• Journal of Powder Materials
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• v.22 no.4
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• pp.266-270
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• 2015

The synthesis of NiTi alloy powders by hydrogen reduction and dehydrogenation process of NiO and $TiH_2$ powder mixtures is investigated. Mixtures of NiO and $TiH_2$ powders are prepared by simple mixing for 1 h or ball milling for 24 h. Simple-mixed mixture shows that fine NiO particles are homogeneously coated on the surface of $TiH_2$ powders, whereas ball milled one exhibits the morphology with mixing of fine NiO and $TiH_2$ particles. Thermogravimetric analysis in hydrogen atmosphere reveals that the NiO and $TiH_2$ phase are changed to metallic Ni and Ti in the temperature range of 260 to $290^{\circ}C$ and 553 to $639^{\circ}C$, respectively. In the simple-mixed powders by heat-up to $700^{\circ}C$, agglomerates with solid particles and solidified liquid phase are observed, and the size of agglomerates is increased at $1000^{\circ}C$. From the XRD analysis, the presence of liquid phase is explained by the formation and melting of $NiTi_2$ inter-metallic compound due to an exothermic reaction between Ni and Ti. The simple-mixed powders, heated to $1000^{\circ}C$, lead to the formation of NiTi phase but additional Ni-, Ti-rich and Ti-oxide phases. In contrast, the microstructure of ball-milled powders is characterized by the neck-grown particles, forming $Ni_3Ti$, Ti-oxide and unreacted Ni phase.

• Proceedings of the IEEK Conference
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• 2003.07c
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• pp.2589-2592
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• 2003

In this paper, a robust mixed H$_2$/H$\_$$\infty$/ output feedback control method is applied to the design of loop filter for PLL carrier phase tracking. The proposed method successfully copes with large S-curve slope uncertainty and a significant decision delay in the closed-loop that may exist In modern receivers due to a convolutional decoder or an equalizer. The objective is to design an output feedback controller which minimizes the H$_2$performance while satisfying the H$\_$$\infty$/ performance to guarantee the gain margin and phase margin for linear time invariant(LTI) polytopic uncertain systems. LMIs based approach is given to solve this problem. We can verify the H$\_$$\infty$/ performance satisfaction and minimize the phase detector error through the simulation result.

• Journal of the Korean Applied Science and Technology
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• v.14 no.2
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• pp.35-40
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• 1997

The organization of phospholipid monolayers and their monolayers mixed with fatty acid containing azobenzene on the water surface was investigated by means of the displacement current measurement method. The phase transition from the gaseous phase to the gaseous-fluid phase which accompanies the polar ordering of phospholipid molecules was detected in the range of immeasurably low surface pressure. The molecular area which gives the onset of the transition was determined for phospholipid monolayers. The Maxwell displacement current(MDC) pulses were generated across mixed monolayers due to the photoisomerization of fatty acid containing azobenzene by alternating irradiation of ultraviolet and visible light, because the condensation of pure azobenzene monolayers was loosened by the introduction of phospholipids into the monolayers. The displacement currents generated during light irradiation were also investgated in connection with monolayer compression cycles. It was found that the maximum of MDC appeared at the molecular area just before the initial rise of surface pressure in compression cycles.

• Journal of Powder Materials
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• v.8 no.1
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• pp.20-25
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• 2001

Most of mold manufacturing procedures have been automated by the introduction of NC machine tool and CAD/CAM system. But the three-dimensional surface curvature of the mold must be done by hand work of well-skilled workers. Magnetic abrasive polishing powders were investigated for surface polishing for 3D curvature. This study aims to investigate homogeneously distributed hard phase in Fe matrix and strong bonding between Fe-matrix and hard phase. The NbC powder, $B_4C$ powder and $Al_2O_3$ powder were mixed in Fe-matrix respectively. Mixed Fe-hard phase powders were compacted by press and then these were melted by plasma melting. According to SEM, XRD and OM observation, Fe-NbC magnetic abrsive powder had the most homogeneous distribution and strong bonding. As a result of magnetic polishing, the surface roughness before magnetic polishing, 1 ${\mu}m$ $R_{max}$, was reduced to 0.2 ${\mu}m$ $R_{max}$ over the entire inner surface of the tube.

• Journal of the Korean institute of surface engineering
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• v.22 no.4
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• pp.207-214
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• 1989

The surface morphology and the proferred orientation of the Pb-Sn alloy electrodeposite were investated by the change of electrolysis conditions in pulse current electroplating. The preferred orientation of Pb-phase in alloy deposits was changed in the sequence of (110)longrightarrow(100)or(100)+(111)longrightarrow(111) with increasing peak current density, while that of $\beta$-Sn phase changed from (321)+(301)to(301)+(111) mixed orientation. The surface morphology was closely related to the preferred orientation of alloy electrodeposits. The alloy deposits, which had (100)or(111) for pb-phase and (321)or(100)(301)for $\beta$-Sn sespectively, showed the surface structure of granular crystallites. The alloy deposits whih mixed orientations for both phases had microstructure of closely the closely stacked crysrallites, which was inclined to the surface.

• Bulletin of the Korean Chemical Society
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• v.13 no.2
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• pp.122-127
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• 1992

Some perovskites $A($Cu_{1}3}Nb_{2}3}$)O_3(A=$Sr^{2+}$$, $Ba^{2+}$ and $Pb^{2+}$) and their series of mixed perovskites have been prepared by solid state reaction. Single perovskite phase was obtained in Sr or Ba rich samples, but pyrochlore phase was found in Pb rich samples. The stability of perovskite phase is dependent on the ionicity of bonding as well as the tolerance factor. All the obtained perovskites have tetragonal symmetry distorted by Jahn-Teller effect of $Cu^{2+}$. In the case of $Sr(Cu_{1}3}Nb_{2}3})O_3$, some superlattice lines caused by threefold enlarging of fundamental unit cell were observed. And, the symmetry of B site octahedron and the bonding character of B-O bond have been studied by IR, ESR and diffuse reflection spectroscopy. It appeared that the symmetry and the bonding character are influenced by such factors as the size and the basicity of A cation.

• Journal of applied mathematics & informatics
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• v.24 no.1_2
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• pp.191-207
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• 2007

Based on a mixed Galerkin approximation, we construct the fully discrete approximations of $U_y$ as well as U to a single-phase quasilinear Stefan problem with a forcing term in non-divergence form. We prove the optimal convergence of approximation to the solution {U, S} and the superconvergence of approximation to $U_y$.

• 한국생물공학회:학술대회논문집
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• 2002.04a
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• pp.504-507
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• 2002

A separation/purification process for enzymatic sugar ester production was investigated The crude reaction mixture contained sugar ester and unreacted fatty acid in acetone. The reaction mixture was mixed with KOH/phosphate buffer. Hexane was then added to enhance phase separation. Three phases formed: a lower aqueous phase containing nothing of interest, a polar organic solvent middle phase that contained mostly fatty acid soaps, and a hexane-rich upper phase that contained mostly sugar ester. Distribution coefficient of each component was measured.

• 유체기계공업학회:학술대회논문집
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• 2000.12a
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• pp.110-115
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• 2000

The mean streamline analysis using the empirical loss correlations has been developed for performance prediction of industrial mixed-flow fan impellers in the present study. New simple, but effective, models for the additional Euler input work characteristic and an internal recirculation loss due to internal flow reversal under the low flowrate conditions are proposed in this paper. Comparison of overall performance predictions with six sets of test data of mixed-flow fans is accomplished to demonstrate the accuracy of the proposed models. Predicted performance curves by the present set of loss models agree fairly well with experimental data for a variety of mixed-flow fan impellers over the entire operating conditions. The prediction method presented herein can be used efficiently in the conceptual design phase of mixed-flow fan impellers.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.23 no.6
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• pp.602-608
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• 2014

Mixed-model production lines are often used in manufacturing systems. In production lines, different product types are simultaneously manufactured by processing small batches. This paper describes a new welding assembly technology involving the development of experimental models for a mixed-model production line in an automobile company. Due to the extensive number of models, the design of a welding assembly system is complicated. Performance evaluation is an important phase in the design of welding assembly lines in a mixed-model production environment. In this study, a new welding assembly technology for a mixed-model production method was used to weld the package tray and dash panel of a vehicle.