• Title/Summary/Keyword: Oil extraction

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Comparative Analysis of Volatile Flavor Compounds from Zanthoxylum pipperitum A.P. DC

  • Chang, Kyung-Mi;Kim, Gun-Hee
    • Preventive Nutrition and Food Science
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    • v.13 no.1
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    • pp.33-39
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    • 2008
  • The volatile flavor components of Zanthoxylum pipperitum A.P. DC. produced in Korea and China were isolated using a Clevenger-type apparatus by steam distillation extraction, and analyzed by gas chromatography-mass spectrometry (GC/MS). The yields of oils from Korean and Chinese Z. pipperitum A.P. DC. were 2.0 and 1.2% (w/w), respectively. From the two Z. pipperitum A.P. DC. oils, sixty and fifty-four volatile flavor compounds were tentatively identified, and they constituted 94.78 and 87.34% of the total peak area, respectively. Piperitone(p-menth-1-en-3-one) (13.48%) was the most abundant compound in the Chinese Zanthoxylum pipperitum A.P. DC. oil, followed by $\beta$-phellandrene, sabinene, terpinen-4-ol and linalool (each >5%). Whereas, the most abundant compound in the Korean Zanthoxylum pipperitum A.P. DC. oil was limonene (18.04%), followed by geranyl acetate, cryptone, citronellal, cuminal and phellandral (each >5%).

Analysis of Essential Oils from Korean Aromatic Tobacco Varieties by GC/MS and data system. (GC/MS와 data system을 이용한 한국산 향끽미종 잎담배의 정유성분 분석)

  • Park, Jeen-Woo;Lee, Un-Chul;Kim, Yong-Tae;Heu, Il
    • Journal of the Korean Society of Tobacco Science
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    • v.4 no.1
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    • pp.61-66
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    • 1982
  • Essential oil components were isolated from Korean aromatic tobaccos by using a simultaneous distillation and extraction apparatus. The essential oils were analyzed by GC/M S and date system. Forty-two volatile components were identified on the basis of their mass spectra. Determination of contents of essential oil components from Hyangcho and Sohyang was achieved by pseudo-multiple ion selection (Ml S) technique. Varietal differences were detected from the quantitative comparison of the MIS data.

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Treatment of ground waters in a hollow-fibre liquid membrane contactor for removal of ions

  • Hossain, Md. M.
    • Membrane and Water Treatment
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    • v.4 no.2
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    • pp.95-108
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    • 2013
  • Metal ions exist in seawater, groundwater and industrial wastewaters. These source waters can be recycled if their concentrations are reduced. A number of processes can be applied for this purpose. Liquid-liquid extraction is one of the promising methods. In this paper, experimental results are presented on the removal of Cr(VI) using Aliquat-336, a reactive carrier, in sunflower oil (a non-toxic solvent). The performance of this new system is compared with those of kerosene (a toxic solvent). The extent of removal of Cr(VI) from samples with high and low concentrations are presented. The process was upgraded to a bench-scale module that can selectively remove about 50-90% Cr(VI) from samples of groundwater. Thus this process can produce water within the acceptable range for recycling and for use in secondary purposes such as irrigation.

Volatile Oil Composition of Boxthorn (Lycium chinense M.) Leaves

  • Ryu, Su-Noh;Kim, Seong-Min
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.43 no.3
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    • pp.189-193
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    • 1998
  • Volatile components were extracted from leaves of two Boxthorn (Lycium chinense M.) cultivars by using simultaneous distillation and extraction, analyzed by gas chromatography-mass spectrometry. Seventy components were identified : 13 acids, 15 alcohols, 18 hydrocarbons, 13 carbonyls, three esters, three ionones, and five others. The principal volatile components (and their peak area percentage) were n-pentanol (11.2~30.2%), phytol (14.5~28.3%), hexadecanoic acid (13.5~17.1%) 2,3-dihydrobenzofuran (1.5~4.2%), benzyl alcohol (1.9-4.8%), phenylacetaldehyde (1.8~3.2%), and octadecadienoic acid (1.7~10.7%). Fresh leaves showed much higher peak area than that of dried leaf in n-pentanol, n-hexanol, cis-2-penten-l-ol, cis-3-hexen-l-ol, benzyl alcohol, and $\beta$-phenylethyl alcohol, while dried leaves showed much higher content than that of fresh leaves in 9-hydroxytheaspran A, octadecanoic acid and octadecadienic acid.

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전기집진기술의 현황과 장래전망(I)

  • 고명삼;이달우
    • The Proceedings of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.11 no.1
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    • pp.24-33
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    • 1997
  • In this paper, aging of insulating oil in pole transformer has been studied by performing accelerated thermal aging test. Dissolved gases were extracted by air bubbling method. Concentration of dissolved gases were modified by extraction ratio of each gases in insulting oil. Aging of insulting materials were proceeded by thermal degradation and oxidation reaction. Both of the reactions followed zeroth order kinetics. Formation rate equations for hydrocarbons, carbon oxides, and hydrogen were derived. It was conformed by gas analysis and UV-visible spectrophotometric method that iron core and copper coil in pole transformer act as catalyst during the aging process.

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Separation of Chromium(VI) Ion in Industrial Waste Water throunh Liquid Surfactant Membrane (산업폐수중 유화액막에 의한 크롬(VI)의 분리)

  • 초민승;강안수;우인성;이영순
    • Journal of the Korean Society of Safety
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    • v.4 no.1
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    • pp.15-24
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    • 1989
  • The transport of Chromium(Vl) ion from waste water throughl the liquid surfactant membrane containing tri-n-octylamine as a carrier, was analyzed by a slab model and was investigated through experiments. For the experiment of membrane stability, concentrations of surfactant and liquid parafnn oil were analyzed. Extraction euperiments were carried out to observe the effect of system variables, such as stirring speed, concentration of carrier, and NaOH in internal aqueous phase, and concentrations of H$_2$SO$_4$and initial chromium(VI) ion in external aqueous phase at $25^{\circ}C$. It is concluded that the most stable formation of liquid membrane emulsion was obtained when surfactant concentration is above 3 wt. % and liquid parafnn oil concentration is 50 vol. %. The transport of chromium(VI) ion in bacth extractor increased with increasing carrier concentration, the volume ratio of emulsion to external aqueous phases, and initial concentration of chromium(VI) ion under the optimum stirring speed of chromium(VI) ion below 2 ppm. The theoretical equation on the transport of chromium(Vl) ion agreed well with the experimental results.

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Comparison of Immune Activities of Essential Oils from Juniperus rigida S. et Z. and Boswellia carteii Birew by Supercritical Fluid Extraction System (노간주나무와 유향나무의 초임계 공법으로 추출한 정유의 면역 활성 비교)

  • Mun, Hyoung-Chul;Park, Jin-Hong;Kim, Dae-Ho;Yoo, Jae-Eun;Kim, Jung-Hwa;Kim, Chang-Ho;Kim, Jong-Dai;Park, Young-Sik;Lee, Hak-Ju;Lee, Hyeon-Yong
    • Korean Journal of Medicinal Crop Science
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    • v.12 no.3
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    • pp.243-248
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    • 2004
  • Essential oils from Needl Juniperrus seed and trunk (Juniperrus rigida Sieb.) and Olibanum resin (Boswellia carteii Birew) were extracted by a supercritical fluid extraction system (SFE) and immune activity of each essential oils were observed. The immune activities of each essential oil were compared. Essential oil from Olibanum resin enhanced the growth of human immune T cell up to 1.33 times, compared to control group. Each essential oils showed the potent inhibitory effect on the human cancer cell lines, and increased the secretion of cytokines, IL-6 and $TNF-{\alpha}$ from human B cell as well as the growth of human immune cells.

Insecticidal activity of Valeriana fauriei oils extracted by three different methods against Ricania shantungensis (3가지 다른 방법으로 추출된 길초근(Valeriana fauriei) 정유의 갈색날개매미충(Ricania shantungensis)에 대한 살충 효과)

  • Lee, Sang-Ku;Jeon, Sung-Wook;Jeong, In-Hong;Park, Se-Keun;Lee, Sang-Bum;Lee, Hoi-Seon;Park, Bueyong
    • Journal of Applied Biological Chemistry
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    • v.61 no.1
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    • pp.47-50
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    • 2018
  • Ricania shantungensis is a pest causiong problems in many crops. We tested the possibility of controling Ricania shantungensis using essential oil of Valeriana fauriei which were extracted by three different methods (steam distillation, solvent and supercritical extraction). Steam distillation were showed the most high mortality to adult ($1,040{\mu}L/mL$) and nymph ($2,370{\mu}L/mL$) of R. shantungensis. The yield of steam distillation extraction was 0.67%, which was lower than other methods. However, it is determined that steam extraction was showed higher efficiency by considering time and cost. The result of this study showed the possibility of control R. shantungensis by essential oil of V. fauriei.

Quality Improvement of Pyrolysis Oil Fraction of Waste Plastic by Dimethylformamide Extraction (디메틸포름아마이드 추출에 의한 폐플라스틱 열분해유 유분의 품질향상)

  • Kim, Su Jin
    • Applied Chemistry for Engineering
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    • v.30 no.2
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    • pp.155-159
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    • 2019
  • As a part of improving the quality for the fraction of the waste plastics pyrolysis oil (WPPO), the recovery of paraffin components contained in the fraction was investigated by dimethylformamide (DMF) equilibrium extraction. The fraction of a distilling temperature of $120{\sim}350^{\circ}C$ recovered from WPPO by the simple distillation and the aqueous solution of DMF were used as a raw material and solvent, respectively. The concentrations of paraffin components ($C_{12}$, $C_{14}$, $C_{16}$ and $C_{18}$) contained in the raffinate decreased by increasing the mass fraction of water in the solvent at an initial state ($y_{w,0}$), whereas, the concentrations of paraffin components contained in the raffinate increased by increasing the mass ratio of the solvent to the feed at an initial state $(S/F)_0$. The concentrations of $C_{12}$, $C_{14}$, $C_{16}$ and $C_{18}$ paraffin components present in the raffinate recovered at $(S/F)_0=10$ were about 1.37, 2.0, 2.46 and 3.16 times higher than those of the raw materials, respectively. Recovery rates (residue rates present in raffinate) of paraffin components rapidly increased with increasing $y_{w,0}$, and decreasing $(S/F)_0$. The raffinate recovered through this study was expected to be used as a renewable energy.

Effects of Pre-treatments on the Oil Palm EFB Fibers (오일팜 EFB 섬유의 전처리 영향 평가)

  • Kim, Dong-Seop;Sung, Yong Joo;Kim, Chul-Hwan;Kim, Se-Bin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.44 no.6
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    • pp.36-42
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    • 2012
  • The empty fruit bunch fibers(EFB) of oil palm were examined for optimal utilization of the EFB fibers. The EFB fibers were obtained by shredding EFB, followe by removal of fines. The surface properties of the fibers were modified with various pre-treatments, such as hot water extraction, the soaking treatments with NaOH, $ClO_2$ and n-hexane. The changes in the fiber surface were examined with FT-IR method, which showed the changes in chemical compositions such as pectin, lignin, and etc. according to the pre-treatment methods. And the z-directional tensile testing of the fiber mold made of the treated EFB fibers showed the changes in the bonding strength by the pre-treatments. The fiber mold made of EFB fibers treated with $ClO_2$ showed the greater increase in the tensile energy absorption although the NaOH treatment resulted in the severer impact on the EFB fibers.