• 제목/요약/키워드: NIR analysis

검색결과 390건 처리시간 0.032초

CHOOSING AN NIR INSTRUMENT AND A SAMPLE PRESENTATION OPTION PLANT AND SOIL ANALYSIS

  • Batten, Graeme-D;Blakeney, Anthony-B;Susan Ciavarella
    • 한국근적외분광분석학회:학술대회논문집
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    • 한국근적외분광분석학회 2001년도 NIR-2001
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    • pp.1022-1022
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    • 2001
  • To obtain accurate and repeatable analyses using NIR technology it is important to select an NIR instrument and / or its sample presentation attachments which allow the operator to minimize sampling errors without compromising the benefits of NIR analysis -namely rapid, low cost, minimal sample preparation, minimal structural facilities, minimal hazards. For each sample type and consistency there may be different optimal combinations of instrument, sample presentation attachment, and sample preparation. This paper will consider options available to NIR users in the area of plant and soil analysis and evaluate the potential benefits and disadvantages of crop nutrient diagnoses using laboratory based and airborne imaging techniques.

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Comparative Study of NIR-based Prediction Methods for Biomass Weight Loss Profiles

  • Cho, Hyun-Woo;Liu, J. Jay
    • 청정기술
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    • 제18권1호
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    • pp.31-37
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    • 2012
  • 바이오매스가 가진 재생 가능성과 환경적인 장점으로 인해 바이오매스는 바이오에너지와 다른 제품의 주요 원료가 되었다. 바이오매스의 중요 성질을 예측하기 위해 분광학 데이터를 이용하는 연구를 포함한 많은 연구가 수행되었는데 근적외선 분광학은 빠르고 신뢰성 있는 결과를 저비용으로 제공하는 비파괴 방법이기 때문에 널리 사용되었다. 이 연구에서는 서로 다른 여섯가지의 목질계 바이오매스의 근적외선 스펙트럼 데이터를 기반으로 질량 손실 프로파일을 예측하는 다변량 통계기법을 개발하였으며, 상관없는 잡음을 제거하고 근적외선 데이터를 잘 설명하는 파장대역을 선택하기 위해 웨이블릿 분석이 사용되었다. 실제 근적외선 데이터를 가지고 개발된 방법을 예시하였는데 이 때 여러가지 예측모델이 예측 성능을 기준으로 평가되었고 적절한 근적외선 스펙트럼 전처리법의 장점 또한 설명되었다. 웨이블릿으로 압축된 근적외선 스펙트럼을 이용한 부분최소자승법 예측모델이 가장 좋은 성능을 보였으며 개발된 방법은 바이오매스의 빠른 분석에 쉽게 적용될 수 있음 또한 증명되었다.

MLE와 A/O 공정에서의 nirS 와 nirK 를 가진 탈질미생물의 정량적 분포 (Quantitative distribution of denitrifying bacteria with nirS and nirK in MLE and A/O process)

  • 임동석;김윤중;김형건;박승국;정태학
    • 상하수도학회지
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    • 제26권4호
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    • pp.591-598
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    • 2012
  • Denitrification is an important biological mechanism in wastewater treatment process because this process is technically to remove nitrogen from water to air. There have been lots of study about denitrification engineering and molecular biological research about denitrifying bacteria, respectively. However, combination of these researches was unusual and rare. This study is about the correlation between quantity of denitrifying bacteria and denitrification potential, and consists of NUR batch test as analysis method of denitrification potential and quantitative molecular analysis for denitrifying bacteria. Three reactors (A/O, MLE and A/O of nitrogen deficiency) are operated to get activated sludge with various denitrification potential. All samples which were acquired from reactors were measured denitrification potential by NUR test and NUiR test. Also, Real-time PCR was conducted for quantification of denitrifying bacteria composition in activated sludge. The various denitrification potentials were measured in the reactors. The denitrifiaction potential was the highest in MLE process and the reactor of the nitrogen deficiency showed the lowest. Genomic DNA of activated sludge was obtained and consequently, real-time PCRuse the primer sets of nirK and nirS were conducted to quantify genes involving denitrification reductase production. As the result of real-time PCR, nirK gene showed more significant influence on denitrification potential comapred with nirS gene.

근적외선 분광분석을 통한 산무수물경화 에폭시 시스템의 경화 동력학 (Cure Kinetics for the Acid Anhydride-cured Epoxy System Using a Near-infrared Reflection Spectroscopy)

  • 곽근호;박수진;이재락
    • 폴리머
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    • 제24권1호
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    • pp.65-71
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    • 2000
  • 산무수물 경화 에폭시 수지의 잠재 특성 및 경화 동력학을 근적외선 분광분석법을 통해서 논의하였다. 잠재 특성과 경화 거동의 확인은 각기 다른 온도에서 에폭사이드와 수산기의 NIR reflectance를 측정함으로써 행해졌으며 반응 과정에서 4000~7100$cm^{-1}$ / 스펙트럼 범위의 주된 NIR 흡수피크의 기점, 위치 그리고 전이에 대한 포괄적인 분석이 이루어졌다. 반응의 정도는 에폭사이드의 함량과 경화 온도에 의존적인 4530$cm^{-1}$ /의 NIR 흡수 피크로부터 결정하였다.

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NIR 관련 논문 통계 분석에 의한 NIR 원격탐사의 기술 및 활용분야 고찰 (A Study for the Techniques and Applications of NIR Remote Sensing Based on Statical Analyses of NIR-related Papers)

  • 백원경;박숭환;정남기;권수경;진원지;정형섭
    • 대한원격탐사학회지
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    • 제33권5_3호
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    • pp.889-900
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    • 2017
  • 본 연구에서는 NIR(Near-Infrared) 원격탐사 자료를 이용한 연구의 결과인 논문을 분석함으로써 NIR의 기술 및 활용 연구 분야를 체계적으로 정리하고, 이후 NIR 영상을 활용한 연구의 흐름과 방향을 정립하는 데에 목표가 있다. 이를 위하여 최근 5년간의 국내 저널들과 활용 분야 SCI저널, 기술 개발 분야 SCI저널에 대하여 NIR 활용 연구에 관하여 사례조사를 실시하였다. 선별작업 이후 총 281편의 논문에 대하여 분석을 수행하였으며 통계 분석을 위해 분류와 소분류로 구분하여 우세한 연구 추세를 살펴보았다. 그 결과 논문 작성을 수행한 연구자들의 소속은 대학이 약 60% 이상으로 가장 높았다. 적용 분야의 경우 국외에서 육지 50%, 환경 30% 그리고 재해 11%의 분포를 나타냈다. 한편 국내의 경우 육지 55%, 환경 24%, 재해 10%의 분포를 보였다. 육지에 대한 국내 연구 사례는 임업과 농업이 각각 47%, 28%로 가장 높은 비율을 차지했다. 그 외에 국토관리(17%), 지질/자원과 관련하여 나머지 8%를 차지했다. NIR을 활용한 재해 관측은 산사태, 가뭄, 기상재해, 홍수 등에 활용되었다. 여기서 특히 기상재해는 황사에 관한 연구 결과로 국내의 실정이 반영된 것으로 보인다. 하지만 국내의 연구 사례 중 산불 탐지에 관한 결과가 존재하지 않았다. 국내의 실정을 고려해 볼 때에 이에 관한 추가적이고 활발한 연구가 수행될 필요가 있어 보인다. 이 통계적 논문 분석 자료가 향후 우리나라의 NIR 기술 개발과 활용 분야 확장에 도움이 될 기초 자료로 활용될 수 있기를 기대한다.

Effect of Organic Solvent Extractives on Korean Softwoods Classification Using Near-infrared Spectroscopy

  • Yeon, Seungheon;Park, Se-Yeong;Kim, Jong-Hwa;Kim, Jong-Chan;Yang, Sang-Yun;Yeo, Hwanmyeong;Kwon, Ohkyung;Choi, In-Gyu
    • Journal of the Korean Wood Science and Technology
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    • 제47권4호
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    • pp.509-518
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    • 2019
  • This study analyzed the effect of organic solvent extractives on the classification of wood species via near-infrared spectroscopy (NIR). In our previous research, five species of Korean softwood were classified into three groups (i.e., Cryptomeria japonica (cedar)/Chamaecyparis obtuse (cypress), Pinus densiflora (red pine)/Pinus koraiensis (Korean pine), and Larix kaempferi (Larch)) using an NIR-based principal component analysis method. Similar tendencies of extractive distribution were observed among the three groups in that study. Therefore, in this study, we qualitatively analyzed extractives extracted by an organic solvent and analyzed the NIR spectra in terms of the extractives' chemical structure and band assignment to determine their effect in more detail. Cedar/cypress showed a similar NIR spectra patterns by removing the extractives at 1695, 1724, and 2291 nm. D-pinitol, which was detected in cedar, contributed to that wavelength. Red pine/Korean pine showed spectra changes at 1616, 1695, 1681, 1705, 1724, 1731, 1765, 1780, and 2300 nm. Diterpenoids and fatty acid, which have a carboxylic group and an aliphatic double bond, contributed to that wavelength. Larch showed a catechin peak in gas chromatography and mass spectroscopy analysis, but it exhibited very small NIR spectra changes. The aromatic bond in larch seemed to have low sensitivity because of the 1st overtone of the O-H bond of the sawdust cellulose. The three groups sorted via NIR spectroscopy in the previous research showed quite different compositions of extractives, in accordance with the NIR band assignment. Thus, organic solvent extractives are expected to affect the classification of wood species using NIR spectroscopy.

근적외분광분석법을 이용한 인도메타신의 정량분석 (Quantitative Analysis of Indomethacin by the Portable Near-Infrared (NIR) System)

  • 김도형;우영아;김효진
    • 약학회지
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    • 제47권5호
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    • pp.261-265
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    • 2003
  • Near-infrared (NIR) system was used to determine rapidly and simply indomethacin in buffer solution for a dissolution test of tablets and capsules. Indomethacin standards were prepared ranging from 10 to 50 ppm using the mixture of phosphate buffer (pH 7.2) and water (1 : 4). The near-infrared (NIR) transmittance spectra of indomethacin standard solutions were collected by using a quartz cell in 1 mm and 2 mm pathlength. Partial least square regression (PLSR) was explored to develop calibration models over the spectral range 1100∼1700 nm. The model using 1 mm quartz cell was better than that using 2 mm quartz cell. The PLSR models developed gave standard error of prediction (SEP) of 0.858 ppm. In order to validate the developed calibration model, routine analysis was performed using another standard solutions. The NIR routine analysis showed good correlation with actual values. Standard error of prediction (SEP) is 1.414 ppm for 7 indomethacin samples in routine analysis and its error was permeable in the regulation of Korean Pharmacopoeia (VII). These results show the potential use of the real time monitoring for indomethacin during a dissolution test.

Differentiation between Normal and White Striped Turkey Breasts by Visible/Near Infrared Spectroscopy and Multivariate Data Analysis

  • Zaid, Amal;Abu-Khalaf, Nawaf;Mudalal, Samer;Petracci, Massimiliano
    • 한국축산식품학회지
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    • 제40권1호
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    • pp.96-105
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    • 2020
  • The appearance of white striations over breast meat is an emerging and growing problem. The main purpose of this study was to employ the reflectance of visible-near infrared (VIS/NIR) spectroscopy to differentiate between normal and white striped turkey breasts. Accordingly, 34 turkey breast fillets were selected representing a different level of white striping (WS) defects (normal, moderate and severe). The findings of VIS/NIR were analyzed by principal component (PC1) analysis (PCA). It was found that the first PC1 for VIS, NIR and VIS/NIR region explained 98%, 97%, and 96% of the total variation, respectively. PCA showed high performance to differentiate normal meat from abnormal meat (moderate and severe WS). In conclusion, the results of this research showed that VIS/NIR spectroscopy was satisfactory to differentiate normal from severe WS turkey fillets by using several quality traits.

Materials Characterization Using A Novel Simultaneous Near-Infrared/X-ray Diffraction Instrument

  • Yeboah, S.Agyare;Blanton, Thomas;Switalski, Steve;Schuler, Julie;Analytical, Craig Barnes
    • 한국근적외분광분석학회:학술대회논문집
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    • 한국근적외분광분석학회 2001년도 NIR-2001
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    • pp.1288-1288
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    • 2001
  • X-ray powder diffraction (XRD) is utilized for determination of polymorphism in crystalline organic materials. Though convenient to use in a laboratory setting, XRD is not easily adapted to in situ monitoring of synthetic chemical production applications. Near-Infrared spectroscopy (NIR) can be adapted to in situ manufacturing schemes by use of a source/detector probe. Conversely, NIR is unable to conclusively define the existence of polymorphism in crystalline materials. By combining the two techniques, a novel simultaneous NIR/XRD instrument has been developed. During material's analysis, results from XRD allow for defining the polymorphic phase present, and NIR data are collected as a fingerprint for each of the observed polymorphs. These NIR fingerprints will allow for the development of a library, which can be referenced during the use of a NIR probe in manufacturing settings.

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Daum 이미지와 QuickBird 위성영상에 의한 NIR 밴드 추출과 정규화식생지수 (NDVI)에의 적용 (NIR Band Extraction for Daum Image and QuickBird Satellite Imagery and its Application in NDVI)

  • 나상일;박종화
    • 한국농공학회논문집
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    • 제51권4호
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    • pp.37-42
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    • 2009
  • This study extracted Near Infrared (NIR) band using Image Processing Technology (IPT), and calculated Normalized Difference Vegetation Index (NDVI). Aerial photography from Daum portal in combination with high resolution satellite image was employed to improve vegetation sensitivity by extracting NIR band and calculating NDVI with comparison to QuickBird result. The extracted NIR band and NDVI through IPT presented similar distribution pattern. In addition, a regression analysis by land cover character showed high correlation paddy and forest Therefore, this approach could be acceptable to acquire vegetation environment information.