• Title/Summary/Keyword: Nano-morphology

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Precipitation Behaviors of Hydroxyapatite on Highly Ordered Nanotubular Ti-35Ta-xNb Alloy Surface

  • Jo, Chae-Ik;Eun, Sang-Won;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2013.05a
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    • pp.81-82
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    • 2013
  • In this study, precipitation behaviors of hydroxyapatite on highly ordered nanotubular Ti-35Ta-xNb alloy surface were researched. Ta and Nb additions to Ti increased corrosion resistance. The surface characteristics of anodized alloy depended on the nanotube formed voltage and alloy element. The HA precipitation morphology was influenced by nanorubular structure of alloys.

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Effects of the Electroplating Duration on the Mechanical Property of the Ni-Co-SiC Composite Coatings

  • Kim, Sung-Min;Lee, Hong-Kee
    • Journal of Surface Science and Engineering
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    • v.43 no.6
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    • pp.255-259
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    • 2010
  • In this work, Ni-Co composites incorporated with nano-sized SiC particles in the range of 45-55 nm are prepared by electroplating. The effects of plating duration on the chemical composition, surface morphology, crystalline structures and hardness have been studied. The maximum hardness of Ni-Co-SiC composite coating is approximately 633 Hv at plating duration of 1 h. The hardness is gradually decreased with increasing plating duration, which can be attributed to the growth of crystalline size and the agglomerates of SiC nano-particles. It is therefore explained that the grain refinement of Ni-Co matrix and stable dispersion of SiC particles play an important role for strengthening, which indicate Hall-Petch relation and Orowan model were dominant for hardening of Ni-Co-SiC composite coatings.

Electromagnetic Interference Reflectivity of Nanostructured Manganese Ferrite Reinforced Polypyrrole Composites

  • Chakraborty, Himel;Chabri, Sumit;Bhowmik, Nandagopal
    • Transactions on Electrical and Electronic Materials
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    • v.14 no.6
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    • pp.295-298
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    • 2013
  • Nano-size manganese ferrite reinforced conductive polypyrrole composites reveal a core-shell structure by in situ polymerization, in the presence of dodecyl benzene sulfonic acid as the surfactant and dopant, and iron chloride as the oxidant. The structure and magnetic properties of manganese ferrite nano-fillers were measured, by using X-ray diffraction and vibrating sample magnetometer. The morphology, microstructure, and conductivity of the composite were characterized by transmission electron microscopy, Fourier transform infrared spectroscopy, and four-wire technique. The microwave-absorbing properties of composites reinforcement dispersed in resin coating with the coating thickness of 1.2 nm were investigated, by using vector network analyzers, in the frequency range of 8~12 GHz. A reflection loss of -8 dB was observed at 10.5 GHz.

Synthesis and Characterization of Cu Nanowires Using Anodic Alumina Template Based Electrochemical Deposition Method (양극산화 알루미나 주형 기반의 전해 증착법을 이용한 구리 나노선의 합성 및 특성 연구)

  • Lee, Young-In;Choa, Yong-Ho
    • Journal of Powder Materials
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    • v.19 no.5
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    • pp.367-372
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    • 2012
  • Single crystalline Cu nanowires with controlled diameters and aspect ratios have been synthesized using electrochemical deposition within confined nanochannels of a porous anodic aluminium oxide(AAO) template. The diameters of nano-sized cylindrical pores in AAO template were adjusted by controlling the anodization conditions. Cu nanowires with diameters of approximately 38, 99, 274 nm were synthesized by the electrodeposition using the AAO templates. The crystal structure, morphology and microstructure of the Cu nanowires were systematically investigated using XRD, FE-SEM, TEM and SAED. Investigation results revealed that the Cu nanowires had the controlled diameter, high aspect ratio and single crystalline nature.

The investigation into Merocyanine Dye J-aggregation of characteristic by STM (STM을 이용한 Merocyanine Dye J-aggregation 특성관찰)

  • Yang, Chang-Heon;Lee, Ji-Yoon;Choi, Won-Suk;Kwon, Young-Soo
    • Proceedings of the KIEE Conference
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    • 2008.05a
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    • pp.165-166
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    • 2008
  • We investigate characteristics of J-aggregation as take advantage of LB technic. In order to confirm the applications possible for the molecular electronic device, the morphological properties of merocyanine dye were investigated by AFM. $\pi$-A curves investigated the surface pressure of the LB film from a liquid to a solid state ranged between 90 and 100 mN/m. We observed aggregation and it's characteristics by using visible reflection spectroscopy. We have observed morphology of merocyanine dye on gold surface by STM. focuses on results obtained in mercocyanide dye of J-aggregation. When LB films of merocyanine dye are mixed with arachidic acid, J-aggregate formation is exhibited. J-aggregate formation has been serving as typical systems in revealing the physical and structural aspects of nano-sized molecular aggregates constructed as muiltilayers.

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The Control of Electrostatic Characteristics in Toner Type Paper-like Display

  • Lee, S.G.;Kwon, S.H.;Cho, W.K.;Song, M.B.;Kim, Y.W.
    • 한국정보디스플레이학회:학술대회논문집
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    • 2006.08a
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    • pp.1158-1161
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    • 2006
  • The toner type paper-like display (PLD) has been developed with two polymer particles having opposite polarity which is composed of polymer, colorant and external additives (nano-sized silica). Nano-sized silica with triboelectric charge was used for the charge control agent (CCA) and influenced on the electrostatic properties of the silica-coated polymer particles. The PLD cell using silica-coated particles (200 seconds) had shown a good white appearance and low driving voltage. The result could be explained in terms of the surface morphology and the cohesiveness depending on the silica coating time.

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Nano $MgB_2$ Powder Synthesis by Spray Pyrolysis Method (분무열분해법에 의한 나노 $MgB_2$ 분말 제조 연구)

  • Ko Jae Woong;Yoo Jai Moo;Kim Young Kuk;Chung Kuk Chae;Yoo Sang lm;Han Bong Soo;Kim Young Jun
    • Progress in Superconductivity and Cryogenics
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    • v.7 no.1
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    • pp.1-4
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    • 2005
  • Nano- sized spherical $MgB_2$ Powders were synthesized by spray Pyrolysis method. The Influence of solution concentration and furnace reaction temperature on morphology and average particle size were investigated. For adequate preparation conditions, it has mostly spherical, solid and narrow particle size distribution. Average particle size$(X_{50})$ distribution was below 100 nm. The critical temperature for the synthesized $MgB_2$ was around 36K.

Nature of Surface and Bulk Defects Induced by Epitaxial Growth in Epitaxial Layer Transfer Wafers

  • Kim, Suk-Goo;Park, Jea-Gun;Paik, Un-Gyu
    • Transactions on Electrical and Electronic Materials
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    • v.5 no.4
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    • pp.143-147
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    • 2004
  • Surface defects and bulk defects on SOI wafers are studied. Two new metrologies have been proposed to characterize surface and bulk defects in epitaxial layer transfer (ELTRAN) wafers. They included the following: i) laser scattering particle counter and coordinated atomic force microscopy (AFM) and Cu-decoration for defect isolation and ii) cross-sectional transmission electron microscope (TEM) foil preparation using focused ion beam (FIB) and TEM investigation for defect morphology observation. The size of defect is 7.29 urn by AFM analysis, the density of defect is 0.36 /cm$^2$ at as-direct surface oxide defect (DSOD), 2.52 /cm$^2$ at ox-DSOD. A hole was formed locally without either the silicon or the buried oxide layer (Square Defect) in surface defect. Most of surface defects in ELTRAN wafers originate from particle on the porous silicon.

Fabrication and Application of Nano-Fibers for Korean Post-Textile Industry (나노섬유의 제조와 응용 및 한국의 차세대 섬유산업)

  • 이재락;박수진;김효중;정효진;지승용;김준현
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2003.10a
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    • pp.3-6
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    • 2003
  • In this work, poly(ethylene oxide) nanofibers were fabricated by electrospinning to prepare nanofibers-reinforced composites. And the PEO powders-impregnated composites were also prepared to compare with physicochemical properties of nanofibers-reinforced composites. Morphology and fiber diameter of PEO nanofibers were determined by SEM observation. Mechanical interfacial properties of the composites were investigated in fracture toughness tests and interlaminar shear strength (ILSS) test. As a result, the fiber diameter decreased in increasing applied voltage. However the optimum condition for the fiber formation was 15 ㎸, resulting from increasing of jet instability at high voltage and the prepared PEO nanofibers were useful in fiber reinforced composites. The PEO-based nanofibers-reinforced composites showed an improvement of fracture toughness factors ($K_{IC} and G_{ IC}$) and ILSS, compared to the composites impregnated with PEO powders. These results were noted that the nanofibers had higher specific surface area and larger aspect ratio than those of the powder, which played an important role in improving the mechanical interfacial properties of the composites.

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Potassium loading effects for nano-porous ACF pre-fronted with phosphoric acid

  • Oh, Won-Chun;Lim, Chang-Sung
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.16 no.3
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    • pp.106-111
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    • 2006
  • The objective of this paper is to compare the surface features of two kinds of nano-porous activated carbon fiber (NPACF) treated with potassium and the variation of their properties by phosphoric acid pre-treatment. X-ray diffraction (XRD) patterns indicate that NPACF containing potassium species show better performance for potassium and potassium salts by pre-treatment with phosphoric acid. In order to present the causes of the differences in surface properties and specific surface area after the samples were treated with phosphoric acid, pore structure and surface morphology are investigated by adsorption analysis and SEM. For the chemical composition microanalysis for potassium loading of the NPACF pre-treated with phosphoric acid, samples were analyzed by EDX. Finally, the type and quality of oxygen groups are determined from the method proposed by Boehm.