• 제목/요약/키워드: Nano-crystal

검색결과 630건 처리시간 0.03초

Synthesis and reactivity over molybdenum carbide crystallites

  • Choi, Jeong-Gil
    • 한국결정성장학회지
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    • 제20권2호
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    • pp.74-79
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    • 2010
  • The synthesis and reactivities of molybdenum carbide crystallites were examined in this study. Especially, the effect of synthesis conditions were scrutinized on the preparation of molybdenum carbide crystallites. In order to perform this purpose, various characterization techniques such as BET surface area and oxygen uptake measurements were employed for the synthesized molybdenum carbide crystallites. First of all, the molybdenum carbide crystallites were synthesized using molybdenum oxide crystallites and methane gas or methane-hydrogen mixture. The experimental results showed that BET surface areas ranged from $7.4m^2/g$ to $31m^2/g$ and oxygen uptake values varied from $8.1{\mu}mol/g$ to $24.3{\mu}mol/g$. The Mo compounds were found to be active for ammonia decomposition reaction. Even though there are some molybdenum carbide crystallites that were exceeded by Pt/$Al_2O_3$ crystallite, the steady state reactivities for other molybdenum carbide crystallites were comparable to or even higher than that determined for the Pt/$Al_2O_3$ crystallite. These results implied that molybdenum carbide crystallites could be one of the promising crystallites that might be substitutes for Pt-like noble metal crystallites in the petroleum processes.

수정진동자를 이용한 메탈 삽입 테프론 다이어프램 압전소자모듈의제조 및 특성 (Fabrication and characteristic of metal insertedteflon diaphragm piezoeletric device module using quartz crystal oscillator)

  • 김경민;박성현;김성우;손원근;신병철
    • 센서학회지
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    • 제19권2호
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    • pp.149-154
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    • 2010
  • Top of the alumina body which is made according to plan has been printed using a screen printer equipment in order to print an electrode pattern. The electrode is connected with the quartz crystal oscillator of the piezoelectricity method which has a piezoelectric characteristic. The pressure contact department has been experimented using three type of the teflon. The teflon is good for pressure delivery vector but it is bad restitution. So we devised the structure which inserts the metal in the teflon. Bottom of the module is connected with the signal processing department which is planned in advance and then has investigated to characteristic. Therefore we have got the best output-voltage and frequency characteristic follows in the pressure.

분자동역학을 이용한 다공성 물질 건조공정 멀티스케일 시뮬레이션(3부: 멀티스케일 시뮬레이션) (Multi-scale simulation of drying process fey porous materials using molecular dynamics (part 3: multi-scale simulation))

  • 백성민;금영탁
    • 한국결정성장학회지
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    • 제15권4호
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    • pp.168-174
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    • 2005
  • 건조공정 중인 다공성 물질의 물성은 재료의 비균질성 즉 전위, 입자, 입계, 균열, 기공과 같은 미시적인 결함 인자들의 영향을 받는다. 따라서 다공성 물질의 건조공정을 전산 시뮬레이션하기 위해서는 연속체 스케일과 원자 스케일해석 그리고 스케일별 해석 한계 극복이 요구된다. 본 연구에서는 분자동역학 시뮬레이션으로 계산한 나노스케일 물성를 연속체 스케일 해석에 연계하는 계층적 멀티스케일 시스템을 구축하고, 다공성 세라믹 애자의 건조공정을 전산 시뮬레이션 하였다. 해석 결과, 온도, 습도, 변형률 그리고 응력 분포를 기존의 결과들과 비교하여 검증하였다.

카본나노튜브가 프린즈 필드 스위칭 액정 셀의 전기 광학적 특성에 미치는 영향 (Effects of carbon nanotubes on electro-optic characteristics of fringe-field switching liquid crystal cell)

  • 최정훈;조은미;김미영;;이승희;배정준;이규;이영희;이희규;이승은
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
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    • pp.435-436
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    • 2008
  • In this paper, the electro-optical characteristics of carbon nano tubes (CNTs) doped liquid crystal (LC), in fringe-field switching cell have been investigated and compared with pure LC. The electro-optical characteristics of CNTs doped LC were found to be improved than that of pure LC. The CNTs doped LC exhibits faster response time and lower driving voltage than that of pure LC.

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Low-threshold Photonic Crystal Lasers from InGaAsP Free-standing Slab Structures

  • Ryu, Han-Youl;Kim, Se-Heom;Kwon, Soon-Hong;Park, Hong-Gyu;Lee, Yong-Hee
    • Journal of the Optical Society of Korea
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    • 제6권3호
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    • pp.59-71
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    • 2002
  • Photonic band gap structures have a high potential for nearly zero-threshold lasers. This paper describes new-types of low-threshold photonic crystal lasers fabricated in InGaAsP slab waveguides free-standing in air. Two-types of photonic crystal lasers are studied. One is a single-cell nano-cavity laser formed in a square array of air holes. This photonic band gap laser operates in the smallest possible whispering gallery mode with a theoretical Q >30000 and exhibits low threshold pump power of 0.8 mW at room temperature. The nther laser does not have any cavity structure and the lasing operation originates from the enhanced optical density of states near photonic band edges. A very low threshold of 35 $\mu$W (incident pump power) is achieved from this laser at 80 K, one of the lowest values ever reported. This low threshold is benefited from low optical losses as well as enhanced material gain at low temperature.

수정진동자를 이용한 Au 표면에서 avidin-biotin 결합 리포좀 막의 형성구조 분석 (Analysis of Avidin-biotinylated Liposome Layers on Au Electrode by Quartz Crystal Analyzer)

  • 송성훈;조홍식;박종원;김광;중촌사;;삼댁순;장상목
    • KSBB Journal
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    • 제15권5호
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    • pp.497-500
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    • 2000
  • Avidin의 금속표변에 대한 강한 결합력과 avidin-biotin의 강한 결합력을 이용하여 금속 표면 위에 라포좀과 같은 유기 분자막의 다층 형성 과정을 수정진동자를 이용하여 분석하였다. 금속 표변위에 적층되는 유기 분자막에 대한 정보를 수 집하고 그 가능성을 검토하여 바이오 센서에서 감도를 향상 시킬 수 있는 새로운 방법을 제시하고자 하였다.

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Preparation of poly(methyl methacrylate)/clay nanocomposites by microwaveassisted in-situ radical polymerization

  • Jeong, Ji-Won;Kim, Dong-Hyun;Jang, Jae-Ho;Lee, Jung-Taek;Yoo, Kyung-Hyeon;Yoon, Seog-Young
    • 한국결정성장학회지
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    • 제29권1호
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    • pp.19-23
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    • 2019
  • The PMMA (polymethyl methacrylate)/clay nanocomposites were synthesized by in situ radical polymerizations with different clay contents (3 and 7 wt%) using microwave heating. The nanostructure, optical, and thermal properties of the synthesized PMMA/clay nanocomposites were measured by XRD, TEM, AFM, UV-vis, and TGA. It was found that the intercalated- or exfoliated structure of PMMA/clay nanocomposites was strongly dependent on the content of clay. Thus, the imposition of microwave-assisted polymerization facilitated a delamination process of layered silicates to achieve exfoliation state of interlayer distance. The PMMA/3 wt% C10A nanocomposite with well-dispersed and exfoliated clay nano-layers showed the good optical transparency similar to pure PMMA in this study. The thermal decomposition rates of the PMMA/clay nanocomposites become to be lower compared to that of the pure PMMA, indicating the intercalated- or exfoliated inorganic silicate has high thermal stability. A possible reason is that the thermally segmental motion of PMMA polymer into inorganic silicate interlayer spacing has increased the thermal stability of the PMMA/clay nanocomposites.

서비스디자인방법론을 통해 분석한 CFRP CNT와 자전거의 적합성에 관한 연구 (A study on the suitability of CFRP CNT and bicycle through service design process)

  • 박성희;송성일;강승민
    • 한국결정성장학회지
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    • 제28권6호
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    • pp.271-276
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    • 2018
  • 서비스 디자인 방법론을 통해 시장의 상황과 사용자가 원하는 니즈를 파악하여 소재 선정에 있어 고려해야 하는 기준을 조사하였고, 이에 따라 자전거 디자인 개발에 있어 CFRP CNT 소재를 선정하였다. 이 소재를 이용하여 자전거 파트 중 프레임 디자인 개발을 진행하였고, 그 이후 시제품 제작 전 진동 감쇄 실험, 인장강도 실험, 강성 실험 결과를 통해 CFRP CNT 소재로 디자인한 자전거 프레임은 강도 및 경량성 등 기능적 측면에서 기존 CNT 소재로 제작된 자전거 프레임보다 향상된 결과를 보여줌으로써 자전거 프레임에 적합하다는 결과를 얻었다.

Hydroxyapatite 소결체의 가소제 첨가에 따른 특성 (Properties of hydroxyapatite sintered body added with plasticizer)

  • 류수착;김재규;김승현
    • 한국결정성장학회지
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    • 제29권4호
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    • pp.167-172
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    • 2019
  • HAp의 성형성과 열처리를 용이하게 하는 유기가소제를 사용하여 첨가량에 따른 강도(MPa)와 경도(Hv), 수축율(%) 및 생물학적 특성 중 항균력을 측정하였다. 가소제의 첨가량이 증가할수록 기계적 특성인 압축강도와 굽힘강도, 경도 등이 증가하였으나 가소제의 첨가량이 7%를 넘을 경우 오히려 기계적 특성이 감소하였다. 이는 허용치 이상의 가소제의 첨가는 성형 시 균열을 발생시키고 이러한 균열은 소결 시 내부에 미세균열 및 산화 시 기공의 발생을 촉진시켜 기계적 특성의 감소를 유발한다. 항균성 측정 결과 가소제 첨가량 에 관계없이 균은 검출되지 않았으며 우수한 항균력을 발휘하였다.

Fabrication of GaN Ring Structure with Broad-band Emission Using MOCVD and Wet Etching Techniques

  • Sim, Young-Chul;Lim, Seung-Hyuk;Cho, Yong-Hoon
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.243.1-243.1
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    • 2016
  • Recently, many groups have attempted to fabricate 3-dimensional (3D) structures of GaN such as pyramids, rods, stripes and annulars. Since quantum structures on non-polar and semi-polar planes of 3D structures have less influence of internal electric filed, multi quantum wells (MQWs) formed on those planes have high quantum efficiency. Especially, pyramidal and annular structures consist of various crystal planes with different emission wavelength, providing a possibillity of phosphor-free white light emtting diodes (WLEDs).[1] However, it still has problem to obtain high color rendering index (CRI) number because of narrow-band emission and poor indium composition caused by the formation of few number of facets during metal-organic chemical vapor deposition growth.[2] If we can fabricate 3D structure having more various facets, we can make broad-band emittied WLEDs and improve CRI number. In this study, we suggest a simple method to fabricate 3D structures having various facet and containing high indium composition by means of a combination of metal-organic chemical vapor deposition and wet chemical etching techniques.

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