• Title/Summary/Keyword: Morphology characteristic

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Synthesis of Porous Carbon Particles for the Absorption of Mercury (액상수은 제어를 위한 다공성 탄소입자 제조에 관한 연구)

  • Lee, Jung-Min;Kang, Shin-Jae;Park, Soo-Jin
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.305-305
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    • 2009
  • The carbon nano-structured materials could be applied to the fields of advanced fillers, templates, electrode materials, sensor, storage, and absorption materials. The polyacrylonitrile (PAN) based carbon nano-particles provide the remarkable properties of high specific surface area, large pore volume, chemical inertness, and good mechanical stability. In this study, well-defined carbon nano-particles were obtained through pyrolysis of polyacrylonitrile based particles. The precursor nano-particles were prepared by modified aqueous dispersion polymerization using hydrophilic poly(vinyl alcohol) in a water/ N,N-dimethylformamide mixture media. Synthesized precursor nanoparticles have relatively monodisperse particles ranging 80 ~ 250nm. Stable spherical particles are obtained without coagulum or secondary particles in our system. The characteristic of the carbon nanoparticles were investigated in terms of surface area, morphology, and size distribution.

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Further Evidence that Ramularia-type Conidia in vivo Plays a Role as a Secondary Inoculum of Mycosphaerella nawae (감나무 둥근무늬낙엽병균 Mycosphaerella nawae 분생포지의 2창 전염원으로서 역할)

  • 권진혁;강수웅;박창석;김희규
    • Korean Journal Plant Pathology
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    • v.14 no.5
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    • pp.393-396
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    • 1998
  • The characteristic Ramularia type conidia of Mycosphaerella nawae were formed on naturally infected leaves. Artificial inoculation with the conidia induced typical symptom on leaves, which was not distinguishable from those of ascospore infection, which has been considered as a primary inoculum source in nature. Also the morphology of the conidia produced on PDA was not different from those formed on artificially inoculated leaves or on naturally infected leaves at later stage of symptom development. Accordingly, we report the role of the conidia as a secondary inoculum of the circular leaf spot pathogen of persimmon for the first time.

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A Study on Automatic wear Debris Recognition by using Particle Feature Extraction (입자 유형별 형상추출에 의한 마모입자 자동인식에 관한 연구)

  • ;;;A. Y. Grigoriev
    • Tribology and Lubricants
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    • v.15 no.2
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    • pp.206-211
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    • 1999
  • Wear debris morphology is closely related to the wear mode and mechanism occured. Image recognition of wear debris is, therefore, a powerful tool in wear monitoring. But it has usually required expert's experience and the results could be too subjective. Development of automatic tools for wear debris recognition is needed to solve this problem. In this work, an algorithm for automatic wear debris recognition was suggested and implemented by PC base software. The presented method defined a characteristic 3-dimensional feature space where typical types of wear debris were separately located by the knowledge-based system and compared the similarity of object wear debris concerned. The 3-dimensional feature space was obtained from multiple feature vectors by using a multi-dimensional scaling technique. The results showed that the presented automatic wear debris recognition was satisfactory in many cases application.

Hydrogen Spillover Kinetics - I. Effect of Surface Morphology on [$Pt/MoO_{3}$] Catalyst (수소 spillover 속도론 - I. $Pt/MoO_{3}$ 촉매의 표면 형상 변화)

  • Kim Jin Gul;Kim Seong-Soo
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.5 no.6
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    • pp.491-494
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    • 2004
  • [ $H_2$ ] uptake into $Pt/MoO_{3}$ was enhanced with an increased calcination temperature. Selective CO pulse chemisorption demonstrated that free Pt surface area was decreased as calcination temperature was increased. Characteristic techniques were dedicated to elucidate the closer contact at adlineation sites between Pt and $MoO_3$ substrates. Calcination resulted in supplying the hydrogen access into more $MoO_3$ particles and controlling the kinetics of hydrogen uptake.

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The Preparation Characteristic of Polyphenylenediamine -Dimercaptan Composite film (Polyphenylenediamine-Dimercaptan 복합 필름의 제막특성)

  • 박수길;나재진;이홍기;임기조;김상욱;이주성
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1996.11a
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    • pp.105-108
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    • 1996
  • The positive active material for polymer film battery was prepared by using Polyphenylenediamine(PPD) synthesized in our lab. and 2.5-dimercapto-1, 3, 4-thiadiazole(DMcT) in various mixture ratio. The transference measurement of surface morphology and thermal stability of prepared composite film was carried out by using SEM and TGA, respectively. Electrocyhemical property and electrical conductivity of composite film were also measured by using cyclic voltammetry and four-probe method in dry box, respectively. The thermal stability of prepared composite film is more than 20$0^{\circ}C$. The electrical conductivity of composite film increased and showed the highest value(about 3 S/cm)when doped at 0.4% LiClO$_4$solution. And we could confirm that DMcT effect on reactiviation of PPD through cyclic voltammogram.

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Effect of Mineralizer Concentration and Starting Materials on the Characteristics of PZT Powders by Hydrothermal Process (수열합성법으로 제조된 PZT 분말의 특성에 미치는 광화제 농도와 출발물질의 영향)

  • Yang, Beom-Seok;Yun, Ki-Seok;Park, Young-Chul;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.42 no.11 s.282
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    • pp.743-748
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    • 2005
  • The effect of reaction parameters in the characteristic of $Pb(Zr_{0.52} Ti_{0.48})O_3$ powders by hydrothermal process was investigated in this study. In the preparation of PZT, the types of starting material and concentration of mineralizer on phase fraction and morphology was investigated respectively. Regardless the types of Pb precursor, PZT was able to synthesize ranging from 7 to 20 on KOH concentration and from 13.01 to 13.55 on pH of solution. The particle size of the PZT powders can be controlled by the mineralizer concentration and various types of precursor.

Control of Morphological Development and Transformation of Curves (곡선의 형태학적 성장과 변환의 제어 방법)

  • Lee, Joo-Haeng;Park, Hyung-Jun
    • Korean Journal of Computational Design and Engineering
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    • v.12 no.5
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    • pp.354-365
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    • 2007
  • We present novel methods to generate a sequence of shapes that represents the pattern of morphological development or transformation of Bezier curves. The presented methods utilize the intrinsic geometric structures of a Bezier curve that are derived from rib and fan decomposition (RFD). Morphological development based on RFD shows a characteristic pattern of structural growth of a Bezier curve, which is the direct consequence of development path defined by fans. Morphological transformation based RFD utilizes development patterns of source and target curves to mimic the theory of evolutionary developmental biology: although the source and target curves are quite different in shapes, we can easily find similarities in their younger shapes, which makes it easier to set up feature correspondences for blending them. We also show that further controls on base transformation for intensity of feature blending, and extrapolation can compensate the immaturity of blended curves. We demonstrate the experimental results where transformation patterns are smoother and have unique geometric style that cannot be generated using conventional methods based on multi-linear blending.

The Characteristics of Resonant Stimulated Raman Scattering in the water droplet (미세 물방울에서의 공명 유도라만산란의 특성)

  • 문희종;김광훈;임용식;고춘수;이재형;장준성
    • Korean Journal of Optics and Photonics
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    • v.6 no.4
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    • pp.337-344
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    • 1995
  • We have detected the resonant stimulated Raman scattering signal when the Q-switched Nd:YAG laser beam are incident on the $35~62{\mu}m$ sized water droplet as pump beam. The signals appeared as uniformly spaced peaks and the intervals between peaks become narrow as the droplet size increases. Also we have confirmed the morphology dependent resonances (MDR's) characteristic of the stimulated Raman scattering signal when the water droplet becomes nearly spherical shape after two water droplets are coupled to a droplet. The error in the measured intervals between MDR's of same mode order is about 5%.out 5%.

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Characterization of PVOH Nonwoven Mats Prepared from Surfactant-Polymer System via Electrospinning

  • Jung, Yoon-Ho;Kim, Hak-Yong;Lee, Douk-Rae;Park, Sun-Young;Khil, Myung-Seob
    • Macromolecular Research
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    • v.13 no.5
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    • pp.385-390
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    • 2005
  • The electrospinning process is a fascinating method to fabricate small nanosized fibers of diameter several hundred nanometers. Surfactant-polymer solutions were prepared by adding poly(vinyl alcohol) (PVOH) to distilled water with cationic, anionic, amphoteric, and non-ionic surfactants. Average diameter of the electrospun PVOH fibers prepared from PVOH solution was over 300 nm, and was decreased to 150 nm for the mixture of PVOH/amphoteric surfactant. To explain the formation of ultra fine fiber, the characteristic properties in a mixture of PVOH/surfactant such as surface tension, viscosity, and conductivity were determined. In this paper, the effect of interactions between polymers with different classes of surfactants on the morphological and mechanical properties of electrospun PVOH nonwoven mats was broadly investigated.

Deformation Characteristic by Compression in High-Nitrogen Austenitic Stainless Steel (고질소강 오스테나이트계 스테인레스강의 압축변형특성)

  • Lee, J.W.;Kim, D.S.;Kim, B.K.;Lee, M.R.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.10a
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    • pp.139-141
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    • 2007
  • Compression tests were carried out to investigate morphologies of compressed specimen, deformation microstructure and stress-strain relation in high-nitrogen austenite stainless steel. Tests were performed under a wide range of temperature and, with true strain rates up to $\dot{\varepsilon}$ =0.05, 0.1, 0.5 and $1.0s^{-1}$. The activation energy of loading force was equal to plastic deformation energy within the temperature range of $900^{\circ}C$ to $1250^{\circ}C$. Dynamically recrystallized grain size decreased with an increasing strain rate and temperature. Flow stresses and deformation microstructures, were used to quantify the critical strain rate and recrystallized grain size. The grain size versus strain rate-temperature map obtained in the study was in good agreement with the deformation microstructures of compressed specimens.

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