• 제목/요약/키워드: Nano-Sized Particles

검색결과 361건 처리시간 0.028초

Influence of Ni Addition on Mechanical and Magnetic Properties of Yttria-Stabilized Tetragonal Zirconia

  • Kondo, H.;Sekino, T.;Choa, Y.H.;Kusunose, T.;Nakayama, T.;Niihara, K.
    • 한국결정성장학회:학술대회논문집
    • /
    • 한국결정성장학회 2000년도 Proceedings of 2000 International Nano Crystals/Ceramics Forum and International Symposium on Intermaterials
    • /
    • pp.243-248
    • /
    • 2000
  • Effect of NiO addition on microstructure, stability of tetragonal phase and mechanical properties was investigated. (Y, Ni)-TZP solid solution was obtained by pressureless sintering. The fracture toughness was increased by solid solution of NiO. Neither reaction phase nor glassy phase was observed at the grain boundaries. From these results, it was determined that solid solution of NiO was destabilized tetragonal phase of Y-TZP. Y-TZP/Ni nanocomposite that contained nano-sized Ni particles was also fabricated by internal reduction method. Some evaluations and discussions were carried out for both (Y, Ni)-TZP solid solution and Y-TZP/Ni nanocomposite.

  • PDF

폴리에스테르 바니시에서 나노 실리카의 분산성 향상과 나노 복합체 에나멜 와이어 개발

  • 김용범;김은진;김선재;황종선;최용성;서영수
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2009년도 추계학술대회 논문집
    • /
    • pp.151-151
    • /
    • 2009
  • A enameled wire may have better corona-resistance when its coating material contains nano-sized inorganic particles. However, industrial applications are still limited because an aggregation between nanofillers may happen during coating processes. In this study we use a novel scheme of surface modification with silane on silica nanoparticles using sonochemical reaction where composition and surface density of silanes can be controlled in order to reduce particle-particle attractive interaction. Functionalized nanoparticles are evenly dispersed in the matrix confirmed by SEM and energy dispersive x-ray analysis. Dielectric strength and thermal resistance of the nanocomposite wires are improved while flexibility of the wire maintains.

  • PDF

단극하전을 이용한 나노입자 응집성장 제어 (Aggregation of Nanoparticles Using a Unipolar Charging Technique)

  • 박형호;김상수;장혁상
    • 대한기계학회논문집B
    • /
    • 제27권1호
    • /
    • pp.46-53
    • /
    • 2003
  • Effects of electric force on the morphology and growth of aggregates were studied experimentally. Nano-sized NaCl particles were supplied to a flame to perform the unipolar charging state. This electric precursor did not modify a temperature profile of the flame. The morphology of aggregates was measured by TEM image processing technique and the light scattering technique. In the unipolar charged state, the fractal dimension of aggregates was smaller than that of' the electrically neutral state. This result was in good agreement with our previous numerical simulations.

플라즈마 아크방전(PAD)법으로 제조된 FeAl 나노분말 특성 (Preparation of FeAl nanopowders by Plasma Arc Discharge Process)

  • 박우영;윤철수;유지훈;오영우;최철진
    • 한국분말재료학회지
    • /
    • 제11권6호
    • /
    • pp.522-527
    • /
    • 2004
  • Nano sized FeAl intermetallic particles were successfully synthesized by plasma arc discharge pro-cess. The synthesized powders shouted core-shell structures with the particle size of 10-20 nm. The core was metallic FeAl and shell was composed of amorphous $AI_{2}O_{3}\;and\;a\;little\;amount\;of\;metallic\;Fe_{3}O_{4}.$ Because of the difference of Fe and Al vapor pressure during synthesis, the Al contents in the nanoparticles depended on the Al contents of master alloy.

Ni-Fe 합금입자 분산 Al2O3 나노복합재료의 미세조직 및 특성 (Microstructure and Properties of Nano-Sized Ni-Fe Alloy Dispersed Al2O3 Composites)

  • 남궁석;정재영;오승탁;이재성;이홍재;정영근
    • 한국분말재료학회지
    • /
    • 제9권3호
    • /
    • pp.161-166
    • /
    • 2002
  • Processing and properties of $Al_2O_3$ composites with Ni-Fe content of 10 and 15 wt% were investigated. Homogeneous powder mixtures of $Al_2O_3$/Ni-Fe alloy were prepared by the solution-chemistry route using $Al_2O_3$, $Ni(NO_3)_2{\cdot}6H_2O$ and $Fe(NO_3)_3{\cdot}9H_2O$ powders. Microstructural observation of composite powder revealed that Ni-Fe alloy particles with a size of 20nm were homogeneously dispersed on $Al_2O_3$ powder surfaces. Hot-pressed composites showed enhanced fracture toughness and magnetic response. The properties are discussed based on the observed microstructural characteristics.

나노 구조 Fe-Co 합금분말의 제조 및 자성특성 (Fabrication and Magnetic Properties of Nanostructured Fe-Co Alloy Powder)

  • 이백희;안봉수;김대건;김영도
    • 한국분말재료학회지
    • /
    • 제9권3호
    • /
    • pp.182-188
    • /
    • 2002
  • Conventional Fe-Co alloys are important soft magnetic materials that have been widely used in industry. Compared to its polycrystalline counterpart, the nanostructured materials have showed superior magnetic properties, such as higher permeability and lower coercivity due to the single domain configuration. However, magnetic properties of nanostructured materials are affected in complicated manner by their microstructure such as grain size, internal strain and crystal structure. Thus, studies on synthesis of nanostructured materials with controlled microstructure are necessary for a significant improvement in magnetic properties. In the present work, starting with two powder mixtures of Fe and Co produced by mechanical alloying (MA) and hydrogen reduction process (HRP), differences in the preparation process and in the resulting microstructural characteristics will be described for the nano-sized Fe-Co alloy particles. Moreover, we discuss the effect of the microstructure such as crystal structure and grain size of Fe-Co alloys on the magnetic properties.

은 용액 처리와 세탁 조건에 따른 면직물의 항균효과 (Antimicrobial Effects of Laundering and Colloidal Silver Treatment on a Cotton Fabric)

  • 정혜원;김미경
    • 한국의류산업학회지
    • /
    • 제7권3호
    • /
    • pp.333-338
    • /
    • 2005
  • We examined the antimicrobial effects of the cotton fabrics which were laundered at different conditions and treated with a colloidal silver solution using Staphylococcus aureus. Colloidal silver solution was made from commercial colloidal silver generator by electrolysis. The fabric which was innoculated and washed with water before drying had no more Staphylococcus aureus, but which was innoculated and dried before washing with detergent solution had lower reduction rate. The fabric washed with oxygen bleach did not have an antimicrobial effect, but rinsed with 0.07% fabric softener showed antimicrobial properties. The fabric rinsed with 0.7ppm colloidal silver solution had better antimicrobial effects. As the treating concentration of silver solution increased, the antimicrobial property of the fabric was increased. The fabric treated with 5% silver solution sustained reflectance and whiteness of untreated fabric. The colloidal silver treated fabric lost antimicrobial property after washing because nano-sized silver particles were located on uneven fiber surface without chemical bonding forces.

Synthesis and Characterization of Hyaluronic Acid-α-Cyclodextrin Conjugate as the Potential Carrier of PEGylated Drugs

  • Sivasubramanian, Maharajan;Park, Jae-Hyung
    • Journal of Pharmaceutical Investigation
    • /
    • 제40권4호
    • /
    • pp.219-223
    • /
    • 2010
  • The hyaluronic acid (HA) conjugate bearing $\alpha$-cyclodextrin ($\alpha$-CD) was synthesized as the potential carrier of poly(ethylene glycol) (PEG)-drug conjugates. The HA conjugate was prepared by the reaction between the carboxylic acid of HA and the primary amine of $\alpha$-CD in the presence of 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide and 1-hydroxybenzotriazole. The chemical structure of the conjugate was confirmed using $^1H$ NMR and FT-IR spectroscopy. The conjugate could form nano-sized particles in the presence of PEG by forming the inclusion complexes between $\alpha$-CD at the backbone of HA, which was demonstrated using electrophoretic light scattering and field emission transmission electron microscopy. It is anticipated that this novel kind of nanoparticles can serve as a useful delivery system for PEGylated drugs.

Mg 결정립의 열적 안정성에 미치는 Zr 첨가의 영향 (Effect of Zr Addition on Thermal Stability of Grains in Mg)

  • 전중환
    • 열처리공학회지
    • /
    • 제23권5호
    • /
    • pp.239-244
    • /
    • 2010
  • Influence of Zr addition on grain stability at elevated temperatures has been investigated for extruded pure Mg and Mg-0.25%Zr alloy. The grain size of pure Mg increases rapidly with increasing annealing temperature when isochronally annealed for 60 min from 573 to 773 K, whereas the grains are stable up to 723 K for the Zr-containing alloy. The activation energies for grain growth ($E_g$) at this temperature range were determined as 75.3 and 105.9 kJ/mole for the pure Mg and Mg-0.25%Zr alloy, respectively. TEM observations on the annealed Mg-Zr samples revealed that higher thermal stability and higher activation energy for grain growth resulting from Zr addition in Mg may well be associated with the restriction of grain growth by nano-sized Zr particles distributed in the microstructure.

저온 플라즈마 공정에서의 나노 미립자 생성 및 성장 (Nanoparticle generation and growth in low temperature plasma process)

  • 김동주;김교선
    • 한국입자에어로졸학회지
    • /
    • 제5권3호
    • /
    • pp.95-109
    • /
    • 2009
  • A low temperature plasma process has been widely used for semiconductor fabrication and can also be applied for the preparation of solar cell, MEMS or NEMS, but they are notorious in the point of particle contamination. The nano-sized particles can be generated in the low temperature plasma process and they can induce several serious defects on the performance and quality of microelectronic devices and also on the cost of final products. For the preparation of high quality thin films of high efficiency by the low temperature plasma process, it is desirable to increase the deposition rate of thin films with reducing the particle contamination in the plasmas. In this paper, we introduced the studies on the generation and growth of nanoparticles in the low temperature plasmas and tried to introduce the recent interesting studies on nanoparticle generation in the plasma reactors.

  • PDF