• 제목/요약/키워드: Ni-foil

검색결과 61건 처리시간 0.037초

Effect of Surface Treatment on the Formation of NiO Nanomaterials by Thermal Oxidation

  • Hien, Vu Xuan;Heo, Young-Woo
    • Applied Science and Convergence Technology
    • /
    • 제25권6호
    • /
    • pp.149-153
    • /
    • 2016
  • Thermal oxidation has significant potential for use in synthesizing metal-oxide nanostructures from metallic materials. However, this method has limited applicability to the synthesis of multi-morphology NiO from Ni foil. Techniques consisting of mechanical and chemical approaches were used to pre-treat the Ni foil (prior to oxidation) to promote the formation of nanowires and nanoplates on the NiO layer. These morphologies were realized on the Ni foils scratched by sand paper and a knife, respectively, and subsequently heat-treated at $500^{\circ}C$ for 24 h. Small nanowires (diameter: <10 nm) formed on the Ni foil treated by absolute $HNO_3$ and then oxidized at $500^{\circ}C$ for 24 h. The formation of various morphologies (on the pre-treated Ni foil), which differ from that formed in the case of pristine Ni foil after oxidation, may be attributed to the surface melting phenomenon that occurs during the nucleation process.

Fe-Ni 합금 극박재 제조를 위한 전주성형기술 및 극박재 특성 (Electroforming and Properties of Fe-Ni alloy thin foil)

  • 임태홍;이흥렬
    • 한국소성가공학회:학술대회논문집
    • /
    • 한국소성가공학회 2004년도 추계학술대회논문집
    • /
    • pp.188-191
    • /
    • 2004
  • Electroforming is a process that employs technology similar to that used for electroplating but which is used for manufacturing metallic articles, rather than as a means of producing surface coatings. Electroforming provides a cost-effective means of producing alloys and fully dense nanocrystalline metals as foils, sheets and complex shapes. It was able to make Fe-Ni foil with $5{\mu}m$ thickness by electroforming. Electroformed Fe-Ni alloy was nanocrystalline and the yield strength was in the range $2000{\sim}2800\;MPa$. The magnetic permeability at high frequency of electroformed Fe-Ni foil was higher than that of thicker foils.

  • PDF

마그네트론 스퍼터링법을 이용한 Al-Ni Nano-foils의 형성 기구 및 미세구조 특성

  • 유광춘;이원범;조용기;유세훈;김형순
    • 한국표면공학회:학술대회논문집
    • /
    • 한국표면공학회 2013년도 춘계학술대회 논문집
    • /
    • pp.175-175
    • /
    • 2013
  • Al-Ni nano-foil은 상온에서 외부 방전 및 촉발에 따라 급속한 자기 발열 반응이 일어나는 특성을 보이며, 외부 촉발을 통해 상온에서 온도를 높일 수 없는 접합이나 마이크로 수준의 미세 접합이 가능한 접합재료로서 현재 상당한 기대가치를 갖고 있는 재료이다. 코팅기술로서 sputtering법을 이용하여 Al-Ni 다층막의 nano-foil를 제조하여 Al-Ni 혼합 비율 및 Bi-layer 수에 따른 self-propagating reaction에 대해 조사하였다.

  • PDF

소형 전기도금장치를 이용한 베타전지용 Ni-63 밀봉선원 제작 (Manufacturing of Ni-63 Sealed Source for Betavoltaic Battery Using the Small-scale Electroplating Device)

  • 김진주;최상무;손광재;홍진태
    • 방사선산업학회지
    • /
    • 제11권3호
    • /
    • pp.173-179
    • /
    • 2017
  • The small-scale electroplating device was designed and fabricated for Ni-63 sealed source (foil type) with a high specific activity needed for production of betavoltaic battery. The condition of Ni electroplating was optimized by using fabricated electroplating device to establish a Ni-63 electroplating condition on the Ni foil. The results showed that the optimum surface morphology and thickness of Ni deposit was obtained for 1,758 seconds at a current density of $15mA{\cdot}cm^{-2}$ with 0.5% tween 20. Radioisotope Ni-63 electroplating was implemented under established condition. The radioactivity of Ni-63 sealed source was calculated to $28mCi{\cdot}cm^{-2}$, and the thickness of Ni-63 deposit was about $2.4{\mu}m$.

Ni/Ni-aluminide//Ti/Ti-aluminide 구조경사형 층상재료의 균열 전파 거동 (Crack propagation behavior of in-situ structural gradient Ni/Ni-aluminide//Ti/Ti-aluminide laminate materials)

  • 정동석;김진곤;조현
    • 한국결정성장학회지
    • /
    • 제15권6호
    • /
    • pp.269-275
    • /
    • 2005
  • Ni/Ni-aluminide//Ti/Ti-aluminide 경사기능 층상 복합재료를 박막 hot press법을 이용하여 제작하였다. NiAl과 $TiAl_3$ 금속간화합물 층이 자전고온합성반응을 통해 비교적 두껍게 형성되었고, 얇고 연속적인 $Ni_3Al$과 TiAl 층이 고상 확산을 통해 형성되었다. 파괴저항은 하중 방향이 crack arrester인 경우가 금속 층이 균열의 성장을 방해하기 때문에 crack divider 방향인 경우보다 높다. $Ni_3Al$과 NiAl 금속간화합물 층은 각각 벽개파괴와 입계파괴 거동을 보였고, $TiAl_3$층의 파괴 형태는 입내벽개파괴이었다. Ni/Ni-aluminide 층에서 관찰되는 기공과 금속 층과 금속간화합물 층의 미결합 부위가 낮은 파괴저항의 원인으로 판단된다. Acoustic emission (AE) 원파형 해석을 통해 제작된 복합재료의 파괴특성을 고찰하였다.

Measurements of proton beam flux and energy of APEP using foil activation technique

  • Wenlin Li;Qifan Dong;Hantao Jing;Li Ou;Zhixin Tan;Sixuan Zhuang;Qingbiao Wu
    • Nuclear Engineering and Technology
    • /
    • 제56권1호
    • /
    • pp.328-334
    • /
    • 2024
  • The activation method of metallic foils is an important technique to measure the flux and energy of proton beams. In this paper, the method was used to measure the CSNS APEP proton flux at seven nominal proton energies ranging from 10 MeV to 70 MeV for beam spot sizes of the 20 mm × 20 mm and 50 mm × 50 mm. The reactions of natTi(p, x)48V, natNi(p, x)57Ni, natCu(p, x)58Co, and 27Al(p, x)24Na were employed to measure the proton beam flux with a range of 107-109 p/cm2/s. Furthermore, we also proposed a method using the activity ratio with a stacked-foil target to determine the energy spread of a Gaussian-like distribution for different nominal proton energies. The optimal combinations of Al, Cu, Ti, Ni, Mo, Fe, Nb, and In foils were adopted for the proton energies. The measured energy spreads for degraded beams of 30 MeV-70 MeV were found to be smaller than 10.00%.

전주성형한 Fe-Ni 합금 극박재의 나노결정질 조직에 관한 연구 (Nanocrystalline structure of electroformed Fe-Ni alloy thin foil)

  • 임태홍;이흥렬;구승현
    • 한국표면공학회:학술대회논문집
    • /
    • 한국표면공학회 2007년도 춘계학술발표회 초록집
    • /
    • pp.27-28
    • /
    • 2007
  • 전주는 표면코팅을 목적으로 하기보다 금속제품을 제조하기 위해 사용하는, 도금법과 유사한 기술이다. 다양한 조성의 Fe-Ni 합금들을 전주성형하여 극박형상으로 제조하였다. 2원계 Fe-Ni 합금의 결정립 크기는 10 nm 정도였으며 P 첨가에 의해 결정립 크기를 더욱 미세하게 할 수 있다. 전주한 2원계 Fe-Ni 합금들의 비저항은 전형적인 나노결정질 소재의 특성을 나타낸다.

  • PDF

Study of a Betavoltaic Battery Using Electroplated Nickel-63 on Nickel Foil as a Power Source

  • Uhm, Young Rang;Choi, Byoung Gun;Kim, Jong Bum;Jeong, Dong-Hyuk;Son, Kwang Jae
    • Nuclear Engineering and Technology
    • /
    • 제48권3호
    • /
    • pp.773-777
    • /
    • 2016
  • A betavoltaic battery was prepared using radioactive $^{63}Ni$ attached to a three-dimensional single trenched P-N absorber. The optimum thickness of a $^{63}Ni$ layer was determined to be approximately $2{\mu}m$, considering the minimum self-shielding effect of beta particles. Electroplating of radioactive $^{63}Ni$ on a nickel (Ni) foil was carried out at a current density of $20mA/cm^2$. The difference of the short-circuit currents ($I_{sc}$) between the pre- and post-deposition of $^{63}Ni$ (16.65 MBq) on the P-N junction was 5.03 nA, as obtained from the I-V characteristics. An improved design with a sandwich structure was provided for enhancing performance.

피에조 팬 냉각 성능 측정을 위한 실험장치 구축 (Experimental Facility for Measuring the Cooling Performance of a Piezoelectric Fan)

  • 오명훈;박수현;고재익;최민석
    • 한국가시화정보학회지
    • /
    • 제16권3호
    • /
    • pp.52-58
    • /
    • 2018
  • In this study, an experimental facility has been built to measure the cooling performance of a piezoelectric fan. The facility is composed of a heat source made of $50{\mu}m$ Ni-Cr foil, a piezoelectric fan and a rotary fan for cooling the heat source. For two cases where the foil is vertical or horizontal, the surface temperature on the foil has been measured by an IR camera with and without cooling and the cooling performance of both fans has been analyzed. With cooling by both fans, the rotary fan lowers the surface temperature of the foil as a whole, while the piezoelectric fan lowers the surface temperature at the center of the foil locally. It is also found that the cooling effectiveness of the piezoelectric fan is higher on the horizontal foil than on the vertical foil because the natural convection interferes with the jet from the piezoelectric fan.