• Title/Summary/Keyword: Particle Composition Analysis

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Particle Crushing Properties of Decomposed Granite Soil due to Changes in the Degree of Weathering (풍화도 변화에 따른 화강풍화토의 파쇄특성)

  • Lee, Kang-Il;Yoon, Young-Goo;Lee, Jae-Wook
    • Journal of the Korean Geosynthetics Society
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    • v.12 no.1
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    • pp.1-10
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    • 2013
  • In this study, the characteristics of particle crash of decomposed granite soil sampled at Pocheon area were presented. The degree of weathering was artificially achieved by means of hydrofluoric acid. Weathering index was firstly determined by the analysis of mineral composition. Then, particle distribution, permeability tests were conducted. The results showed that weathering effects on particle crash over entire particle sizes. Comparative analysis on specific surface between $D_{10}$ and $D_{50}$ indicated that the smaller the particle size, the more the particle crash. In addition, the most particle crashing due to compaction appeared around the optimum moisture content. The incremental ratio of specific surface appeared to decrease as weathering proceeds, which means that the higher the weathering index the less the particle crash.

Evaluation of Characteristics of Particle Composition and Pollution of Heavy Metals for Tidal Flat Sediments in Julpo Bay, Korea (줄포만 갯벌의 입도특성 및 중금속 오염도 평가)

  • Kim, Jong-Gu;You, Sun-Jae;Ahn, Wook-Sung
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.14 no.4
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    • pp.247-256
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    • 2008
  • For the systematic scientific management of tidal flat sediment in Julpo bay of Korea, this study conducted a survey of particle composition, organic matter(l.L) and heavy metals for three lines ; including F, R and L lines in tidal flat sediment. Particle composition of tidal flat sediments consisted predominantly of clay at F line which was in right angle direction to the coast, whereas R and L lines were located horizontally along the coast and consisted predominantly of silt. Mean grain size values of tidal flat sediments were in the range of 3.7 ${\phi}{\sim}$10.4 ${\phi}$(average 7${\phi}$). The contents of heavy metals observed at R and L lines were lower than those at F line. The correlation analysis among heavy metals, organic matter and particle size was found to have a good interrelationship. For the evaluation of heavy metals pollution, two criteria of US NOAA and KEI(in Korea) were applied Heavy metals pollution level of tidal flat sediments belonged in Non polluted and Moderately polluted groups in US EPA criteria, and its pollution levels sat below ERL in NOAA criteria. The results of heavy metals pollution level obtained by KEI criteria were found to be less than the goal level.

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A Study on Analysis of J85 Engine V.G. Actuator Arm Shaft Crack

  • Hwang, Young-Ha;Son, Kyung-Sug;Kim, Tae-Gu
    • International Journal of Safety
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    • v.8 no.1
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    • pp.6-9
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    • 2009
  • The crack in a J85 engine V.G. actuator arm shaft for a bell crank on the engine compressor was investigated. The crack was observed in twenty two shafts during the inspection of 238 shafts. The failure analysis of shaft cracks was performed by chemical composition analysis using ICP(Inductively Coupled Plasma) and by fracture surface and microstructure analysis using FE-SEM and optical microscope. The crack initiated from the top and bottom and propagated to the center along the grain boundaries. From the chemical composition analysis, the fractography of the fracture surface and the microstructure, it was found that the failure mechanism of the shafts is the inclusion-related intergranular decohesion crack. The inclusion was found out from MnS particle by EDS(Energy Dispersive Spectroscopy). The crack initiated MnS inclusion in the grain boundary and propagated with the increase of applied shear stress during long operation. In order to prevent the fracture, NDI(Nondestructive inspection) is needed periodically as recommended.

Quantitative Analysis of Wear Debris for Surface Modification Layer by Ferrography (Ferrography에 의한 표면개질층의 마모분 정량분석)

  • 오성모;이봉구
    • Tribology and Lubricants
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    • v.15 no.3
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    • pp.265-271
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    • 1999
  • Wherever there are rotating equipment and contact between surface, there is wear and the generation of wear particles. The particles contained in the lubricating oil carry detailed and important information about the condition monitoring of the machine. This information may be deduced from particle shape, composition, size distribution, and concentration. Therefore, This paper was undertaken to Ferrography system of wear debris generated from lubricated moving machine surface. The lubricating wear test was performed under different experimental conditions using the Falex wear test of Pin and V-Block type by Ti(C, N) coated. It was shown from the test results that wear particle concentration (WPC) and wear severity Index( $I_{S}$), size distribution in normal and abnormal wear have come out all the higher value by increases sliding friction time. Wear shape is observed on the Ferrogram it was discovered a thin leaf wear debris as well as ball and plate type wear particles. This kind of large wear shape have an important effect not only metals damage, but also seizure phenomenon.

Uranium Isotopic Ratio Analysis of U-Bearing Particulates By SIMS in CIAE

  • Yonggang, Zhao
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2004.02a
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    • pp.257-259
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    • 2004
  • In this paper measurement method of uranium isotope ratio of uranium-bearing particles in swipe samples was introduced; Swipe sample screening program was proposed on the basis of studying various destructive assay and non-destructive assays. Scanning electron microscope(SEM) equipped with an energy dispersive X-ray fluorescence(XRF) system was applied to locate the deposited uranium-containing particles on the graphite support, particle's composition and size can be identified. Some isotope ratio results were compared with those of other bulk analytical methods; By measuring the same prepared sample, we got the U-particle isotopic ratio data similar to those from IAEA NWAL, indicating that our operation parameters and experimental conditions are viable and can be used for measurement of U-particle isotopic ratio from swipe samples.

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Analytical Method for Determination of the Content of Tire Wear Particle in Tire and Road Wear Particles

  • Son, Chae Eun;Choi, Sung-Seen
    • Elastomers and Composites
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    • v.56 no.1
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    • pp.1-5
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    • 2021
  • Tire and road wear particles (TRWPs) were collected from road dust and thermogravimetric analysis (TGA) was performed to measure the content of tire wear particles (TWPs) in the TRWPs. The TGA thermograms of TRWPs showed two weight loss steps associated with polymer decomposition including weight loss after 480℃ which may be due to road wear particles. Different samples gave different TGA thermograms because the types and contents of the road wear particles attached to the TWPs should be different from each other, and each TWP might have different composition. The TGA results of the model asphalt pavement wear particles, with (volatile organics + polymers + carbon black) : ash = 33.5 : 66.5, was applied to the TRWP results, and the TWP contents of TRWPs were found to be 50-65%. The zinc oxide content in the rubber compound was negligible.

Analysis of Deposited Dust Particles using SEM/EDX (SEM/EDX 분석법을 이용한 침착먼지에 대한 분석사례)

  • Ha, Eun-Ji;Park, Jeong-Ho
    • Journal of Environmental Science International
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    • v.30 no.3
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    • pp.279-287
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    • 2021
  • In this study, the composition and morphology of deposited dust particles with size ranging from a few to tens ㎛ were investigated using SEM/EDX (scanning electron microscopy with energy dispersive x-ray spectrometer). Then deposited dust particles were classified into 8 groups: quartz, aluminosilicates, ca-rich, Fe/Ti oxide, carbon-rich, industrial particle, Fe-rich, and biogenic particle. The sources of deposited dust were high in the order of aluminosilicates 41% > biogenic 18% > Fe-rich 11% > quartz and C-rich 8% > industrial 7% > Fe/Ti oxide 5% > Ca-rich 1%. In particular, the ratio of biogenic particles was relatively high due to influence of pollen. The ratio of carbon-rich was 11% at YM site, 10% at MD site, and 4% at MO site, and the site close to the large emission source was high.

PRELIMINARY STUDY ON THE ALPHA TRACK ANALYSIS OF SPHERICAL URANIUM METAL PARTICLES

  • Pyo Hyung-Yeol;Kim Jong-Yun;Lee Myung-Ho;Park Yong-Jun;Jee Kwang-Yong;Kim Won-Ho
    • Nuclear Engineering and Technology
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    • v.38 no.4
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    • pp.353-358
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    • 2006
  • Alpha track analysis for the determination of the trace amount of alpha emitting nuclides in a very small particle was performed as an efficient and powerful technique during safeguard inspection. Metal particles with well-defined spherical shape, size and isotopic compositions as a reference material were used to correlate the number of tracks or track diameter with an isotopic composition eventually to identify the uranium enrichment in the environmental swipe samples. Slopes in the number of tracks versus the exposure time curve provide a simple insight into the uranium enrichment of an unknown particle. Low enriched uranium metal particles result in slopes still steeper than the depleted or natural uranium metal particles. In addition, a linear relationship between track diameter and particle size Is thought to be a useful first stage analytical tool as an efficient and convenient inspection guide. The significance of the simple linear model was also judged using the usual statistical tests.

Comparison of Dustiness of Eleven Nanomaterials using Voltex Shaker Method (볼텍스쉐이커를 이용한 11개 나노물질의 분진날림 비교)

  • Lee, Naroo;Park, Jinwoo
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.28 no.3
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    • pp.273-282
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    • 2018
  • Objectives: Dustiness of nanomaterials is considered as exposure index of essential material. Research on dustiness of nanomaterial is needed to control exposure in workplaces. Method: Dustiness measurement using vortex shaker were installed in the laboratory. Nanomaterials, 1 g, was put in the glass test tube and shaked using vortex shaker. Aerosol dispersed was measured using scanning mobility particle sizer(SMPS) and optical particle counter(OPC). Mass concentration using PVC filter and cassette was measured and TEM grid sampling was conducted. Total particle concentration and size distribution were calculated. Image and chemical composition of particles in the air were observed using transmission electron microscopy and energy dispersive X-ray spectrometer. Eleven different test nanomaterials were used in the study. Results: Rank of mass concentration and particle number concentration were coincided in most cases. Rank of nanomateirals with low concentration were not coincided. Two types of fumed silica had the highest mass concentration and particle number concentration. Indium tin oxide, a mixture of indium oxide and tin oxide, had high mass concentration and particle number concentration. Indium oxide had very low mass concentration and particle number concentration. Agglomeration of nanoparticles in the air were observed in TEM analysis and size distribution. In this study, mass concentration and particle number concentration were coincided and two index can be used together. The range of dustiness in particle number concentration were too wide to measure in one method. Conclusion: Particle number concentration ranged from low concentration to high concentration depend on type of nanomaterial, and varied by preparation and amount of nanomaterial used. Further study is needed to measure dustiness of all nanomaterial as one reference method.

Mathematical Model and Numerical Analysis for Packed Bed Methanation Reactors (충전층 메탄화 반응기의 수학적 모델 및 전산 수치해석)

  • CHI, JUNHWA
    • Transactions of the Korean hydrogen and new energy society
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    • v.26 no.3
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    • pp.260-270
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    • 2015
  • One-dimensional packed bed reactor model accounting for interfacial and intra-particle gradients was developed and based on it numerical analyses were performed to investigate the dynamic behavior of a commercial scale methanation reactor. Methanation reaction was almost complete near the reactor inlet and gases with equilibrated composition were discharged from the reactor. Both the intra-particle temperature gradient and differential surface temperature rise were found to be severe near the reactor inlet. To reduce the possible degradation or fracture of catalyst particles and prevent local overheating on the catalyst, addition of inert material can be an effective way.