• Title/Summary/Keyword: Oils coating

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Fabrication of In-needle Microextraction Device Using Nichrome Wire Coated with Poly(ethylene glycol) and Poly(dimethylsiloxane) for Determination of Volatile Compounds in Lavender Oils

  • Lee, Eun Ji;Lee, Dong-Sun
    • Bulletin of the Korean Chemical Society
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    • v.35 no.1
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    • pp.211-217
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    • 2014
  • A new needle-based device for headspace wire coated in-needle microextraction (HS-WC-INME) was fabricated using a nichrome wire coated with poly(ethylene glycol) (PEG) and poly(dimethylsiloxane) (PDMS) mixture. The proposed needle device was applied for the determination of volatile compounds in lavender and lavandin essential oils by gas chromatography. Fundamental parameters such as needle design, conditions of extraction and desorption were optimized along with the validation of the extraction and desorption efficiency. The optimal conditions were 30 min extraction at $50^{\circ}C$ and 2 min desorption at $240^{\circ}C$. The calibration curves showed good linearity with the suitable values of the coefficients of determination ($r^2$) greater than 0.99. The limits of detection for linalyl acetate, ${\beta}$-caryophyllene, linalool and (+)-limonene were 7.15, 9.04, 10.79 and 22.26 ng, respectively. Analytical recoveries were acceptable in the test samples, varying from 86.7% to 108.0%. The values of relative standard deviations for run to run showed range less than 0.9% while 3.9% through 7.2% for needle to needle. The proposed PEG-PDMS coating could be more suitable than PDMS coating to extract particular polar groups such as alcohols.

Quality Stability of the Herb Pill Coated with Edible Oils Containing Rosemary Essential Oil (로즈마리를 첨가만 유지 코팅 생약제 환의 품질안정성)

  • Kwak, Yi-Sung;Choo, Jong-Jae
    • Journal of the Korean Society of Food Culture
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    • v.18 no.2
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    • pp.134-138
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    • 2003
  • Quality stability of the herb pill coated with edible oils containing rosemary was investigated. Herb pills were made of herb powders such as Panax ginseng, Cinnamomum cassia, Lycium chinense, Zyzyphus jujuba and Zingiber officinale. Rapeseed oil and lubriol were used as edible coating oil. After herb pills coated with edible oils with or without rosemary were stored at $40^{\circ}C$ for 180 days, the microbial viable cell counts and peroxide values(POV) of the herb pill were investigated. After 180 day storage, POVs of herb pills with only rapeseed oil or lubriol were 0.51 and 0.49 meq/kg, respectively. However, when rosemary was added in herb pills the POVs were decreased to 0.30 and 0.39 meq/kg, respectively. The addition of rosemary to the rapeseed oil and lubriol tended to decrease the microbial viable cell counts of the herb pill. The microbial viable cell counts of rapeseed oil and lubriol were 940 and 820CFU/g, respectively after 180 days of storage. However, these levels were suppressed to 720 and 640CFU/g by the resemary addition. On the other hand, the ginseng saponin content of herb pills was not affected by the rosemary addition during storage.

Synthesis and Lubrication Properties of Semi-Fluorinated Polyol Esters (불소계 폴리올에스테르의 합성과 윤활 특성)

  • 백진욱;정근우;김영운
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2001.06a
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    • pp.149-155
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    • 2001
  • New semi-fluorinated polyol esters were synthesized by condensation reaction of polyols (NPG and TMP) and carboxylic acids such as 2-ethylhexanoic acid, stearic acid and perfluorooctanoic acid. The structures of polyol esters were confirmed by FT-IR and H-NMR etc. And, the fluorinated polyol esters were insoluble in several oils, however, the semi-fluorinated polyol esters were soluble in several oils depended on the structure of polyol esters. The physical properties such as 4-ball wear property and extreme-pressure (EP) properties were characterized by measuring wear scar diameter through ASTM D2266 and by determining the load-carrying through ASTM D2783 method, respectively. As the results, wear scar diameters of oils in which the semi-fluorinated polyol esters were added were not changed compared to those of not added oils. While extreme-pressure properties remarkably Increased with fluorine contents of the esters depended on the structure of acid moiety and polyol moiety. Also, the extreme-pressure property of semi-fluorinated NPG polyol ester in gasoline engine oil was better than that of commercial Teflon coating additive.

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A Survey on the Use of Deep-fat-fried Foods and Treatment of the Used Oils at Home in Chonbuk Area (전북지역의 가정에서 튀김조리 이용과 사용된 튀김유의 관리실태)

  • 윤계순
    • Korean journal of food and cookery science
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    • v.17 no.6
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    • pp.533-541
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    • 2001
  • This research was carried out to obtain the information about the use of deep-fat-fried foods and treatment of oils used for deep-fat-frying at home. Data were obtained through questionnaires from 442 housewives in Chonbuk area. The frequency of taking deep-fat-fried foods was affected by ages and residential area. Average score for the preference of deep-fat-fried foods was 3.60 in the 5 point scale. Fifty three percent of the respondents prepared deep-fat-fried foods by themselves at home. The oil most commonly used for deep-fat-frying was soybean oil followed by com oil. Proper frying temperature was determined by dropping salt or food coating materials into the oil. Oil color was used as a parameter for determining the life of frying oils by 81.2% of the respondents. Most of the respondents appealed to use oils one more time after filtering. For the disposal of used frying oil, 65.7% of the respondents used some kinds of absorbing papers; 16.1% made soaps and 10.7% discarded into a sink. According to correlation analysis, the frequency of taking deep-fat-fried food had positive relationships with housewives's health status, preference for foods prepared with oil and fats and family's preference for deep-fat-fried foods.

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Water Resistance Evaluation of the Oils Coating for Conservation of Wooden Cultural Heritage (목조문화재 보존을 위한 유지류 코팅제의 방수 성능 평가)

  • Na, Won Ju;Cho, So Yeong;Kim, Do Rae;Chung, Woo Yang
    • Journal of Conservation Science
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    • v.31 no.1
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    • pp.13-20
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    • 2015
  • Surface of the wooden cultural heritage has been protected from moisture by natural oils (such as perilla oil and tung oil), which accelerated degradation. But we can find seldom the research on the processes and performances of oil coatings. In this study, the water resistant performances by wood direction were compared to 3 types of natural oil and 2 types of oil stain, and the effect of additional indoor conditioning and temperature of oil were appraised in longitudinal direction. The natural oils block moisture about 79.2% comparing to the control in longitudinal direction. Especially the tung oil showed the outstanding water resistance about 90.5%. The water resistant performances decreased about 8.8% by additional indoor conditioning for 2 years. Heated oil improved the water resistance about average 5.0%.(Max. 9.6% with linseed oil).

Plant Oils for Improving Thermotolerance of Beauveria bassiana

  • Kim, Jae-Su;Skinner, Margaret;Parker, Bruce L.
    • Journal of Microbiology and Biotechnology
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    • v.20 no.9
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    • pp.1348-1350
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    • 2010
  • Conidia of Beauveria bassiana ARSEF-7060, produced in millet amended with plant oils such as sunflower, corn, or cotton seed oil, were exposed to $45^{\circ}C$ of wet heat for 90 min. Conidia from millet+corn oil medium had the highest thermotolerance [$LT_{50}$ (median survival time): 45.7 min]. The mycotized millet grains were coated with each of the same plant oils as a granular formulation and subjected to $50^{\circ}C$ of dry heat for 8 h. Corn oil coating ($LT_{50}$: 8.68 h) was superior to sunflower and cotton seed oil coatings, suggesting the feasibility of using corn oil to increase conidial thermotolerance.

Consumption of Edible Oil Food Service Institutions in Inchon (인천지역 집단급식소의 식용유 소비실태)

  • Hong, Mi-Ye;Choe, Eun-Ok
    • Journal of the Korean Society of Food Culture
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    • v.13 no.1
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    • pp.27-35
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    • 1998
  • Consumption of edible oil at food service institutions in Inchon was surveyed to provide basic data for continuous education of dietitians. Manufacturing industry was the major food service institution(78.8%) in Inchon followed by schools, hospitals and social welfare service centers. Most dietitians were at the age of twenties and college graduates with professional careers of 1-5 years. Oil was purchased on the basis of its quality within 1-3% of total food costs four times a month. Proper frying temperature was determined by dropping salt or food coating materials into the oil. Soybean oil was the most frequently used and commercial frying mix powder and flour and eggs in water were the most common food coating materials. Fish and commercial frozen foods were the most frequently used materials for frying. Fried foods were stored with covers in a basket and consumed within 30 minutes after cooking. Frying oils were used one more time after filtering and color was the index for determination of re-use.

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Friction Reduction Properties of Evaporation Coated Petroleum and Silicone Oil Lubricants (증발 코팅법으로 증착된 광유와 실리콘 오일 윤활제의 마찰 저감 특성)

  • Yoo, Shin Sung;Kim, Dae Eun
    • Journal of the Korean Society for Precision Engineering
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    • v.30 no.8
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    • pp.864-869
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    • 2013
  • As the size of mechanical components decreases, capillary forces and surface tension become increasingly significant. A major problem in maintaining high reliability of these small components is that of large frictional forces due to capillary action and surface tension. Unlike the situation with macro-scale systems, liquid lubrication cannot be used to reduce friction of micro-scale components because of the excessive capillary and drag forces. In this work, the feasibility of using evaporation to coat a thin film of organic lubricant on a solid surface was investigated with the aim of reducing friction. Petroleum and silicone oils were used as lubricants to coat a silicon substrate. It was found that friction could be significantly reduced and, furthermore, that the effectiveness of this method was strongly dependent on the coating conditions.

Development of Coating Process of Citric Acid Using Vegetable Oil (식물성 유지를 이용한 구연산코팅 공정의 개발)

  • Kim, Bok-Hee;Kim, Dong-Man;Lee, Sang-Hwa;Shin, Hyun-Jae
    • KSBB Journal
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    • v.25 no.2
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    • pp.137-141
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    • 2010
  • Citric acid is a natural preservative and is used to add a sour taste to foods and soft drinks. For the preparation of stable food additives of citric acid, a coating process using vegetable oil was developed. Coating materials used were purified soy bean oil and carnauba wax. The yield of coated citric acid was up to 95% in both cases. The contents of coating materials was 20~33% in the total composition and the coating efficiency was 95.2 ${\pm}$ 0.01%. The surface of coated citric acid was much smoother and more homogeneous than that of original citric acid according to SEM data. The coated citric acid can be used to as a stable food additive and also would be applied to nutraceuticals and cosmetic ingredients.

A Study on the Triglyceride Composition of Sesame Oil by Gas Chromatography (Gas Chromatography에 의(依)한 참깨기름의 Triglyceride 조성(組成)에 관(關)한 연구(硏究))

  • Ko, Young-Su
    • Korean Journal of Food Science and Technology
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    • v.5 no.3
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    • pp.153-156
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    • 1973
  • Five samples of triglyceride compositions of sesame oil and decuticled sesame oil have been determined by a gas chromatographic analysis. A similar distribution pattern of triglycerides was found in these five sesame oils. It was noted that $C_{50},\;C_{52}\;and\;C_{54}$ were the major components in these samples. The results showed that contents of $C_{50},\;C_{52}\;and\;C_{54}$ triglyceride types in five sesame oils were within $3.0{\sim}4.5%,\;23{\sim}28%\;and\;68{\sim}74%,$ respectively.

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