Si-Cheol;Park, Ji-Koon;Choi, Il-Hong;Jung, Hyoung-Jin;Kang, Sang-Sik;Jung, Bong-Jae
    • Journal of the Korean Society of Radiology
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    • v.8 no.7
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    • pp.429-433
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    • 2014
  • In this study, the morphology and the x-ray quantum efficient of mercury oxide (HgO) and lead oxide (PbO) sensors derived by particle sedimentation method were discussed. In the pursuit of this purpose, we investigated the electrical characteristics and the x-ray quantum efficiency of various thicknesses of HgO and PbO films in mammographic x-ray energy. We have therefore developed a particle-in-binder sedimentation method of fabricating large area polycrystalline films onto transparent glass substrates coated with indium tin oxide. We are currently optimizing the growth method to improve the quantum efficiency with the ultimate goal of obtaining as quantum efficiency close to that of single crystal performance. Our future efforts will concentrate on optimization of large area film growth techniques specifically for deposition on a-Si:H flat panel readout arrays.

Time-series Changes in Particle Size Characteristics of Suspended Sediment at the Seungchon and the Juksan Weir in the Yeongsan River (영산강 부유하중의 시계열적 입도 특성 변화: 승촌보, 죽산보를 중심으로)

  • Lim, Young Shin;Kim, Jin Kwan
    • Journal of The Geomorphological Association of Korea
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    • v.26 no.4
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    • pp.1-20
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    • 2019
  • In order to establish appropriate policy to control sediment-associated problems, it is necessary to identify the physical characteristics of the reservoir sediments in particulate form in the Yeongsan River. Two time-integrated suspended sediment samplers were installed at Seungchon and Juksan weir on the upper and middle Yeongsan River in July 2012. Reservoir sediment samples were obtained at monthly intervals until October 2014. During the monitoring period, a total of 38 sediment samples were obtained and analyzed. Seasonal trends of suspended sedimentation rates and grain size distributions were examined based on variations in precipitation and discharge fluctuations. Moreover, stream flow characteristics, which has a great influence on the physical characteristics of the river sediment, was analyzed using flow duration curve for the period 2003-2019 at Naju gauging station. Sedimentation rates during summer, when heavy rainfall was concentrated due to the monsoonal front and typhoon, were very high, indicating the positive relationship between sediment concentration and discharge. Particle size analysis of the collected sediment showed that coarse silt and very fine sand-sized sediment dominated most of the Seungchon weir sediment. On the other hand, medium silt-sized sediment dominated the downstream Juksan weir except for a few summer samples. These results implied that the physical characteristics of the suspended sediment are determined not only due to flow fluctuations, but also with regard to the antecedent rainfall conditions, hillslope-channel connectivity, and the supply of materials from various contributing regions. This information about flow characteristics and temporal variations in reservoir sediment can be used for safe management of the weir and discussing the issues on the dismantling of the weirs.

Enhanced Dispersion of Yttria Stabilized Zirconia by Mixed Dispersants Containing Carboxyl Group in Aqueous System (수성 현탁액에서 카르복실기를 포함하는 혼합 분산제에 의한 이트리아 안정화 지르코니아의 분산성 향상)

  • Kim, Soo-Hyun;Kang, Jong-Bong;Bae, Sung-Hwan
    • Korean Journal of Materials Research
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    • v.28 no.2
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    • pp.82-88
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    • 2018
  • Stable slurries of YSZ in aqueous suspension with added polymer dispersants, namely, poly-methacrylic acid ammonium salt (PMMA), poly-acrylic acid (PAA) and poly-acrylic-co-maleic acid (PAMA), were mixed with the monomolecular dispersants citric acid and oxalic acid. The dispersion properties of the suspension were investigated using PSA, viscosity, sedimentation, and FT-IR. The polymer dispersants and monomolecular dispersants were attached to the YSZ surface by the carboxylic group, as shown by the FTIR results. A stabilized aqueous suspension was obtained when the polymer dispersant and citric acid were mixed and compared to the use of citric acid alone as a dispersant agent. When the polymer dispersant and citric acid were mixed and milled through attrition milling, there was a smaller particle size compared to when the polymer dispersant alone was used as a dispersant agent. This study determined that the particle size of the mixed dispersant was affected by the properties of the monomolecular dispersant and that the stability of the suspension was affected by the polymer dispersant. However, when slurries of YSZ were mixed with oxalic acid, the particle bridging behavior was the result of the high degree of viscosity and the small sedimentation height.

Simulation of Solid Particle Sedimentation by Using Moving Particle Semi-implicit Method (고체 입자형 MPS법을 이용한 토사물 퇴적 시뮬레이션)

  • Kim, Kyung Sung;Yu, Sunjin;Ahn, Il-Hyuk
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.24 no.1
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    • pp.119-125
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    • 2018
  • The particle based computational fluid dynamics (CFD) method, which follow Lagrangian approach for fluid dynamics, fluid particle behavior by tracking all particle calculation physical quantities of each particle. According to basic concept of particle based CFD method, it is difficult to satisfy continuum theory and measure influences from neighboring particle. Article number density and weight function were used to solve aforementioned issue. Difficulties continuum mean simulate non-continuum particles such as solid including granular and sand. In this regard, the particle based CFD method modified solid particle problems by replacing viscous and surface tension forces friction and drag forces. In this paper, particle interaction model for solid particle friction model implemented to simulate solid particle problems. The broken dam problem, which is common to verify particle based CFD method, used fluid or solid particles. The angle of repose was observed in the simulation results the solid particle not fluid particle.

Dispersion of nanodiamond by Chemical treatment (나노다이아몬드의 화학적 처리에 따른 분산 특성)

  • Park, Jong-Soon;Kim, Hong;Kang, Soon-Kuk
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.12 no.2
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    • pp.999-1004
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    • 2011
  • In this study, nanodiamod's surface have formed carboxyl, hydroxyl, amine radical for the purpose of use of nanodiamond synthesized by detonation, and then it has widely stable dispersion and slowly sedimentation in solvent. Thus nanodiamonds obtained by chemical treatment were used to analyze the structure, surface statement, particle size and sedimentation specification in solvent for method X-ray diffration(XRD), scanning electron microscope energy diffraction spectroscopy(SEM-EDS), Fourier transform infrared spectroscopy (FTIR), automic force microscope(AFM).

Rates of Sediment Accumulation and Particle Mixing in the KODOS Site of the Clarion-Clipperton Fracture Zones (클라리온-클리퍼톤 KODOS 지역 퇴적물의 퇴적율과 입자혼합율)

  • MOON, DEOK SOO;KIM, KEE HYUN
    • 한국해양학회지
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    • v.30 no.4
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    • pp.288-301
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    • 1995
  • Rates of the sedimentation and particle mixing have been estimated by applying uranium-series disequilibrium techniques to three sediment cores collected from the korea Deep Ocean Study (KODOS) site between the clarion and Clipperton Fracture Zones (CCFZ) of the Equatorial Pacific. Sedimentation rates based on the profiles of excess /SUP 230/Th activity and /SUP 230/ Th/SUB xs//SUP 232/ Th activity ratios at the southeastern part of the study area were estimated to be in the order of a few millimeters per thousand year, while at the northwestern part a factor of ten lower. Excess activities of /SUP 230/Th and /SUP 230/Th ratios showed intervals of constant values in the upper part of the sediment cores, probably generated by biological particle mixing. A "two-box" advection-diffusion steady state mixing model was employed in order to estimate particle mixing rates in the upper and the lower layers, based on the distribution profiles of excess /SUP 210/Pb activities. Particle mixing coefficients were estimated to be in the order of 10$^1$ cm$^2$/y in the upper layer and 10/SUP -1/-10/SUP 0/ cm$^2$/y in the lower layer.

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The Evaluation of White Water Sedimentation Efficiency in Settling Tank by the Addition of Flocculents (응집제 첨가에 의한 침전조의 백수침전 효율 평가)

  • Kim Hyoung Jin;An Jung Song;Yoo Sung Ho
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.36 no.4 s.107
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    • pp.67-76
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    • 2004
  • Because paper industry spends lots amount of water, the recycling of water is very important in economical as well as environmental aspects. In order to optimize the process water recycling system, the efficiency of unit operation for water circulation, such as save-all system, CDS and settling tank, plays an important role in. In this study, the sedimentation efficiency of process water was evaluated by SS measurement with the different amounts of flocculent addition. 3 different kinds of process water were collected from fine paper mill, and applied in laboratory sedimentation equipment for the measurement of settling efficiency of SS materials. The addition amounts of alum and PAC were resulted in optimum efficiency of sediments in the condition of 100 ppm of alum and 500 ppm of PAC respectively. In the comparison of sedimentation efficiency between alum and PAC, alum showed more economical and efficient results. The SS of spill water and the particle size of suspended materials treated by alum flocculents were below 50 ppm and about 1 $\mu$m. It would be considered that the spill water can be substituted to superclear water grade.

Characteristics of Particle Deposition onto Cleanroom Wall Panel for Varying Particle Charging Rates (입자하전량에 따른 클린룸 수직벽체로의 입자침착 특성)

  • Kim, Jong-Jun;Noh, Kwang-Chul;Sung, Sang-Chul;Baek, Sun-Ho;Oh, Myung-Do
    • Proceedings of the SAREK Conference
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    • 2008.06a
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    • pp.725-730
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    • 2008
  • In this study, we found out charged particle's deposition characteristic by experiments of $0.5{\mu}m$, $1.0{\mu}m$, $3.0{\mu}m$ size particle's concentration decay. We carried out the experiments on charged particle deposition onto the vertical cleanroom wall panel and some other fundamental experiments. The particle deposition mechanism is consist of sedimentation, convection, diffusion, thermophoresis, electrostatic and so on. Particle size determines mainly working deposition mechanism. The charged particle is made with corona discharge that are constituted field charging and diffusion charging. In addition, this combinational mechanism is called combined charging. The type of corona discharge determines quantity of particle electrical charge. In conclusion, we assumed that quantity of particle electrical charge accelerations deposition velocity onto the vertical cleanroom wall panel and proved it. And we figured out particle's deposition characteristic through compared between our experiment's results.

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