• Transactions of Materials Processing
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• v.20 no.7
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• pp.491-497
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• 2011

This work describes a method for determining material parameters included in recrystallization and grain growth models of metallic materials. The focus is on the recrystallization and grain growth models of Ni-Fe based superalloy, Alloy 718. High temperature compression test data at different strain, strain rate and temperature conditions were chosen to determine the material parameters of the model. The critical strain and dynamically recrystallized grain size and fraction at various process conditions were generated from the microstructural analysis and strain-stress relationships of the compression tests. Also, isothermal heat treatments were utilized to fit the material constants included in the grain growth model. Verification of the determined material parameters is carried out by comparing the average grain size data obtained from other compression tests of the Alloy 718 specimens with the initial grain size of $59.5{\mu}m$.

• Journal of the Korea Institute of Military Science and Technology
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• v.7 no.4 s.19
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• pp.70-78
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• 2004

A study has been made to investigate the high temperature deformation behavior of Ti-6Al-4V alloyand to predict the final microstructure under given forming conditions. Equiaxed and $Widmanst\ddot{a}tten$ microstructures of Ti-6Al-4V alloys were prepared as initial microstructures. By performing the compression tests at high temperatures$(700\~1100^{\circ}C)$ and at a wide range of strain rates$(10^{-4}\~10^2/s)$, various parameters such as strain rate sensitivity(m) and activation energy(Q) were calculated and used to establish constitutive equations. When the specimens were deformed up to strain 0.6, equiaxed microstructure did not show any significant changes in microstructure, while $Widmanst\ddot{a}tten$ microstructure revealed considerable flow softening, which was attributed to the globularization of a platelet at the temperature range of $800\~970^{\circ}C$ and at the strain rate range of $10^{-4}\~10^{-2}/s$. To predict the final microstructure after forming, finite element analysis was performed considering the microstructural evolution during the deformation. The grain size and the volume fraction of second phase of deformed body were predicted and compared with the experimental results.

• Transactions of Materials Processing
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• v.14 no.4 s.76
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• pp.384-391
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• 2005

The nickel-based alloy Nimonic 80A possesses the excellent strength, and the resistance against corrosion, creep and oxidation at high temperature. Its products are used in aerospace engineering, marine engineering and power generation, etc. Control of forging parameters such as strain, strain rate, temperature and holding time is important because change of the microstructure in hot working affects the mechanical properties. Change of the microstructure evolves by recovery, recrystallization and grain growth phenomena. The dynamic recrystallization evolution has been studied in the temperature range of $950\~1250^{\circ}C$ and strain rate range of $0.05\~5s^{-1}$ using hot compression tests. The metadynamic recrystallization and grain growth evolution has been studied in the temperature range of $950\~1250^{\circ}C$ and strain rate range $0.05,\;5s^{-1}$, holding time range of 5, 10, 100, 600 sec using hot compression tests. Modeling equations are proposed to represent the flow curve, recrystallized grain size, recrystallized fraction and grain growth phenomena by various tests. Parameters in modeling equations are expressed as a function of the Zener-Hollomon parameter. The modeling equation for grain growth is expressed as a function of the initial grain size and holding time. The modeling equations developed were combined with thermo-viscoplastic finite element modeling to predict the microstructure change evolution during hot forging process. The grain size predicted from FE simulation results is compared with results obtained in field product.

• Journal of the Korean Ceramic Society
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• v.29 no.7
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• pp.517-524
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• 1992

For the present study two alumina bodies were prepared. The sinter-aid alumina body(SAA) was made by conventional sinter-process using sintering additives of TiO2 & MgO/CaO and the reaction-bonded alumina (RBA) made from Al-Al2O3 mixed powder. A comparison was made between those two bodies and this investigation seeks to evaluate their microstructure, physical properties and material's reliability as well as their fracture behaviour. In spite of its considerable microstructural densification accompanied by sintering shrinkage, SAA is largely inferior to RBA in fracture strength. However, SAA shows a somewhat higher m-value than RBA in respect to the material's reliability, the Weibull modulus(m). RBA, which has high fracture strength, shows much longer lifetime under static loading than SAA. Though, as with m of fracture strength, the reliability(mt) of lifetime prediction in RBA is less high than of SAA.

• Proceedings of the KSME Conference
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• 2008.11b
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• pp.2578-2582
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• 2008

In predicting the critical heat flux (CHF) in pool boiling systems, the contact angle between the boiling surface and the liquid and the surface roughness are considered to be the important parameters. From the microscopic viewpoint, those are affected by the micro/nano structure of the surface. Several studies have been reported on the dependence of CHF on the surface microstructure such as height and width of the cavities and distances between them. In this paper, the effects of the boiling surface characteristics on CHF are reviewed and the future research issues are discussed for better prediction of CHF.

• Journal of the Korea Institute of Military Science and Technology
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• v.9 no.2 s.25
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• pp.70-76
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• 2006

The microstructure evolution during a hot forging of Waspaloy was investigated using the recrystallization model and FEM simulation. In order to obtain an uniform microstructure, hot forging was carried out by two step. The change of grain size during hot forging has a deep connection with dynamic recrystallization behavior. Avrami-type constitutive equation for the dynamic recrystallization was implemented into an user subroutine of 2D FE simulator. The evolution of grain structure in the two-step forging of Waspaloy was simulated using the 2D FEM user-subroutine. The detailed variation of microstructures due to dynamic recrystallization could effectively be predicted at various locations in a forged pancake.

• Transactions of Materials Processing
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• v.10 no.1
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• pp.35-41
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• 2001

The high temperature deformation behavior of SCM 440 can be characterized by the hot torsion test in the temperature ranges of $900^{\circ}C$~$1100^{\circ}C$ and strain rate ranges of 0.05/sec~5/sec. The aim of this paper is to establish the quantitative equation of the volume fraction of dynamic recrystallization (DRX) as a function of processing variables, such as strain rate ($\varepsilon$), temperature (T), and strain ('$\varepsilon$). During hot deformation, the evolution of microstructure could be analyzed from work hardening rate ($\theta$). For the exact prediction of dynamic softening mechanism the critical strain ($\varepsilon_c$), the strain for maximum softening rate ($\varepsilon^*$ and Avrami' exponent (m') were quantitatively expressed by dimensionless parameter, Z/A, respectively. The transformation-effective strain-temperature curve for DRX could be composed. It was found that the calculated results were agreed with the experimental data for the steel at any deformation conditions.

• Journal of Welding and Joining
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• v.18 no.2
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• pp.184-184
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• 2000

In this study, the lap welding between austenitic stainless steel and carbon steel was carried out using arc spot welding process and weldability of welded specimens was estimated. From the tensile-shear strength test, micro Vickers hardness test, and microstructure observation, specimen of 6.5mm(hole of upper plate) showed the best results in terms of tensile-shear strength and nugget shape. And there was an unmixed zone in fusion boundary between the carbon steel base metal and bulk weld metal. This zone had very thin width with the hard microstructure. The shape of weld nugget in arc spot welding of dissimilar metal welds was predicted by searching thermal history of a weld joint through a three-dimensional finite element model. From the numerical analysis, predicted the shape of weld nugget showed good agreement with the experiment(Received August 24, 1999)

• Journal of Welding and Joining
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• v.18 no.2
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• pp.57-63
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• 2000

In this study, the lap welding between austenitic stainless steel and carbon steel was carried out using arc spot welding process and weldability of welded specimens was estimated. From the tensile-shear strength test, micro Vickers harness test, and microstructure observation, specimen of $psi6.5mm$(hole of upper plate) showed the best results in terms of tensile-shear strength and nugget shape. And there was an unmix zone in fusion boundary between the carbon steel base metal and bulk weld metal. This zone had very width with the hard microstructure. The shape of weld nugget in arc spot welding of dissimilar metal melds was predicted by searching thermal history of a weld joint through a three-dimensional finite element model. From the numerical analysis, predicted the shape of weld nugget showed good agreement with the experiment.

• Journal of Welding and Joining
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• v.24 no.1
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• pp.77-87
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• 2006

Considering ferrite grain size in the base metal, the prediction model for $A_{c3}$ temperature and prior austenite grain size at just above $A_{c3}$ temperature was proposed. In order to predict $A_{c3}$ temperature, the Avrami equation was modified with the variation of ferrite grain size, and its kinetic parameters were measured from non-isothermal data during continuous heating. From calculation using a proposed model, $A_{c3}$ temperatures increased with increasing ferrite grain size and heating rate. Meanwhile, by converting the phase transformation kinetic model that predicts the ferrite grain size from austenite grain size during cooling, a prediction model for prior austenite grain size at just above the $A_{c3}$ temperature during heating was developed.