• Title/Summary/Keyword: Microwave processing

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EFFECTS OF SUBSTRATE TEMPERATURE ON PROPERTIES OF FLUORINE CONTAINED SILICON OXIDE FILMS PREPARED BY MICROWAVE PLASMA- ENHANCED CVD

  • Sugimoto, Nobuhisa;Hozumi, Atsushi;Takai, Osamu
    • Journal of Surface Science and Engineering
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    • v.29 no.5
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    • pp.577-584
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    • 1996
  • Silicon oxide films with high hardness and water repellency were prepared by microwave plasma-enhanced CVD using four kind of organosilicon compound-fluoro-alkyl silane mixtures as source gases. An argon gas was used as a carrier gas for fluoro-alkyl silane. The substrate temperatures during deposition were controlled by resistant heating at a constant value between 50 and $300^{\circ}C$. The hardness of the films increased, but the deposition rate and the contact angle for a water drop decreased with increasing substrate temperature. The number of methoxy groups also affected the water repellency and hardness. The deposited films became more inorganic with increasing substrate temperature because of the thermal dissociation of reactants.

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Microwave Dielectric Properties of (1-X) ${Na}_{1/2}{Sm}_{1/2}TiO_3-X\;{Li}_{1/2}{Nd}_{1/2}TiO_3$ Ceramics ((1-X) ${Na}_{1/2}{Sm}_{1/2}TiO_3-X\;{Li}_{1/2}{Nd}_{1/2}TiO_3$ 세라믹스의 고주파 유전특성)

  • Yun, Jung-Rag;Hong, Suk-Kyung;Kim, Kyung-Yong
    • Proceedings of the KIEE Conference
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    • 1993.07b
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    • pp.1103-1105
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    • 1993
  • Microwave characteristics of the system (1-X) ${Na}_{1/2}{Sm}_{1/2}TiO_3$[NST]-X ${Li}_{1/2}{Nd}_{1/2}TiO_3$[LNT] were investigated. The dielectric constant and unloaded Q were 86,1950 respectively for NST at 3GHz and 80,500 for LNT. 0.4 NST - 0.6 LNT system has the dielectric constant ${\varepsilon}r$=86.2, Q=930(3GHz), temperature coefficient of the resonant frequency ${\tau}f$ = 8 ppm/$^{\circ}C$ when sintered at $1450^{\circ}C$ for 2h.

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Changes in Phytochemical Compounds and Hazardous Factors of Spinach by Blanching Methods (데치는 방법에 따른 시금치의 phytochemical 성분 및 위해성 요인 변화)

  • Hong, Jeong-Jin;Ahn, Tae-Hyun
    • Korean Journal of Food Science and Technology
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    • v.37 no.2
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    • pp.268-273
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    • 2005
  • Changes in contents of phytochemical compounds (${\beta}$-carotene, ascorbic acid, chlorophylls, total flavonoid, total polyphenol) and hazardous factors (microbial counts, nitrate) of spinach (Spinacia oleracia L.) were investigated by conventional and microwave blanching methods. ${\beta}$-Carotene and chlorophylls contents of spinach were significantly increased by blanching, with conventional blanching resulting in higher contents than microwave blanching. In contrast, contents of ascorbic acid, total flavonoid, and total polyphenol of blanched spinach decreased, with microwave blanching resulting in higher ascorbic acid, total flavonoid, and total polyphenol contents than conventional blanching. Total plate count and total coliforms of blanched spinach significantly decreased, with conventional blanching showing less than 20-25% of microwave blanching. Nitrate content of blanched spinach also showed decreasing pattern, with decrease due to microwave blanching being lower, although not significantly, than that of conventional blanching.

Design and Fabrication of Thin Microwave Absorbers of ITO/Dielectric Structures Used for Mobile Telecommunication Frequency Bands (ITO박막/세라믹유전체 구조의 이동통신 주파수대역용 박형 전파흡수체의 설계 및 제조)

  • Yoon, Yeo-Choon;Kim, Sung-Soo
    • Korean Journal of Materials Research
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    • v.13 no.4
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    • pp.259-265
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    • 2003
  • For the aim of thin microwave absorbers used in mobile telecommunication frequency band, this study proposed a high permittivity dielectrics(λ/4 spacer) coated with ITO thin films of 377 $\Omega$/sq(impedance transformer). High frequency dielectric properties of ferroelectric ceramics, electrical properties of ITO thin films and microwave absorbing properties of ITO/dielectrics were investigated. Ferroelectric materials including $BaTiO_3$(BT), 0.9Pb($Mg_{1}$3/Nb$_{2}$3/)$O_3$-0.1 $PbTiO_3$(PMN-PT), 0.8 Pb (Mg$_{1}$3/$Nb_{2}$3/)$O_3$-0.2 Pb($Zn_{1}$3$_Nb{2}$3/)$O_3$(PMN-PZN) were prepared by ceramic processing for high permittivity dielectrics,. The ferroelectric materials show high dielectric constant and dielectric loss in the microwave frequency range. The microwave absorbance (at 2 ㎓) of BT, 0.9PMN-0.1PT, and 0.8PMN-0.2PZN were found to be 60%(at a thickness of 3.5 mm), 20% (2.5 mm), and 30% (2.5 mm), respectively. By coating the ITO thin films on the ferroelectric substrates with λ/4 thickness, the microwave absorbance is greatly improved. Particularly, when the surface resistance of ITO films is closed of 377 $\Omega$/sq, the reflection loss is reduced to -20 ㏈(99% absorbance). This is attributed to the wave impedance matching controlled by ITO thin films at a given thickness of high permittivity dielectrics of λ/4 (3.5 mm for BT, 2.5 mm for PMN-PT and PMN-PZN at 2 ㎓). It is, therefore, successfully proposed that the ITO/ferroelectric materials with controlled surface resistance and high dielectric constant can be useful as a thin microwave absorbers in mobile telecommunication frequency band.

The Change of Ginsenoside Composition in Notoginseng Root(Panax notoginseng) Extract by the Microwave and Vinegar Process (초단파 및 식초 처리에 의한 삼칠삼 추출물의 인삼 사포닌 성분 변화)

  • Jo, Hee Kyung;Cho, Soon Hyun;Ko, Sung Kwon
    • Korean Journal of Pharmacognosy
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    • v.45 no.4
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    • pp.320-325
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    • 2014
  • The purpose of this study is to develop a new preparation process of Notoginseng root(Panax notoginseng) extracts having high concentrations of ginsenoside $Rg_3$, $Rg_5$, $Rk_1$ and $Rh_4$, a special component of Red and Black ginseng(Panax ginseng). Chemical transformation from ginseng saponin to prosapogenin was analyzed by the HPLC. Extracts of Notoginseng root was processed under several treatment conditions including microwave and vinegar(about 14% acidity) treatments. Results of those treatments showed that the quantity of ginsenoside $Rg_3$ increased by over 7.6% at 15 minutes of pH 2~4 vinegar and microwave treatments. The results of processing with MPN-15 indicate that the microwave and vinegar(about 14% acidity) processed Notoginseng root extracts that had gone through 15-minute treatments were found to contain the largest amount of ginsenoside $Rg_3$(7.639%), $Rg_5$(6.061%), $Rk_1$(1.516%) and $Rh_4$(1.599). It is thought that such results provide basic information in preparing Notoginseng root extracts with functionality enhanced.

Ammonia Nitrogen Removal in Wastewater Using Microwave Irradiation (마이크로웨이브를 이용한 폐수 내 고농도 암모니아성질소 제거)

  • Shin, Soyeun;Koo, Bonheung;Kim, Taehyun;Lee, Yuhak;Ahn, Johng-Hwa
    • Journal of Korean Society on Water Environment
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    • v.30 no.5
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    • pp.486-490
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    • 2014
  • Industrial use of microwave heating as an alternative to conventional heating is becoming popular mainly due to dramatic reductions in reaction time. Therefore, this work experimentally determined the effect of microwave irradiation on ammonia nitrogen removal in wastewater. The effects of air flow rate (0.3~0.9 L/min), treatment temperature ($70{\sim}100^{\circ}C$), and initial pH (9~11) were characterized. As the air flow rate increased from 0.3 to 0.9 L/min, the ammonia removal rate constant (k) increased from -0.6642 to $-1.0755min^{-1}$. As the temperature increased from 70 to $100^{\circ}C$, k increased -0.0338 to $-1.0755min^{-1}$. As the pH increased from 9 to 11, k increased -0.2443 to $-1.0755min^{-1}$. Ammonia removal was strongly dependent on temperature and pH rather than air flow rate. The results show that microwave irradiation is effective in ammonia nitrogen removal in wastewater due to advantages of fast and effective processing.

Microwave Instantaneous Frequency Measurement (IFM) Approach Based on an Integrated Photonic Ti:LiNbO3 Y Branch

  • Zhang, Changsheng;Zhang, Jiahong;Zhao, Zhengang
    • Current Optics and Photonics
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    • v.4 no.4
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    • pp.361-367
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    • 2020
  • An approach based on an integrated photonic Ti:LiNbO3 Y branch has been proposed, designed, and analyzed for the microwave instantaneous frequency measurement (IFM). By designing the Y branch with length L = 6545 ㎛ and refractive index NTE - NTM = 0.0764, a complementary optical filter with free spectral range (FSR) of 600 GHz is constituted, which results in a maximum measureable frequency of 300 GHz being obtained. Theoretical analysis on the temperature stability of the Ti:LiNbO3 Y branch shows that the FSR variation of the complementary filter is 0.3% for the temperature change of 100 K, which indicates that the IFM approach will have a better stability. All these results demonstrate that the proposed IFM approach has potential capability to be used for the increasingly higher microwave IFM with better stability.

3D Printed Flexible Cathode Based on Cu-EDTA that Prepared by Molecular Precursor Method and Microwave Processing for Electrochemical Machining

  • Yan, Binggong;Song, Xuan;Tian, Zhao;Huang, Xiaodi;Jiang, Kaiyong
    • Journal of Electrochemical Science and Technology
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    • v.11 no.2
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    • pp.180-186
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    • 2020
  • In this work, a metal-ligand solution (Cu-EDTA) was prepared based on the molecular precursor method and the solution was spin-coated onto 3D printed flexible photosensitive resin sheets. After being processed by microwave, a laser with a wavelength of 355 nm was utilized to scan the spin-coated sheets and then the sheets were immersed in an electroless copper plating solution to deposit copper wires. With the help of microwave processing, the adhesion between copper wires and substrate was improved which should result from the increase of roughness, decrease of contact angle and the consistent orientation of coated film according to the results of 3D profilometer and SEM. XPS results showed that copper seeds formed after laser scanning. Using the 3D printed flexible sheets as cathode and galvanized iron as anode, electrochemical machining was conducted.

Experimental Study on Manufacturing Fiber Metal Laminate using Microwave Heating Based on PTFE Mold (섬유금속적층판 제작을 위한 PTFE 몰드 기반 마이크로파 공정에 대한 실험적 연구)

  • Park, E.T.;Lee, Y.H.;Kim, J.;Kang, B.S.;Song, W.J.
    • Transactions of Materials Processing
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    • v.29 no.4
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    • pp.179-187
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    • 2020
  • Existing composite forming processes such as the autoclave, prepreg compression forming (PCF), RTM, etc. require high production costs because of their long processing time. On the other hand, microwave heating process (MHP) can reduce the production costs since both mold and composite material can be heated directly. The aim of this study is to manufacture a mold consisting of polytetrafluoroethylene (PTFE), quartz glass, stainless steel clamps, and polyether ether ketone (PEEK) bolts for fabricating FML based on self-reinforced polypropylene (SRPP) using the MHP. First, the flame test was carried out prior to the MHP to check the temperature on the mold and whether the spark occurred at the mold and the edge of the FML. Second, the uniaxial tensile test was then conducted to obtain the mechanical properties of the FML manufactured by the MHP. The mechanical properties were compared with those of the FML fabricated by the PCF. As a result, the MHP using the PTFE mold can manufacture the FML more rapidly than the PCF, and obtain acceptable mechanical properties.