• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 추계학술대회 논문집
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• pp.89-92
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• 2009

As a class of materials, Ni-base superalloys are among the most difficult metal alloys to forge together with refractory metals and cobalt-base superalloys. The mechanical properties of Ni-base superalloys depend very much on grain size and the strengthening phases, $\gamma$' ($Ni_3$(Al,Ti)-type) and $\gamma$".($Ni_3$Nb-type). Especially, the control of grain size remains as a sole means for the control of mechanical properties. The grain size and distribution changes of the wrought superalloys during hot working and heat treatment are mainly controlled by the recrystallization and grain growth behaviors. In this presentation, prediction technology of grain size through the computer-aided process design, and numerical modeling for predicting the microstructure evolution of Ni-base superalloy during hot working were introduced. Also, some case studies were dealt with actual forming processes of Ni-base superalloys.

• 열처리공학회지
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• 제16권6호
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• pp.341-348
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• 2003

Superalloys which can be devided into three categohes, i.e. Ni-base, Co-base, and Fe-base alloys are widely used for high temperature applications. Since superalloys contain many alloying elements and precipitates, its chemistry and processing parameters need to be carefully designed. In this review, current state-of-the art in the superalloy technologies is described with special attention to the heat-treatment for the control of the microstructures and mechanical properties.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.803-808
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• 2002

A computer-aided alloy-designing technique to develop the insert metal for transient liquid phase (TLP) bonding was applied to high aluminum Ni-base superalloys. The main procedure of a mathematical programming method was to obtain the optimal chemical composition through rationally compromising the plural objective performances of insert metal by a grid-search which involved data estimation from the limited experimental data using interpolation method. The objective function Z which was introduced as an index of bonding performance of insert metal involved the melting point, hardness (strength), formability of brittle phases and void ratio (bonding defects) in bond layer as the evaluating factors. The contour maps of objective function Z were also obtained applying the interpolation method. The compositions of Ni-3.0%Cr-4.0%B-0.5%Ce (for ${\gamma}$/${\gamma}$/${\beta}$ type alloy) and Ni3.5%Cr-3.5%B-3%Ti (for ${\gamma}$/${\gamma}$ type alloy) which optimized the objective function were determined as insert metal. SEM observations revealed that the microstructure in bond layers using the newly developed insert metals indicated quite sound morphologies without forming microconstituents and voids. The creep rupture properties of both joints were much improved compared to a commercial insert metal of MBF-80 (Ni-15.5%Cr-3.7%B), and were fairly comparable to those of base metals.

• Journal of Welding and Joining
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• 제15권4호
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• pp.78-89
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• 1997

This study has evaluated the weld metal solidification cracking behavior of several Ni base superalloys (Incoloy 825, Inconel 718 and Inconel 600). Austenitic stainless steels(304, 310S) were also included for comparison. In addition, a possible mechanism of solidification cracking in the fusion zone was suggested based on the extensive microstructural examinations with SEM, EDAX, TEM, SADP and AEM. The solidification cracking resistance of Ni base superalloys was found to be far inferior to that of austenitic stainless steels. The solidification cracking of Incoloy 825 and Inconel 718 was believel to be closely related with the Laves-austenite (Ti rich in 825 and Nb rich in 718) and MC-austenite eutectic phases formed along the grain boundaries during solidification. Cracking in Inconel 600 was always found along the grain boundaries which were enriched with Ti and P. Further, solidifidcation cracking resistance was dependent not only upon the type of love melting phases but also on the amount of the phases along the solidification grain boundaries.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2000년도 춘계학술발표회 초록집
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• pp.41-42
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• 2000

• 열처리공학회지
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• 제27권4호
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• pp.180-184
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• 2014

In order to make clear relationship between high temperature tensile properties and fine microstructure of rapidly solidified cast-type Ni-base superalloys without heat treatment required for consolidation process, tensile test was carried out by changing strain rate from $5{\times}10^{-5}s^{-1}$ to $2{\times}10^{-2}s^{-1}$ and test temperature from $900^{\circ}C$ to $1050^{\circ}C$ using IN738LC and Rene'80 melt-spinning ribbons by twin roll process which were superior to ribbons by single roll process from the viewpoint of structure homogeneity. The dependence of tensile strength on strain rate and test temperature was studied and strain rate sensitivity, m, were estimated from tensile test results. From this study, it was found that tensile strength was influenced by ${\gamma}^{\prime}$ particle diameter, test temperature and strain rate, and m of ribbons exhibited above 0.3 over $950^{\circ}C$.

• Journal of Welding and Joining
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• 제15권5호
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• pp.46-55
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• 1997

This study has evaluated the liquation cracking behavior in the heat affected zone of several Ni base superalloys (Incoloy 825, Inconel 718 and Inconel 600). 304 and 310S austenitic stainless steels were also included for comparison. In addition, the mechanism of liquation cracking in the HAZ was postulated based on the extensive microstructural examinations with SEM, EDAX and TEM. The liquation cracking resistance of Ni base alloys was found to be far inferior to that of austenitic stainless steels. The liquation cracking of Incoloy 825 and Inconel 718 was believed to be closely related with the Laves-austenite(Ti rich in 825 and Nb rich in 718) and MC-austenitic eutectic phases formed along the grain boundaries by constitutional liquation and incipient melting under rapid welding thermal contraction. Further, liquation cracking resistance of the HAZ was dependent not only upon the type and amount of low melting phases but also on the grain size.

• 한국추진공학회지
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• 제2권1호
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• pp.67-77
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• 1998

Ni/$Ni_3$Al-$Ni_3$Nb(${\gamma}$/${\gamma}$'-${\delta}$), Ni-$Ni_3$Nb(${\gamma}$-${\delta}$) 공정복합재료를 일방향 응고하였으며, 성장속도에 따른 경도변화, 고온에서 미세조직의 안정성을 층상간격의 영향에 대해 연구하였다. 초내열합금 공정복합재료의 층상간격은 ${\lambda}^2$R＝상수라는 관계식에 의하여 성장속도(R)와 함께 변화하였다. 초내열합금 공정복합 재료를 위한 항온열처리의 결과는 이 연구에 이용되었다. 공정복합재료는 고온에서 미세구조의 안정성이 층상간격의 증가 때문에, 경도는 성장속도의 증가 때문에 향상되었다.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2000년도 특별강연 및 춘계학술발표대회 개요집
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• pp.60-63
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• 2000

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2000년도 특별강연 및 추계학술발표대회 개요집
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• pp.204-207
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• 2000