• Title/Summary/Keyword: Nano-silver

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Highly Sensitive Biological Analysis Using Optical Microfluidic Sensor

  • Lee, Sang-Yeop;Chen, Ling-Xin;Choo, Jae-Bum;Lee, Eun-Kyu;Lee, Sang-Hoon
    • Journal of the Optical Society of Korea
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    • v.10 no.3
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    • pp.130-142
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    • 2006
  • Lab-on-a-chip technology is attracting great interest because the miniaturization of reaction systems offers practical advantages over classical bench-top chemical systems. Rapid mixing of the fluids flowing through a microchannel is very important for various applications of microfluidic systems. In addition, highly sensitive on-chip detection techniques are essential for the in situ monitoring of chemical reactions because the detection volume in a channel is extremely small. Recently, a confocal surface enhanced Raman spectroscopic (SERS) technique, for the highly sensitive biological analysis in a microfluidic sensor, has been developed in our research group. Here, a highly precise quantitative measurement can be obtained if continuous flow and homogeneous mixing condition between analytes and silver nano-colloids are maintained. Recently, we also reported a new analytical method of DNA hybridization involving a PDMS microfluidic sensor using fluorescence energy transfer (FRET). This method overcomes many of the drawbacks of microarray chips, such as long hybridization times and inconvenient immobilization procedures. In this paper, our recent applications of the confocal Raman/fluorescence microscopic technology to a highly sensitive lab-on-a-chip detection will be reviewed.

Pinched Flow Fractionation Microchannel to Sort Microring-Containing Immiscible Emulsion Droplets (마이크로 링이 함유된 비혼합성 에멀젼 액적의 분류를 위한 Pinched Flow Fractionation 마이크로 채널)

  • Ye, Woojun;Kim, Hyunggun;Byun, Doyoung
    • Journal of the Korean Society of Visualization
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    • v.15 no.2
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    • pp.41-47
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    • 2017
  • Microring/nanoring structure has high applicability for nano-antenna and biosensor thanks to its superior optical characteristics. Although coiling nanowires manufactured using immiscible emulsion droplets have an advantage in mass production, this process also forms nanowire bundles. In this study, we solved the nanowire bundle problem by size-selective sorting of the emulsion droplets in a pinched flow fractionation microchannel. Utilizing silver nanowires and immiscible emsulsion droplets, we investigated the correlation between the size of ring droplets and bundle droplet. We visualized the sorting process for glass particles and microring-containing emulsion droplets. Droplets were sorted based on their size, and the ratio of bundle droplets in solution decreased. This droplet-sorting strategy has potential to help the printing and coating process for manufacturing of ring structure patterns and developing of functional materials.

A Study for Development of Smart Taekwondo Uniform with Enhanced Functionality for Children (기능성이 향상된 아동용 스마트 태권도복 개발을 위한 연구)

  • Kim, Kyung-A
    • Journal of the Korea Fashion and Costume Design Association
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    • v.11 no.2
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    • pp.169-181
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    • 2009
  • The purpose of this study was to provide basic information for developing a smart taekwondo uniform with enhanced functionality for children by investigating the wearing condition and satisfaction of taekwondo uniform among taekwondo training children. The data were collected from 162 children living in Seoul and Daegu. For data analysis were performed descriptive statistics, ${\chi}2$ -test and t-test using SPSS Ver. 12. The results of the analysis are as follows. The results revealed that respondents wearing the general training uniform during their training period were the most. The dissatisfaction for the general training uniform was a high price, lack of symbolic, lack of functionality in textiles, lack of variety in design and unfittness of size in order. The developed uniform can adjust the length using a zipper type fastener, and can be used in all seasons as the lining is detachable. It also uses nano-silver material, and soil release finish. It enhances the functionality of movement by treating with raglan sleeve and sleeve hem velcro tape, and designs the upper garment in the draping. Safety is improved through attaching GPS, and elastic material is mixed in the neckline for putting on and off easily. Piece of cloth is added inside the closing of the upper garment. Rings are made for fixing the taekwondo uniform belt. Pocket is designed in the lower garment and colors are multiplied.

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Synthesis of Copper Nanoparticle by Multiple Thermal Decomposition and Electroless Ag Plating (복합적 열분해법을 이용한 구리 나노분말의 합성 및 무전해 은도금에 관한 연구)

  • PARK, JEONGSOO;KIM, SANGHO;HAN, JEONGSEB
    • Journal of Hydrogen and New Energy
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    • v.28 no.1
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    • pp.70-76
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    • 2017
  • To synthesize copper nanoparticle a thermal decomposition was adopted. And to solve the problem of surface oxidation of the synthesized copper powder an electroless Ag plating method was used. The size and shape of synthesized Cu nanoparticle were affected by the size of copper oxalate used as a precursor, reaction solvent, reaction temperature and amount of reducing agent. Especially reaction solvent is dominant factor to control shape of Cu nano-particle which can have the shapes of sphere, polygon and rod. In case of glycerol, it produced spherical shape of about 500 nm in size. Poly ethylene produced uniform polygonal shape in about 700 nm and ethylene glycol produced both of polygon and rod having size range between 500 and 1500 nm. The silver coated copper powder showed a high electrical conductivity.

Synthesis of Silver Nano-Particles using Alcohol Reducing Process and Antibacterial Properties of its Ag/PET Master Batch (알코올환원법을 이용한 은나노입자 제조 및 이를 함유한 Ag/PET 마스터배치칩의 항균특성에 관한 연구)

  • Son, Eun-Jong;Hwang, Young-Gu;Shin, Yu-Shik;Jung, Gi-Hoon;Jung, Hae-Rim;Jeong, Sung-Hoon
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2011.03a
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    • pp.56-56
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    • 2011
  • 알코올 환원법(alcohol reducing process)은 화학적 환원제가 필요하지 않은 화학합성법으로 메탄올, 에탄올, 프로판올, 이소프로판올, 부탄올 등 C1-C4의 알코올류, 에틸렌 글라이콜, 디에틸렌 글라이콜, 프로필렌 글라이콜과 같은 글리콜류 등이 용매이자 환원제로써 사용된다. 전형적으로 금속 전구체를 상기의 알코올류나 글리콜류에 용해 또는 분산시킨 후 그 용액을 환류 조건하에서 가열하게 되면 금속 이온과 용매간의 산화, 환원반응에 의하여 금속이온이 금속원자로 환원되며, 환원된 금속 입자들은 핵 행성과 성장 과정을 거쳐서 입자를 형성하게 된다. 본 연구에서는 알코올환원법을 이용하여 나노크기의 은입자제조를 시도하였고, 이를 PET 칩과의 마스터배치 제조을 시도하였으며, 이의 항균성능을 연구 고찰하였다. 30 ~ 80 nm의 은파우더를 제조할 수 있었으며, 우수한 항균성능을 갖는 Ag/PET 마스터배치를 제조할 수 있었다. 이를 활용하여 나노은입자기반의 항균섬유을 제조하여 이를 활용한 기모경편성물 제조의 기초데이타로 활용이 가능하리라고 사료된다.

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The Spinnability of Ag/PET Master Batch containing Silver Nano Particles according to Changing of Intrinsic Viscosity (은나노입자 함유 M/B의 고유점도(IV)변화에 따른 제사성 및 가연성에 관한 연구)

  • Son, Eun-Jong;Kim, Hyun-Sun;Choi, Tae-Soo;Jeong, Sung-Hoon
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2011.03a
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    • pp.54-54
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    • 2011
  • 방사 공정 최적화를 위해 칩(chip)건조를 실시하여 칩의 수분을 모두 제거한 후 실험을 진행하게 된다. 칩은 그 자체가 공정수분율(0.4%) 또는 그 이상의 수분을 함유하고 있으므로 건조하지 않고 방사하면 현저히 가수분해가 일어난다. 가수분해가 일어난다면 PET 분자량도 저하되어 고분자의 성질을 잃게 되어 방사된 섬유의 물리 화학적 성질에 중요한 영향을 받게 된다. 그러므로 가수분해를 방지하기 위하여 칩내 수분을 제거하는 건조 공정을 거치는 것이다. 개발된 나노은입자을 함유한 Ag/PET 마스터배치의 제사성 및 가연성 평가을 위한 파일럿연구를 행했다. 본 연구에서 사용한 은나노 M/B 칩(chip)의 경우 일반적으로 사용하는 PET 칩에 비하여 낮은 고유점도를 가지므로 방사성에 칩의 수분이 더욱 영향을 미칠 것이라 판단되어 건조공정에 특별한 주의을 하여 진행하였다. 마스터배치의 고유점도(IV)값의 변화에 따른 제사성 및 가연성 평가를 관찰하였다. #3 M/B 칩의 제사성이 #1 M/B 칩 대비 공정성이 개선되어 두 품종 모두 비출사가 발생하지 않았으며, M/B 제조시 분산제 유무에 따른 방사공정성의 차이는 없는 것으로 보인다. 따라서 #1 M/B 대비 공정성이 개선된 점은 M/B의 IV개선에 기인하는 것으로 판단되었다.

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Content Analysis of advertised Eco-interior Materials and Products in Domestic Interior Magazines (국내 친환경 실내 마감재 및 제품의 전문잡지 광고지면 내용분석 연구)

  • Lee, Yeun-Sook;Lee, Soo-Jin;Kim, Kyu-Lee;Oh, So-Yeon;Kwon, Hyun-Joo
    • Korean Institute of Interior Design Journal
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    • v.15 no.5 s.58
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    • pp.298-305
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    • 2006
  • The purpose of this study is to figure out the profiles of eco-friendly finishing materials and intoner products through content analysis on the advertisements of three domestic interior design magazines, which have been published for 4 years since 2002. The amount of advertisements has been continuously increasing due to the public concerns on well-being. Finishing material types absolutely took the greatest proportion (92.8%), while products such as furniture and household equipments were only 7.2% among the advertisements. Charcoal, natural jade, yellow soil and nano-silver were the frequently mentioned health-related components in the finishing material. Only 35.7% of the finishing materials hold certification on indoor air quality. Among the interior products, phytonchid in air cleaner was the only advertised component related to health. In conclusion, controlling pollutants of indoor air quality, such as HCHO, VOC, seems to be the big issue in both materials and products due to the concern of Sick Building Syndrome. However, more scientific and objective guidelines are necessary for consumers to live in healthy interior environment.

Copper micro/nanostructures as effective SERS active substrates for pathogen detection

  • Ankamwar, Balaprasad;Sur, Ujjal Kumar
    • Advances in nano research
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    • v.9 no.2
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    • pp.113-122
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    • 2020
  • Surface-Enhanced Raman Scattering (SERS) spectroscopy is a multifaceted surface sensitive methodology which exploits spectroscopy-based analysis for various applications. This technique is based on the massive amplification of Raman signals which were feeble previously in order to use them for appropriate identification at qualitative and quantitative in chemical as well as biological systems. This novel powerful technique can be utilized to identify pathogens such as bacteria and viruses. As far as SERS is concerned, one of the most studied problems has been functionalization of SERS active substrate. Metal colloids and nanostructures or microstructures synthesized using noble metals such as Au, Ag and Cu are considered to be SERS active. Silver and gold are extensively used as SERS active substrates due to chemical inertness and stability in air compare to copper. However, use of Cu as a suitable alternative has been taken into account as it is cheap. Herein, we have synthesized air-stable copper microstructures/nanostructures by chemical, electrochemical and microwave-assisted methods. In this paper, we have also discussed the use of as synthesized copper micro/nanostructures as inexpensive yet effective SERS active substrates for the fast identification of micro-organisms like Staphylococcus aureus and Escherichia coli.

Nanoscale Pyramid Texture for High Efficiency Multi-Crystalline Silicon Solar Cells (고효율 다결정 실리콘 태양전지 제작을 위한 나노크기의 피라미드 텍스쳐 제작)

  • Heo, Jong;Park, Min-Joon;Jee, Hong sub;Kim, Jin Hyeok;Jeong, Chaehwan
    • Current Photovoltaic Research
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    • v.5 no.1
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    • pp.25-27
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    • 2017
  • Nanoscale textured black silicon has attracted intensive attention due to its great potential as applications in multicrystalline silicon-based solar cells. It absorbs sunlight over a broad range of wavelengths but introduces large recombination centers, non-uniform doping into cell. In this study, we present a metal-assisted chemical etching technique plus alkaline etching process to fabricate nanoscale pyramid structures with optimized condition. To make the structures, silver nanoparticles-loaded mc-Si wafer was submerged into $H_2O_2/HF$ solution first for nanohole texturing the wafer and textured wafer etched again with KOH solution for making nanoscale pyramid structures. The average reflectivity (350-1050 nm) is about 8.42% with anti-reflection coating.

Synthesis of Copper Nanoparticles by a Chemical Reduction Method (화학적 환원법에 의한 구리 나노분말 합성)

  • Choi, Min Woo;Bae, Min Hwan;Ahn, Jung-Ho
    • Journal of Powder Materials
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    • v.23 no.3
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    • pp.228-234
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    • 2016
  • Copper nanoparticles attract much attention as substitutes of noble metals such as silver and can help reduce the manufacturing cost of electronic products due to their lower cost and good conductivity. In the present work, the chemical reduction is examined to optimize the synthesis of nano-sized copper particles from copper sulfate. Sodium borohydride and ascorbic acid are used as reducing and antioxidant agents, respectively. Polyethylene glycol (PEG) is used as a size-control and capping agent. An appropriate dose of PEG inhibits the abnormal growth of copper nanoparticles, maintaining chemical stability. The addition of ascorbic acid prevents the oxidation of nanoparticles during synthesis and storage. Transmission electron microscopy (TEM) and Fourier transform infrared spectroscopy (FTIR) are used to investigate the size of the synthesized nanoparticles and the coordination between copper nanoparticles and PEG. For chemical reduction, copper nanoparticles less than 100 nm in size without oxidized layers are successfully obtained by the present method.