• Title/Summary/Keyword: Normal Separation

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Enantiomer separation using a covalently immobilized chiral column derived from polysaccharide derivative by reversed phase liquid chromatography (역상 크로마토그래피에서 다당유도체로 공유결합된 키랄 컬럼을 이용한 거울상 이성질체의 광학분리)

  • Huang, Hu;Jin, Jing Yu;Baek, Chae-Sun;Lee, Wonjae
    • Analytical Science and Technology
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    • v.22 no.2
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    • pp.148-151
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    • 2009
  • Enantiomer separation of N-fluorenylmethoxycarbonyl (FMOC) $\alpha$-amino acid was performed on covalently immobilized chiral column (Chiralpak IB) based on polysaccharide derivative as a chiral selector by reversed phase liquid chromatography. The effect of the reversed mobile phase on the chromatographic parameters of the enantioselectivities, resolution factors and retention times using covalently immobilized Chiralpak IB was shown. Also the enantiomer separation of N-FMOC $\alpha$-amino acid in the reversed and normal phase was compared and the results obtained in the former mobile phase were generally lower than those in the latter mobile phase.

Contact analysis in functionally graded layer loaded with circular two punches

  • Muhammed T. Polat;Alper Polat
    • Computers and Concrete
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    • v.33 no.1
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    • pp.13-25
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    • 2024
  • In this study, contact analysis in a functionally graded (FG) layer loaded with two circular punches is solved using the finite element method (FEM). The problem is consisted of a functionally graded layer that resting on an elastic semi-infinite plane and is loaded with two rigid punches of circular geometry. External loads P and Q are transferred to the layer via two rigid punches. The finite element model of the functionally graded layer is created using the ANSYS package program and a 2-dimensional analysis of the problem is analyzed. The contact lengths, obtained as a result of the analysis are compared with the analytical solution in the literature. In the study, the effects of parameters such as distances between punches, loads, inhomogenity parameter on contact zones, initial separation loads and distances, normal stresses, stresses across depth and contact stresses are investigated. As a result, in this study, it can be said that the magnitude of the stresses occurring in the FG layer is less than the homogeneous layer, therefore the life of FG materials will be longer than the homogeneous layer. When the distance between the punches is 2.25, the initial separation distance is 6.98, and when the distance between the punches is 4, the initial separation distance decreases to 6.10. In addition, when the load increased in the second punch, the initial separation load decreased from 55 to 18. The obtained results are presented in the form of graphs and tables.

Selective Concentration of Viable Spermatozoa by Standardized Glass-wool Column and Its Use for IVF (Standardized Glass-wool Column을 이용한 운동성 정자의 선택적 분리 및 이의 체외수정에의 이용)

  • Kim, Sun-Haeng;Ku, Pyung-Sham
    • Clinical and Experimental Reproductive Medicine
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    • v.15 no.2
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    • pp.149-155
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    • 1988
  • To increase fertilization rate in vitro, separation of viable spermatozoa from the seminal plasma and its other components may be a useful procedure. Ejaculates from healthy men, whose semen analysis findings were normal in 19, and abnormal in 10, were filtered using the glass-wool filtration technique to yield a concentrated, viable sperm samples for IVF, and the usefulness and safety of this method were evaluated. The recovery rate of motile sperm in abnormal groups was 46.2% and 54.5% in normal group. The % motility was increased significantly compared with original sample after filtration, and the grade motility was improved, too. The sperm population with normal morphology was also increased significantly in both group. Using transmission electron microscopy, the ultrastructural integrity of acrosomal segment was examined in order to evaluate the potentially hazardous effect of glass-wool filtration to sperm head, however, sperm population with normal ultrastructure was increased compared with that of original ejaculate after separation. The filtered sperm was then processed for IVF, as the fertilizing capacity is the ultimate parameter of the sperm function. In abnormal group, the fertilization rate(41.5 %) and the ET rate per stimulated cycle were much lower than that of mormal group(69.6%). However, the cleavage rate and the number of embryos transfered per ET cycle were comparable with those of nomal group. The results suggest that the glass-wool filtration of sperm, particularly in oligo-asthenozoospsrmia, may be useful and safe method in the preparation of sperm for IVF.

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Flow Separation Control Effects of Blowing Jet on an Airfoil (블로잉 제트에 의한 에어포일에서의 유동박리 제어효과)

  • Lee, Ki-Young;Chung, Heong-Seok;Cho, Dong-Hyun;Sohn, Myong-Hwan
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.35 no.12
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    • pp.1059-1066
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    • 2007
  • An experimental study has been conducted to investigate the flow separation control effects of a blowing jet on an elliptic airfoil at a Reynolds number of 7.84×105 based on the chord length. A blowing jet was obtained by pressing a plenum inside the airfoil and ejecting flow out of a thin jet slot that located in leading edge or trailing edge. The experimental results have shown that the blowing jet had an effect of suppressing the flow separation, resulting in the higher suction pressure distribution and higher normal force. The increase in Cn was more pronounced at higher incidence, whereas the effectiveness of the blowing jet reduced at lower incidences. The leading edge pulsating blowing with 90° was the most effective in controlling the flow separation than other types of blowing jet configuration tested in this research. Moreover, when the pulsating blowing was applied, the stall angle was postponed about 2°-3°. The continuous and pulsating blowing jet is a direct and effective flow separation control for improving the aerodynamic characteristics and performances of airfoil.

Real-time security Monitroing assessment model for cybersecurity vulnera bilities in network separation situations (망분리 네트워크 상황에서 사이버보안 취약점 실시간 보안관제 평가모델)

  • Lee, DongHwi;Kim, Hong-Ki
    • Convergence Security Journal
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    • v.21 no.1
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    • pp.45-53
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    • 2021
  • When the security monitoring system is performed in a separation network, there is little normal anomaly detection in internal networks or high-risk sections. Therefore, after the establishment of the security network, a model is needed to evaluate state-of-the-art cyber threat anomalies for internal network in separation network to complete the optimized security structure. In this study, We evaluate it by generating datasets of cyber vulnerabilities and malicious code arising from general and separation networks, It prepare for the latest cyber vulnerabilities in internal network cyber attacks to analyze threats, and established a cyber security test evaluation system that fits the characteristics. The study designed an evaluation model that can be applied to actual separation network institutions, and constructed a test data set for each situation and applied a real-time security assessment model.

Separation of Functionalized Heterocyclic Compounds by High Performance Liquid Chromatography (II) (고성능 액체 크로마토그래피에 의한 기능성 헤테로 고리 화합물의 분리(II))

  • Cho, Yun Jin;Lee, Young Cheol;Lee, Kwang-PiII;Park, Keung-Shik
    • Analytical Science and Technology
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    • v.11 no.4
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    • pp.292-296
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    • 1998
  • Normal phase or reversed phase liquid chromatographic separation of isoquinoline of heterocyclic compounds and structural isomers of external substituents, $COOCH_3$, CN and $CH_3$ has been carried out by using several different columns and various mobile phases. From this results, the order of elution of heterocyclic compounds appears to depend on the solvent effect with kinds of mobile phases. Retention mechanism of normal phase system for 2-methylindoline, 2-methylindole, benzoxazole and benzothiazole was also studied depending on adsorption strength between solute and stationary phase of column. However, retention factors of reversed phase system were found on hydrophobic interaction with solvophobic effect.

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Numerical Study on Viscous Wakes of Two-Dimensional Screens Normal to the Uniform Stream (균일유동에 수직인 2차원 스크린 후류의 점성유동에 관한 수치적 연구)

  • 강신형;전우평
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.12 no.3
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    • pp.590-598
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    • 1988
  • Viscous flows through a screen normal to an uniform flow are numerically simulated. A .kappa.-.epsilon. model is adopted for evaluation of the Reynolds stresses. The existence of a screen is regarded as extra sources in the momentum equations. The amount of extra sources is related to the resistance coefficient and the refraction coefficient of the screen. Flows are numerically simulated for various resistance coefficients and heights of the screen and Reynolds numbers. The present method has been verified to reasonably simulate viscous wakes and shear layers of the screen, for which the inviscid theory is quite limitted. As the fluids approach the screen, the velocity is reduced and the pressure is raised to satisfy the Bernoulli equation. After passing the screen, the velocity shows its minimum value at the down-stream, but static pressure is slowly recovered. A detached separation-bubble from the screen appears as the resistance coefficient is increased to a certain level. Such results are qualitatively in agreement with limitted experimental data available. The turbulent kinetic energy shows its maximum value at further down stream and decrease thereafter.

Home Environment, Moral Judgement, and Moral Behavior in Childhood (아동의 가정환경과 도덕적 판단능력 및 도덕적 행동과의 관계)

  • Yo, In Sook
    • Korean Journal of Child Studies
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    • v.6 no.1
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    • pp.75-92
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    • 1985
  • The purpose of this study was to investigate the relationship between the psychological/physical home environment, and children's moral judgement and moral behaviors. The subjects for this study were a normal group of 58 children and a delinquent group of 54 children. The normal children were selected from elementary and middle schools in Taegu city, and the delinquent children were from two juvenile prisons in the Taegu area. Children's moral judgement scores were measured by levels of moral judgement as conceptualized by Kohlberg. The major findings of this study were that: 1) There were significant differences between the normal and delinquent groups on democratic conduct, permissive attitude, degree of intimacy between parent and child, and materialism orientation. 2) There were significant differences between the normal and delinquent group on life or death of real parent, living with parents, separation, bereavement or divorce, mother's age, father's educational level, and father's occupational level. 3) There were significant differences between the normal and delinquent group on children's moral judgement scales. 4) Father's educational level was the best index for predicting psychological and physical home environment variables and differences between normal and delinquent children on level of moral judgement.

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Comparative study of flow over a circular disk using RANS turbulence models (원형 디스크 주위 유동에 대한 RANS 유동해석 비교 연구)

  • Ryu, Nam Kyu;Kim, Byoung Jae
    • Journal of the Korean Society of Visualization
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    • v.19 no.1
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    • pp.88-93
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    • 2021
  • For a flow normal to a circular disk, the flow separation occurs from the edge of the disk and the flow recirculation zone exists behind the disk. Many existing studies conducted simulations of flow normal to a circular disk under low Reynolds numbers. Some studies performed LES or DES simulations under high Reynolds numbers. However, comparative study for different RANS models for high Reynolds numbers is very limited. This study presents numerical simulations of a flow normal to a circular disk using Realizable k-ε model and SST k-ω model. The recirculation bubble length and drag coefficient were compared with the experimental data. The SST k-ω model showed the excellent predictions for the recirculation bubble length and drag coefficient.

Double-talk Control using Blind Signal Separation based on Geometric Concept in Acoustic Echo Canceller (음향반향제거기에서 기하학적 개념의 BSS를 이용한 동시통화 제어)

  • Lee, Haeng-Woo
    • The Journal of the Korea institute of electronic communication sciences
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    • v.12 no.3
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    • pp.419-426
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    • 2017
  • This paper describes an acoustic echo canceller with double-talk using BSS(: Blind Signal Separation) based on the geometric concept. The acoustic echo canceller may be deteriorated or diverged during the double-talk period. So we use the blind signal separation to detect the double talking by separating the near-end speech signal from the mixed microphone signal. In the closed reverberation environment, the blind signal separation extracts the near-end signal from unknown signals with the transformation and rotation based on the geometric concept. By this method, the acoustic echo canceller operates irrespective of double-talking. We verified performances of the proposed acoustic echo canceller by computer simulations. The results show that the acoustic echo canceller with this algorithm detects the double-talk periods thoroughly, and operates stably in the normal state without diverging of coefficients after ending the double-talking.