• Journal of Sericultural and Entomological Science
• /
• v.37 no.2
• /
• pp.154-160
• /
• 1995

Dyeing behavior of Silk/Cationic dyeable polyester(CDP) mixed filament was investigated by using a cationic dye. The effect of pH, temperature and additives such as carrier, levelling agent and salt were examined for each silk and CDP component of mixed filament in order to find out the optimum dyeing condition. Based on these results, the dyeing behavior was investigated for Silk/CDP mixed filaments concering various dyeing parameters. The dye adsorption was significantly changed on the dyeing temperature, carrier addition and pH of the dyebath. Specially, the dye migration phynomena were observed for a mixed filament, showing that the dyes initially observed on the surface of silk fiber migrate to the CDP component during a dyeing process. The dyeing of Silk/CDP mixed filaments accompanied by dye migration and as a result, dye adsorption can be developed only for a CDP component. Therefore, the control of dyeing temperature is most important for a Silk/CDP mixed filament, in order that both silk and CDP component are able to be dyed by a cationic dye simultaneously in one bath/one dye system.

• Fashion & Textile Research Journal
• /
• v.19 no.5
• /
• pp.620-625
• /
• 2017

In this study, the dyeing conditions(temperature, time, concentration) are changed from various conditions on wool fabrics by using corydalis tuber extract in order to develop new natural dyes. The purpose of this study is to improve the dyeability, color fastness, and functionality and to derive optimal dyeing conditions by comparing and analyzing the changes of K/S values and surface color by dyeing pH changes, mordant method, and mordant type. As a result of the experiment, the optimum dyeing condition of the wool fabrics is shown dyeing temperature:$80^{\circ}C$, dyeing time:90min, dyeing concentration:100%. The dyeability by pH variants of corydalis tuber extract indicates that K/S values is higher alkaline than acidic. The mordant method of corydalis tuber extract showed pre-mordant has high K/S values. In terms of color fastness, marked improvement has not been shown despite of mordant treatment on wool fabrics. In particular, color change of color fastness to washing, color fastness to light indicates the low fastness. In addition, the functionality such as antibacterial activities and deodorization can be given at dyeing with corydalis tuber extract thus it is expected to be applied to underwear or apparel products for the elderly and infirm and children with weak skin that required high functionality.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.33 no.7
• /
• pp.1121-1127
• /
• 2009

This study presents an eco-friendly and one-step finishing method for modifying fiber property that reduces fiber damage in wool/polyester blend fabrics. Lipase from aspergillus oryzae is used in this experiment. The enzymatic treatment condition is optimized by measuring the relative activity of lipase depending on pH level, temperature, concentration of lipase, and treatment time. The concentration of $CaCl_2$as an activator is determined by the characteristics including whiteness, water contact angle (WCA), and dyeing property. The modified properties of lipase treated fabrics are tested for pill resistance and surface morphology. The results are described as follows: the optimum condions for lipase treatment constitute a pH level of 8.0, treatment temperature of 40$^{\circ}$$_C$, concentration of lipase at 100% (o.w.f), and a treatment time of 90 minutes. $CaCl_2$helps in raising lipase activation, and the optimum concentration is 50mM. The whiteness, wet ability, and pill resistance of lipase treated fabrics improves as compared to the control. The dyeing property of lipase treated fabrics improved by 53.5% after using the one-bath dyeing method. This means that lipase treatment can save time and cost during the dyeing process since lipase treatment modifies wool and polyester fibers. The surface of lipase treated wool fibers do not exhibit any change, however voids and cracks manifest on the surface of lipase treated polyester fibers.

• Journal of Biosystems Engineering
• /
• v.30 no.4 s.111
• /
• pp.242-248
• /
• 2005

There was no useful milling standard to produce high quality milled rice efficiently and adequately in Rice Processing Complex. Therefore, the whiteness of milled rice produced Rice Processing Complexes were different according to Rice Processing Complexes and milling periods at the same Rice Processing Complex. This research was carried out to contribute the production and distribution of high quality milled rice through determination of whiteness condition of milled rice as a milling stndard based on degree of bran removal using New $May-Gr\ddot{u}wald$ reagent dyeing method and taste of cooked rice. The optimum whiteness value of milled rice for efficient milling in Rice Processing Complex was found to be from 40 to 41, while the degree of milling was from $8.9\%\;to\;9.2\%.$ At this whiteness condition, the first derivative of whiteness value according to degree of milling was higher than the average value from brown rice to well milled rice, and the broken kernel ratio was from $3.0\%\;to\;3.4\%.$ This whiteness condition ($40\~41$) could be considered as a milling condition in Rice Processing Complex.

• Fashion & Textile Research Journal
• /
• v.18 no.4
• /
• pp.531-539
• /
• 2016

Charcoal dyed fabrics have been widely used in home textiles and functional clothing due to their anti-statics, antibacterial, deodorization, far infrared emitting and anion releasing. Soybean fiber were regenerated from soybean. Soybean fiber have biodegradable, microbiocidal, non-allergic, and anti-ageing properties. The purpose of this study is to investigate the dyeing characteristics of soybean fabric using charcoal as colorants. Soybean fabrics were dyed with charcoal solution according to concentration of charcoal, dyeing temperature, and dyeing time. To improve washing fastness and investigate mordanting condition, soybean fabric and dyed soybean fabric with charcoal were mordanted by mordanting agents such as $CH_3COOH$(acetic acid), NaCl(sodium chloride) and $AlK(SO_4)_2{\cdot}12H_2O$(Aluminium Potassium Sulfate). Dyeability and color characteristics of charcoal dyed soybean fabric were obtained by computer color matching and SEM morphology analysis. Particle size of charcoal and color fastness were also investigated. The results obtained were as follows; Mean average diameter of charcoal was $1.39{\mu}m$. The dyeability of soybean fabric using charcoal as colorants was increased gradually with increasing concentration of charcoal dyeing solution and saturated at about 8%(o.w.b.). The optimum dyeing temperature and dyeing time were $90{\sim}105^{\circ}C$ and 60~90 minutes respectively. The overall wash fastness at dyeing concentration 2~4%(o.w.b.) and 6~10%(o.w.b.) were 4 degree and 3-4 degree respectively. The fastness to washing according to mordanting method indicated good grade result as more than 4 degree in all conditions. On the other hand, the staining of adjacent fabrics, i.e. PET, Acryl, Wool, Acetate, Nylon and Cotton was found to be of grade 4 or 4-5 in all conditions.

• Journal of Korea Foresty Energy
• /
• v.25 no.2
• /
• pp.22-27
• /
• 2006

K/S values, Hue, Value, and Chroma changes of the hot-water and alkali extract of Boehmeria tricuspis have investigated to obtain an optimum dyeing conditions. Maximum optical absorption of the cotton, Hanji, and silk dyed with the extract were observed at 400 nm. The K/S value of the dyed silk was higher than those of other materials in the treatments with the temperature and time condition and there was not much changes in the treatments near $80\;^{\circ}C$ and 40 minutes. Also, the K/S value of the dyed silk was drastically increased as the concentration of the dye was increased. In the treatments with temperature and time condition, Hue of the materials dyed with alkali extracts resulted in YR color, whereas materials dyed with hot-water extracts provided R color. In the time and temperature condition of treatment, there were no significant changes in the samples treated near $80\;^{\circ}C$ and 40 minutes. The Value and Chroma of the dyed materials were not significantly changed. As a result, it is suggested that the optimum temperature, time, and concentration of dye would be $80\;^{\circ}C$, 40 minutes, and 100%, respectively, when cotton, Hanji, and silk are dyed with Boehmeria tricuspis extract.

• Korean Journal of Human Ecology
• /
• v.18 no.6
• /
• pp.1315-1321
• /
• 2009

The chemical composition of natural powder dye $Pinux^{TM}$ manufactured from Pinus radiata bark and dyeability of dyed silk fabrics with $Pinux^{TM}$ were examined. It is made up of the optimum dyeing condition of silk fabric according to the dyeing concentration, dyeing time, and dyeing temperature. Also, we examined the colorfastness and antibiosis of dyed silk fabrics to washing, rubbing, perspiration and light. For the analysis of the chemical composition of $Pinux^{TM}$, the total contents of phenolic compound, proanthocyanidin(PA) and anti-oxidative activities of the dye were analyzed. As a result, it was found that the main components of the $Pinux^{TM}$ manufactured from Pinus radiata bark is proanthocyanidin, mostly a flavonoid containing a procyanidin structure, and it consists of approximately 63% phenol. As a result of examining the dyeability of silk fabrics with $Pinux^{TM}$, it showed that the dyeability was best under the conditions of the concentration of dye $1{\sim}1.5%$(wt/v%), dyeing time of 90 minutes, and dyeing temperature at $90^{\circ}C$. It was found that the colorfastness of dyed silk fabrics, colorfastness to washing, perspiration for acidic and rubbing were as good as grade 4 or 4-5. However, the colorfastness to light was low at grade 1, the same as the results of other natural dyed fabrics. As a result of the antibiosis measurement for the $Pinux^{TM}$-dyed silk fabrics, it showed high antibacterial properties to Staphylococcus sureus at 99.6%.

• Textile Coloration and Finishing
• /
• v.22 no.3
• /
• pp.194-206
• /
• 2010

This study was carried out to identify the optimum dyeing conditions for maximum dye uptake of Prunus yedoensis Matsumura flower extract on silk fabric and to investigate hue/tone characteristics and fastness properties of the dyed fabrics. As results, the flower extract was found to contain flavonoids by FT-IR and to show yellowish shade by UV-vis spectrum. Silk fabric was optimized for maximum dye uptake to five repetitions of dyeing at $80^{\circ}C$ for 60 min with an extract concentration of 600% owf in terms of both K/S and color differences. Pre-mordanting was more effective to dye uptake than post-mordanting for all of the mordants used. Un-mordanted and pre-mordanted fabric showed YR(Yellow Red) while most of post-mordanted ones did Y(Yellow). Main tones of dyed fabrics were sf(soft) and lt(light) in the case of unmordanting or Al-mordanting whereas they were d(dull) and g(grayish) by post-mordanting with Cu, Cr, and Fe, respectively. The fastness grades to rub and dry cleaning were reasonably good for most dyeing conditions while those to light were poor. Finally dyeing condition for each hue/tone of the dyed silk with the flower extract was optimized considering fastness properties.

• Journal of the Korean Society of Industry Convergence
• /
• v.9 no.2
• /
• pp.111-116
• /
• 2006

This study provides the optimal conditions treating with the coagulation process and the other chemical treatment processes for dyeing wastewater, especially various dyeing complex wastewater. The results are shown as follows: 1. Optimum reaction condition of pH for ferrous sulfate was the range of 9 to 12. And when 3,000ppm(mg/l) of ferrous sulfate was dosed, the maximum $COD_{Mn}$ removal rate was approximately 40%. 2. In case of ferrous chloride and Bittern as coagulants, optimum pH range was 10 to 11. And maximum $COD_{Mn}$ removal rate was approximately 46% to 50% for dose of 2,000ppm(mg/l) to 6,000 ppm. 3. It is confirmed that the activated sludge process following coagulation precipitation method provides better treatment efficiency than the coagulation precipitation method following the activated sludge process. 4. The purpose of this study was to produce CGF (Cyanoguanidineformaldehyde resin) by organic compounds. 5. The complex coagulation agent by this study is the most economical coagulant with Alum(aluminum sulfate) and the removal efficiency is approximately 54% with 1,000ppm(mg/l) of pH range 6 to 7.

• Textile Coloration and Finishing
• /
• v.16 no.2
• /
• pp.8-14
• /
• 2004

The purpose of this study was to investigate dyeing properties and antibacterial activities of cotton and silk fabrics treated with Ginkgo biloba leaf extracted with three kinds of aqueous solvents: distilled water, electrolytic reduction water and electrolytic oxidation water. The optimum dyeing condition of Ginkgo biloba leaf was 120 min at 8$0^{\circ}C$. Electrolytic reduction water had the highest dyeability to both cotton and silk compared with electrolytic oxidation water and distilled water. A color of extract by distilled water and electrolytic oxidation water showed yellowish Yellow Red, extract by electrolytic reduction water showed reddish Yellow Red. Irrespective of kinds of extraction solvents, appropriate acidity of medium was pH 9∼11 and pH 3 for cotton and silk fabrics, respectively. Colorfastness to laundering and Light fastness showed generally low but crocking fastness was excellent. Antibacterial activities of the treated fabrics above were 99.9%.