• Journal of Korean Society of Forest Science
• /
• v.60 no.1
• /
• pp.51-57
• /
• 1983

Properties and glue shear strength of each water soluble rues-phenol copolymer adhesive and phenolic resin adhesive were examined as a high temperature curing binder through the manufacture of plywood made of Kapur veneer. The former has different molar ratio and the latter was made from different catalyst method. The results are summarized as follows: 1) Specific gravities of air dried plywood manufactured from each adhesive ranged from 0.67 to 0.82 and their moisture contents met the K.S. standard 2) In dry and wet shear strength, adhesives with 60 percent of non volatile content showed higher values than those with 50 percent except phenolic resin. Urea-phenol copolymer resin with 20 percent of phenol content exhibited the highest, and that with 70 percent the lowest. Filling effect of wood flour on the bonding strength is great in urea-phenol copolymer resin with more than 50 percent of phenol content, especially significant in 50 percent of non volatile content including alkali catalyst phenolic resin. Alkali and acid catalyst methods were the highest among the adhesive manufacture methods. In wet strength, urea resin belongs to the lowest group. 3) In glue shear strength after boiling and drying test, no method for manufacturing phenolic formaldehyde resin adhesive was stronger than alkali and acid catalyst methods. Phenolic resin made from alkali catalyst method needs a wood flour filler to improve the bonding quality. Urea-phenol copolymer resin with 10 percent of phenol content showed the reasonable water resistance.

• Structural Engineering and Mechanics
• /
• v.13 no.1
• /
• pp.91-101
• /
• 2002

During the last several years, research activity on non-tubular bonded joints has concentrated on the effects of normal stress, bending moments and shear. Nevertheless, in certain situations, the structure may be subjected to twisting moments, so that the evaluation of its dynamic behaviour to torsional vibrations becomes of great importance even though evaluations of such loading conditions is entirely lacking in the literature. The aim of this article is to show that torsional natural frequencies of the non-tubular joint can be evaluated by determining the roots of a determinantal equation, derived by taking advantage of some analytical results obtained in a previous paper dealing with the analysis of the state of stress in the adhesive. Numerical results related to clamped-free and clamped-clamped joints complete the article.

• The Journal of Advanced Prosthodontics
• /
• v.9 no.5
• /
• pp.364-370
• /
• 2017

PURPOSE. To explore the influence of different surface conditionings on surface changes and the influence of surface treatments and aging on the bond strengths of composites to non-aged and aged resin nanoceramics. MATERIALS AND METHODS. Rectangular-shaped non-aged and aged (5000 thermocycles) resin nanoceramic specimens (Lava Ultimate) (n=63, each) were divided into 3 groups according to surface treatments (untreated, air abrasion, or silica coating) (n=21). The surface roughness was measured and scanning electron microscopy was used to examine one specimen from each group. Afterwards, the specimens were repaired with a composite resin (Filtek Z550) and half were sent for aging (5000 thermocycles, n=10, each). Shear bond strengths and failure types were evaluated. Roughness and bond strength were investigated by two- and three-way analysis of variance, respectively. The correlation between the roughness and bond strength was investigated by Pearson's correlation test. RESULTS. Surface-treated samples had higher roughness compared with the untreated specimens (P=.000). For the non-aged resin nanoceramic groups, aging was a significant factor for bond strength; for the aged resin nanoceramic groups, surface treatment and aging were significant factors. The failures were mostly adhesive after thermal cycling, except in the non-aged untreated group and the aged air-abraded group, which had mostly mixed failures. Roughness and bond strength were positively correlated (P=.003). CONCLUSION. Surface treatment is not required for the repair of non-aged resin nanoceramic; for the repair of aged resin nanoceramic restorations, air abrasion is recommended.

• The Journal of Korean Academy of Prosthodontics
• /
• v.17 no.1
• /
• pp.23-34
• /
• 1979

In this study, the adhesive strength of three commercial polycarboxylate cements to ten types of dental casting alloys, such as gold, palladium, silver, indium, copper, nickel, chromium, and human enamel and dentine were measured and compared with that of a conventional zinc phosphate cement. The $8.0mm{\times}3.0mm$ cylindrical alloy specimens were made by casting. The enamel specimens were prepared from the labial surface of human upper incisor, and the dentine specimens were prepared from the occulusal surface of the human molar respectively. Sound extracted human teeth, which had been kept in a fresh condition since, extraction, were mounted in a wax box with a cold-curing acrylic resin to expose the flattened area. The mounted teeth were then placed in a Specimen Cutter (Technicut) and were cut down under a water spray, and then the flat area on the all specimens were ground by hand with 400 and 600 grit wet silicone carbide paper. Two such specimens were then cemented together face-to-face with freshly mixed cement, and moderate finger pressure was applied to squeeze the cement to a thin and uniform film. All cemented specimens were then kept in a thermostatic humidor cabinet regulated at $23{\pm}2^{\circ}C.$ and more than 95 per cent relative humidity and tested after 24 hours and 1 week. Link chain was attached to each alloy specimen to reduce the rigidity of the jig assembly, and then all the specimens were mounted in the grips of the Instron Universal Testing Machine, and a tensile load was delivered to the adhering surface at a cross head speed of 0.20 mm/min. The loads to which the specimens were subjected were recorded on a chart moving at 0.50 mm/min. The adhesive strength was determined by measuring the load when the specimen separated from the cement block and by dividing the load by the area. The test was performed in a room at $23{\pm}2^{\circ}C.$ and $50{\pm}10$ per cent relative humidity. A minimum of five specimens were tested each material and those which deviated more than 15 per cent from the mean were discarded and new specimens prepared. From the experiments, the following results were obtained. 1) It was found that the adhesive strength of the polycarboxylate cement to all alloys tested was considerably greater than that of the zinc phosphate cement. 2) The adhesive strength of the polycarboxylate cements was superior to the non precious alloys, such as the copper, indium, nickel and chromium alloys, but it was inferior to the precious gold, silver and palladium alloys. 3) Surface treatment of the alloy was found to be an important factor in achieving adhesion. It appears that a polycarboxylate cement will adhere better to a smooth surface than to a rough one. This contrasts with zinc phosphate cements, where a rough helps mechanical interlocking. 4) The adhesion of the polycarboxylate cement with enamel was found superior to its adhesion with dentine.

• The korean journal of orthodontics
• /
• v.39 no.6
• /
• pp.393-401
• /
• 2009

Objective: The purpose of this study was to compare the shear bond strength (SBS) of brackets and microleakage of a tooth-adhesive-bracket complex bonded with a direct and an indirect bonding technique after thermocycling. Methods: Fifty non-carious human premolars were divided into two equal groups. In the direct bonding group a light-cured adhesive and a primer (Transbond XT) was used. In the indirect-bonding group, a light-cured adhesive (Transbond XT) and chemical-cured primer (Sondhi Rapid Set) were used. After polymerization, the teeth were kept in distilled water for 24 hours and thereafter subjected to thermal cycling (500 cycles). For the microleakage evaluation, 10 teeth from each group were further sealed with nail varnish, stained with 0.5% basic fuchsin for 24 hours, and examined under a stereomicroscope. Fifteen teeth from each group were used for SBS testing with the universal testing machine and adhesive remnant index (ARI) evaluation. Data were analyzed using the Mann-Whitney U test, Chi-square test, and Fisher's exact test. Results: There were no statistical differences on SBS and microleakage between the two bonding techniques. The indirect bonding group had a significantly lower ARI score. Bracket failures were obtained between enamel-resin interfaces. Conclusions: The type of bonding technique did not significantly affect the amount of microleakage and SBS.

• Journal of Korea Technical Association of The Pulp and Paper Industry
• /
• v.39 no.1 s.119
• /
• pp.69-77
• /
• 2007

Carton and corrugated paperboard have excellent convertibility characteristics that could be easily slitted, folded, and inserted to become a certain shape of box or case. This excellent processing characteristics of carton and corrugated paperboard as well as their recyclability will continue to make them possess high portion in packaging markets. However, staple, tape, or adhesive have been used to seal a paperboard packaging box or case. Staples among them have been frequently used in many cases because of their convenience. Staples could enter the inside the box and give wounds to the goods in the box or case. Furthermore additional handling and waste treatment costs in the making and recycling processes would be necessary when staple is used to seal box or case. This study has been carried out to develop non-staple paperboard packaging box & case designs that can be used to make non-staple boxes & cases. It is believed that the non-staple folding paperboard boxes & cases could be more environmental-friendly, beautiful, and economic than staple boxes & cases.

• The korean journal of orthodontics
• /
• v.43 no.2
• /
• pp.96-100
• /
• 2013

Objective: To evaluate the effects of contamination by either blood or a hemostatic agent on the shear bond strength (SBS) of orthodontic buttons. Methods: We used 45 freshly extracted, non-carious, impacted third molars that were divided into 3 groups of 15. Each tooth was etched with 37% phosphoric acid gel for 30 s. Human blood or the blood stopper agent was applied to the tooth surface in groups I and II, respectively. Group III teeth were untreated (controls). Orthodontic buttons were bonded to the teeth using light-curing composite resin. After bonding, the SBS of the button was determined using a Universal testing machine. Any adhesive remaining after debonding was assessed and scored according to the modified adhesive remnant index (ARI). ANOVA with post-hoc Tukey's test was used to determine significant differences in SBS and Fisher's exact test, to determine significant differences in ARI scores among groups. Results: ANOVA indicated a significant difference between groups (p < 0.001). The highest SBS values were measured in group III ($10.73{\pm}0.96$ MPa). The SBS values for teeth in groups I and II were significantly lower than that of group III (p < 0.001). The lowest SBS values were observed in group I teeth ($4.17{\pm}1.11$ MPa) (p < 0.001). Conclusions: Contamination of tooth surfaces with either blood or hemostatic agent significantly decreased the SBS of orthodontic buttons. When the contamination risk is high, it is recommended to use the blood stopper agent when bonding orthodontic buttons on impacted teeth.

• Structural Engineering and Mechanics
• /
• v.74 no.4
• /
• pp.457-470
• /
• 2020

The force resisting ability of a connection has direct implications on the overall response of a timber framed structure to various actions, thereby governing the integrity and safety of such constructions. The behavior of timber framed structures has been studied by many researchers by testing full-scale-connections in timber frames so as to establish consistent design provisions on the same. However, much emphasis in this approach has been unidirectional, that has focused on a particular connection configuration, with no research output stressing on the refinement of the existing connection details in order to optimize their performance. In this regard, addition of adhesive to dowelled timber connections is an economically effective technique that has a potential to improve their performance. Therefore, a comparative study to evaluate the performance of various full-scale timber frame Nailed connections (Bridled Tenon, Cross Halved, Dovetail Halved and Mortise Tenon) supplemented by adhesive with respect to Nailed-Only counterparts under tensile loading has been investigated in this paper. The load-deformation values measured have been used to calculate stiffness, load capacity and ductility in both the connection forms (with and without adhesion) which in turn have been compared to other configurations along with the observed failure modes. The observed load capacity of the tested models has also been compared to the design strengths predicted by National Design Specifications (NDS-2018) for timber construction. Additionally, the experimental behavior was validated by developing non-linear finite element models in ABAQUS. All the results showed incorporation of adhesive to be an efficient and an economical technique in significantly enhancing the performance of various timber nailed connections under tensile action. Thus, this research is novel in a sense that it not only explores the tensile behavior of different nailed joint configurations common in timber construction but also stresses on improvising the same in a logical manner hence making it distinctive in its approach.

• Proceedings of the KWS Conference
• /
• 2010.05a
• /
• pp.74-74
• /
• 2010

모바일 정보통신기기를 중심으로 전자패키지의 초소형화, 고집적화를 위해 플립칩 공법의 적용이 증가되고 있는 추세이다. 플립칩 패키징 접합소재로는 솔더, ICA(Isotropic Conductive Adhesive), ACA(Anisotropic Conductive Adhesive), NCA(Non Conductive Adhesive) 등과 같은 다양한 접합소재가 사용되고 있다. 최근에는 언더필을 사용하는 플립칩 공법보다 미세피치 대응성을 위해 NCP를 이용한 플립칩 공법에 대한 요구가 증가되고 있는데, NCP의 상용화를 위해서는 공정성과 함께 신뢰성 확보가 필요하다. 본 연구에서는 LDI(LCD drive IC) 모듈을 위한 COF(Chip-on-Film) 플립칩 패키징용 NCP 포뮬레이션을 개발하고 이를 적용한 COF 패키지의 신뢰성을 조사하였다. 테스트베드는 면적 $1.2{\times}0.9mm$, 두께 $470{\mu}m$, 접속피치 $25{\mu}m$의 Au범프가 형성된 플리칩 실리콘다이와 접속패드가 Sn으로 finish된 폴리이미드 재질의 flexible 기판을 사용하였다. NCP는 에폭시 레진과 산무수물계 경화제, 이미다졸계 촉매제를 사용하여 다양하게 포뮬레이션을 하였다. DSC(Differential Scanning Calorimeter), TGA(Thermogravimetric Analysis), DEA(Dielectric Analysis) 등의 열분석장비를 이용하여 NCP의 물성과 경화거동을 확인하였으며, 본딩 후에는 보이드를 평가하고 Peel 강도를 측정하였다. 최적의 공정으로 제작된 COF 패키지에 대한 HTS (High Temperature Stress), TC (Thermal Cycling), PCT (Pressure Cooker Test)등의 신뢰성 시험을 수행한 결과 양산 적용 가능 수준의 신뢰성을 갖는 것을 확인할 수 있었다.

• Journal of the Korea institute for structural maintenance and inspection
• /
• v.21 no.4
• /
• pp.21-29
• /
• 2017

The use of post installed anchors with adhesive type has lately been increasing when it is necessary to repair, reinforce, or remodel structures. This method provides flexibility and simplicity for construction of structural members that require adhering or fixing. Meanwhile, strength evaluation of anchors with expansion type among post installed anchors systems has nearly reached setting up stage like design code through continual experimental studies for the last ten years, but analyses or experimental studies on anchor system with adhesive type are not yet sufficient. Accordingly, the designers and builders of korea depend on foreign design codes since there are no exact domestic design code they could credit. In this study, the objectives are investigating the effects on adhesive strength of anchors embedded into plain concrete by shear experiments of anchors with variables such as edge distance, anchor interval, and load direction and supplying basic data for enactment of domestic design code.