• Title/Summary/Keyword: ND5

Search Result 4,313, Processing Time 0.032 seconds

Exchange Coupling in Massively Produced Nd2Fe14B+Fe3B Nanocomposite Powders

  • Yang, Choong Jin;Park, Eon Byung;Han, Jong Soo;Kim, Eung Chan
    • Journal of Magnetics
    • /
    • v.9 no.2
    • /
    • pp.27-33
    • /
    • 2004
  • Magnetic properties of $Nd_4Fe_{77.5}B_{18.5}$ compound in term of exchange coupling between $Nd_2Fe_{14}B$ and $Fe_3B$ magnetic nano crystals in melt spun powders were characterized by varying the quenching speed in mass production line. The exchange coupled phenomenon was characterized as functions of nano crystal size and volume fraction of each magnetic phase which was possible by employing Henkel plot (${\delta}M$) and refined Mossbauer spectroscopy. The optimized magnetic properties obtained from the present volume production line were: $B_r= 11.73 kG,{_i}H_c/ = 3.082 kOe$, and $(BH)_{max} = 12.28 MGOe.$ The volume fraction of each magnetic phase for those conditions giving the grain size of 10 nm were ${\alpha}-Fe; 4.2%, Fe_3B; 60.1 %$, and $Nd_2Fe_{14}B; 35.7%$. The superior magnetic properties in the $Nd_2Fe_{14}Fe_3B$ based nanocomposites were confirmed to be dependant on the volume fraction of $Fe_3B$.

Coercivity of Hot-pressed Compacts of Nd-Fe-B-type HDDR-treated Powder

  • Abdul Matin, Md.;Kwon, Hae-Woong;Lee, Jung-Goo;Yu, Ji-Hun
    • Journal of Magnetics
    • /
    • v.19 no.2
    • /
    • pp.106-110
    • /
    • 2014
  • $Nd_{12.5}Fe_{80.6}B_{6.4}Ga_{0.3}Nb_{0.2}$ HDDR-treated powder was compacted by hot-pressing using different configurations of dies and heating rates. The die configurations were especially different in terms of the evacuation system that was used in heating for hot-pressing. The coercivity in the compacts was influenced by the evacuation system of the die and heating rate. In spite of the identical hot-pressing temperature and heating rate, coercivity was radically reduced above $600^{\circ}C$ in the compacts prepared in the closed-type die compared to that in the compacts prepared in the open-type die. The coercivity in the compacts prepared in the closed-type die decreased with increasing heating rate and the value further increased when extreme high heating rate was employed. $Nd_{12.5}Fe_{80.6}B_{6.4}Ga_{0.3}Nb_{0.2}$ HDDR-treated powder contained a significant amount of residual hydrogen (approx. 1500 ppm) in the form of $Nd_2Fe_{14}BH_x$ hydride. The dramatic coercivity decrease in the compact prepared in the closed die is attributed to the disproportionation of $Nd_2Fe_{14}BH_x$ hydride. High coercivity is mainly due to the effective desorption of hydrogen or the suppression of hydrogen-related disproportionation upon hot-pressing.

Effect of Magnetic properties and Microstructure of Hydrogenation stage in HDDR process (HDDR 반응시 수소화 반응이 Nd-Fe-B계 분말의 미세조직과 자기적 특성에 미치는 영향)

  • Lee, S.H.;Yu, J.H.;Kim, Y.D.
    • Journal of Powder Materials
    • /
    • v.18 no.5
    • /
    • pp.443-448
    • /
    • 2011
  • The HDDR(hydrogenation-disproportionation-desorption-recombination) process can be used as an effective way of converting no coercivity Nd-Fe-B material, with a coarse $Nd_2Fe_{14}B$ grain structure to a highly coercive one with a fine grain. Careful control of the HDDR process can lead to an anisotropic $Nd_2Fe_{14}B$ without any post aligning process. In this study, the effect of hydrogen gas input at various temperature in range of $200{\sim}500^{\circ}C$ of hydrogenation stage (named Modified-solid HDDR, MS-HDDR) on the magnetic properties has been investigated. The powder from the modified-solid HDDR process exhibits Br of 11.7 kG and iHc of 10.7 kOe, which are superior to those of the powder prepared using the normal HDDR process.

Genetic Differentiation among the Mitochondrial ND2 Gene and $tRNA^{Trp}$ Gene Sequences of Genus Rana (Anura) in Korea

  • Lee, Hyuk;Yang, Suh-Yung;Lee, Hei-Yung
    • Animal cells and systems
    • /
    • v.4 no.1
    • /
    • pp.31-37
    • /
    • 2000
  • The genetic variations among six species of Rana from Korea (R. nigro-maculata, R. piancyi, R. dybowskii, R. sp, R. rugosa type A, B and R. amurensis) were investigated using 499 bases of mitochondrial DNA sequences for ND2 (NADH dehydrogenase subunit 2) gene and $tRNA^{Trp}$ gene. Partial sequences of ND2 gene (427 bp) and full sequences of $tRNA^{Trp}$ gene (73 bp) were identified. The level of sequence divergences ranged from 0.2 to 5.2% within species and 4.9-28.0% among 6 species of the genus Rana. The $tRNA^{Trp}$ gene of the genus Rana was composed of 77 nucleotides which showed a two dimensional "cloverleaf" structure. The secondary structure of $tRNA^{Trp}$ was not found compensatory changes which could potentially confound phylogenetic inference. In the neighborjoining tree, brown frogs were clustered first with the level of sequence divergence of 13.20% between R. amurensis and R. dybowskii, and 9% between R. dybowskii and R. sp. supported by 99% bootstrap iterations, respectively. R. nigromaculata and R. plancyi were clustered into another group with 5.1% divergence supported by 100% bootstrap iteration. R. rugosa A 8nd B types were grouped by 4.9% divergence and clustered into the last group with other two groups with 100% bootstrap iterations.

  • PDF

Effects of Nd Addition to Sr Ferrite Bonded Magnet (Sr 페라이트 본드자석의 Nd 첨가효과)

  • 정왕일;진성빈;강재덕;신용진
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1997.11a
    • /
    • pp.120-123
    • /
    • 1997
  • In this paper, we deal with the effect on magnetic properties when Nd is added to Sr ferrite bonded magnet. First, we choose SrO$_{n}$.Fe$_2$O$_3$(n=5.9), which is nonstoichiomatric composition, as specimen ferrite. Then, we add 5wt% polyvinyl alcohol and calcinate at 12$25^{\circ}C$ under $N_2$ environment for carbon coating on chemical compound specimen. After that we obtain 1.2${\mu}{\textrm}{m}$ single domain powder through grinding process for 18 hours. The single domain Sr ferrite Powder is well mixed with silage coupling and calcium stearate of 1wt% Then, it is kneaded by using polyamide12 as a binder and is pelleted. After adding Nd-Fe-B powder to the pelleted specimen, we injection-mould it under magnetic field by using anisotropic mould. Especially, when we add l3wt% Nd-Fe-B powder to the polyamide12, we obtain excellent magnetic propertiecs which are $_{B}$H$_{C}$=2.65KOe, Br=3.16KG and (BH)$_{max}$=2.61MGOeOeOeOeOe

  • PDF

A Longitudinal Study on Energy, Protein, Lipid and Lactose Intakes of Breast-fed Infants of Lacto-ovo-vegetarian (채식 수유부의 수유기간별 영야의 에너지, 단백질, 지질, 락토오스 섭취량에 관한 연구)

  • 최경순
    • Journal of Nutrition and Health
    • /
    • v.30 no.5
    • /
    • pp.512-519
    • /
    • 1997
  • To investigate the energy, protein, lipid, and lactose intakes of breast-fed infants of lacto-ove-vegetarians, 25 infants(13 boys, 10 girls) were examined on the 0.5th, 1st, 2nd, and 3nd months of lactation. The amount of breast milk intake was determined by a test-weighing method, and the energy content of protein, lipid, and lactose was calculated using the Atwater factor. Thedaily energy intake for boys averaged 316, 436, 447, and 431kcal and that of girls averaged 284, 399, 401, and 390kcal during lactation, respectively. Average energy intake of boys from milk from 2nd week to the 3rd month postpartum was significantly higher than that of girls(p<0.05), because milk intake volume of boys was much higher than that of girls. The protein intake of boys on 2nd week-3rd month averaged 7.33g/day and that of girls averaged 6.29g/day. The lipid intake of 2nd week, months averaged 21.8g/day and that of girls averaged 20.1g/day. The lactose intake of boys averaged 45.48g/day, while that of girls averaged 41.09g/day. The mean intake of protein and lactose in boys was significantly higher than that of girls.

  • PDF

Magnetic Microstructures and Corrosion Behaviors of Nd-Fe-B-Ti-C Alloy by Ga Doping

  • Wu, Qiong;Zhang, Pengyue;Ge, Hongliang;Yan, Aru;Li, Dongyun
    • Journal of Magnetics
    • /
    • v.18 no.3
    • /
    • pp.240-244
    • /
    • 2013
  • The influences of Gallium doping on the magnetic microstructures and corrosion behaviors of Nd-Fe-B-Ti-C alloys are investigated. The cooling rate for obtaining fully amorphous structure is raised, and the glassforming ability is improved by the Ga addition. The High Resolution Transmission Electron Microscopy image shows that the ${\alpha}$-Fe and $Fe_3B$ soft magnetic phases become granular surrounded by the $Nd_2Fe_{14}B$ hard magnetic phase. The rms and $({\Delta}{\varphi})_{rms}$ value of Nd-Fe-B-Ti-C nanocomposite alloy thick ribbons in the typical topographic and magnetic force images detected by Magnetic Force Microscopy(MFM) decreases with 0.5 at% Ga addition. The corrosion resistances of $Nd_9Fe_{73}B_{12.6}C_{1.4}Ti_{4-x}Ga_x$ (x = 0, 0.5, 1) alloys are enhanced by the Ga addition. It can be attributed to the formation of more amorphous phases in the Ga doped samples.

Histologic changes of pulpal tissue after laser-aided ceramic bracket debonding (레이저를 이용한 도재 브라켓 제거 술식 후 치수의 조직학적 변화)

  • Kim, Yu-Jeong;Lim, Sung-Hoon;Yoon, Young-Joo;Park, Joo-Cheol;Kim, Kwang-Won
    • The korean journal of orthodontics
    • /
    • v.34 no.4 s.105
    • /
    • pp.343-349
    • /
    • 2004
  • Laser-aided debonding has advantages in that the heat produced is localized and controlled, the debonding tool is not heated, and it can be used for the removal of various types of ceramic brackets, regardless of their design. However, the range of safe power usage for laser-aided debonding has not vet been confirmed. The Purpose of this study was to evaluate the histologic changes of pulpal tissue in a rabbit's incisor after Nd-YAG laser-aided ceramic bracket debonding at different levels of power. The result were as follows: 1. At 3-5W Nd-YAG laser power level and 3 seconds of exposure time, the ceramic bracket debonding procedure was not easy. At 5W of power a tie-wing fracture occurred on one bracket during debonding using Weingart plier. The histologic section of pulp represented no adverse changes. 2. At 7-13 W power level and less than 5 seconds of exposure time, the debracketing procedure was done easily and bracket facture did not occur. The histologic section of pulp represented mild and reversible changes. All the results were reversible and no pulpal degeneration or necrosis occurred. Considering the results, it appears that the laser-aided debonding technique is a safe method that does not result in irreversible pulpal changes, softens bracket bonding resin within a saie range of power and exposure time, and is useful for ceramic bracket recycling by lowering the tie- wing fracture rate.

Monitoring of Biogenic Amines Content in Commercial Fermented Alcoholic Beverages in Gangwon-do and Risk Assessment (강원도 유통 발효주 중 바이오제닉 아민류 함량 조사 및 위해도 평가)

  • Bae, Cheol-Min;Shin, In-Cheol;Lee, Woan;Lee, Heok-Hwa;Choi, Yeo-Eun;Kim, Young-Ju;Lee, Ga-Hee;Jeong, Kyung-Jin;Choi, Seung-Bong
    • Journal of Environmental Health Sciences
    • /
    • v.46 no.3
    • /
    • pp.324-334
    • /
    • 2020
  • Objectives: This study was conducted to estimate the related health risk by investigating the content of biogenic amines (BAs) in commercial fermented alcoholic beverages. Methods: Ninety-seven samples, including takjus (34), fruit wines (26), distilled liquors (20) and beers (17) were purchased in Gangwon-do (Province) in 2019. The eight BAs (putrescine, cadaverine, spermine, spermidine, tyramine, β-phenylethylamine, histamine, and tryptamine) were analyzed by high performance liquid chromatograph (HPLC) after extraction (0.4 M HClO4), pigment removal (carbon cartridge) and derivatization (1% dansylchloride). The health risk of exposure to BAs due to ingestion of commercial fermented alcoholic beverages was estimated as the margin of exposure (MOE). Results: Various BAs were detected in takju, fruit wine, distilled liquor and beer. Putrescine (not detected (ND)-12.60 mg/L), cadaverine (ND-5.45 mg/L), tyramine (ND-8.34 mg/L), β-phenylethylamine (ND-13.73 mg/L), histamine (ND-7.96 mg/L), and tryptamine (ND-19.00 mg/L) were found in takju. Putrescine (ND-15.34 mg/L), cadaverine (ND-7.90 mg/L), β-phenylethylamine (ND-3.06 mg/L), histamine (ND-9.68 mg/L), and tryptamine (ND-14.06 mg/L) were identified in fruit wine. Putrescine (less than limit of detection (

Nd-Sr Isotope and Gas Composition for the Sangdong Granites Related to the Tungsten-Molybdenum Ore Mineralization (상동 중석-몰리브덴 광상의 광화관련 상동화강암의 Nd-Sr 동위원소비 및 가스 성분)

  • Kim, Kyu Han;Shin, Yu Hee
    • Economic and Environmental Geology
    • /
    • v.28 no.2
    • /
    • pp.139-145
    • /
    • 1995
  • Tungsten skarn mineralization of the Sangdong mine is localized in the interbedded limestone layers of the Myobong Slate Formation and in the limestone of the Pungchon Limestone Formation of Cambrian age. Fluid inclusion, gas composition and Nd-Sr isotope for granites and skarns have been investigated. Gas compositions show $CO_2$ rich in the Sangdong granite and CH, rich in the Nonggeori and Eopyeong granites. The initial $^{87}Sr/^{86}Sr$ and $^{143}Nd/^{144}Nd$ ratios of the Sangdong granites have 0.714~0.716(${\varepsilon}_{Sr}$=138~162) and 0.51173~0.51178(${\varepsilon}_{Nd}$=-14.4~15.5), respectively. And their two stage model ages range from 1687 to 1764 Ma. The granite characterized by high strontium initial ratios and negative eNd value could have originated from the old continental crust source. Low homogenization temperature of the Sangdong granite having $203{\sim}296^{\circ}C$ with 1.9~9.2 NaCl equiv. wt% indicates the post-magmatic hydrothermal alteration temperature. Skarn ore fluid responsible for tungsten mineralization has been evolved from CH, rich fluid of early pyroxene garnet skarn to $CO_2$ rich later quartz-mica skarn.

  • PDF