• 제목/요약/키워드: Microstructure development

검색결과 654건 처리시간 0.029초

분말야금법으로 제조된 FeSi2 열전특성 화합물의 열처리 시간에 따른 미세조직과 상변화 (Phase Transformation and Microstructure of FeSi2 Thermoelectric Compounds Manufactured by Powder Metallurgy)

  • 박경태;신진교;홍순직;천병선
    • 한국분말재료학회지
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    • 제17권6호
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    • pp.482-488
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    • 2010
  • In this study, $FeSi_2$ as high temperature performance capable thermoelectric materials was manufactured by powder metallurgy.The as-casted Fe-Si alloy was annealed for homogenization below $1200^{\circ}C$ for 3 h. Due to its high brittleness, the cast alloy transformed to fine powders by ball-milling, followed by subsequent compaction (hydraulic pressure; 2 GPa) and sintering ($1200^{\circ}C$, 12 h). In order to precipitate ${\beta}-FeSi_2$, heat treatment was performed at $850^{\circ}C$ with varying dwell time (7, 15 and 55 h). As a result of this experiment thermoelectric phase ${\beta}-FeSi_2$ was quickly transformed by powder metallurgical process. There was not much change in powder factor between 7h and 55h specimens.

고강도 ADI의 기어부품 개발에 관한 연구 (Development of Control Technology of Austempered Ductile Iron with High Strength and High Toughness for Gear Parts.)

  • 김원용;김광배;강인찬;안상욱
    • 한국주조공학회지
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    • 제13권2호
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    • pp.187-193
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    • 1993
  • In this study, it was examined the relationship between the microstructure, fatigue properties, mechanical properties and retained austenite volume of Mo-Ni ADI corresponding to various austempering temperatures. When the austempering temperature is increased to $370^{\circ}C$, acicular bainite structure was found to be transformed to feathery bainite structure. But at the austempering temperature of $420^{\circ}C$, the dissolved bainite lath was showned. Up to the austempering temperature of $370^{\circ}C$, the volume of retained austenite was increased. However at the austempering temperature of $420^{\circ}C$ a large amount of retained austenite was decreased. In this study, the retained austenite volume was determined by XRD(X-ray diffraction). It was observed that the optimum fatigue properties can be obtained at the condition of austempering temperature $370^{\circ}C$. Under the such conditions, fatigue limit determined as the value of 290 MPa, tensile strength 877MPa elongation 6%, hardness 285(BHN), impact values(CVN) 9.2J and retained austenite volume 30.3%, respectively.

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Ramjet 고속 추진체용 Alloy 718 합금 노즐 단조품 개발 (Development of Alloy 718 Nozzle for Ramjet Propulsion Component)

  • 박노광;김정한;김남용;이채훈;염종택;홍재근;백동규;최성규
    • 한국군사과학기술학회지
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    • 제11권4호
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    • pp.76-82
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    • 2008
  • Alloy 718 nozzle component was manufactured by hot forging and electron beam welding process. In this process, 718 billets produced in domestic company were used and evaluated. Before performing industrial scale hot forging, small size hot compression tests were carried out under various process conditions and then microstructural evaluations were analyzed. Using the results, FEM simulations were performed in order to optimize the hot working process. After hot working, forged work-pieces were machined and welded by electron beam. Final nozzle components were heat treated and their microstructure and mechanical properties were investigated.

자동차 박강판용 고강도 DP강 표면층의 수소거동 (The Hydrogen Behavior of Surface Layers of High Strength DP Thin Sheet Steels for Automobile)

  • 박재우;강계명
    • 한국가스학회지
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    • 제14권6호
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    • pp.38-43
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    • 2010
  • 자원 부족과 환경규제의 강화에 따라 자동차 강판재의 고강도화와 박강판화가 주요 이슈로 대두되고 있다. 그러나 고강도 강판재 사용에 있어 수소취성은 기계적 성질 저하의 문제가 되고 있다. 본 연구에서는 개발중인 590MPa급 DP강을 대상으로 조성 및 조직특성에 따른 표면층에서의 수소의 거동에 대해 연구하였다. 수소주입은 음극전기분해법을 이용하여 강제 주입시켰고, 수소주입조건에 따른 수소주입량과 표면층 조직관찰 및 미소경도시험 결과의 관계로 부터 표면층의 수소거동을 평가하였다.

제어압연${\cdot}$제어냉각기술을 이용한 고강도 냉간성형용 비조질강의 개발 (Development of High Strength Microalloyed Steel for Cold Forming by Controlled Rolling and Cooling Technology)

  • 김남규;박상덕;김병옥;최회진
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2005년도 춘계학술대회 논문집
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    • pp.321-324
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    • 2005
  • The main purpose of the present study has been placed on investigating the effects of controlled rolling and cooling on the microstructures and mechanical properties of C-Si-Mn-V steels for cold forming. The steels were manufactured in vacuum induction melting(VIM) furnace and casted to 1.1ton Ingots and the ingots were forged to $\Box150$ billet. The forged billets were reheated in walking beam furnace and rolled to coil, the stocks were rolled by Controlled Rolling and Cooling Technology (CRCT), so rolled at low temperature by water spraying applied in rolling stage and acceleratly cooled before coiling. Rolled coils were cold drawed to the degree of $27\%$ of area reduction without heat treatment. Microstructual observation, tensile test, compression test and charpy impact tests were conducted. The mechanical properties of the steels were changed by area reduction of cold drawing and it is founded that there are optimum level of cold drawing to minimize compression stress for these steels. From the result of this study, it is conformed that mechanical properties and microstructure of C-Si-Mn-V steels for cold forming were enhanced by accelerated cooling and founded optimum level of cold drawing.

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LIGA 공정을 이용한 삼면반사체 제작 (Fabrication of A 3-facet Mirror Using the LIGA Process)

  • 오동영;정동관;박노열;장석상;이승섭
    • 한국정밀공학회지
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    • 제17권8호
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    • pp.172-179
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    • 2000
  • In this paper a technology for the fabrication of the oblique structure using the LIGA process will be presented. The fabricated microstructure is a tetrahedral 3- facet mirror. The mirror has an equilateral triangular base of hundreds ${\mu}m$ length mirror-like three side-facets inclined to the base at 45$^{\circ}$ and knife edges. Two regular triangles of 45$^{\circ}$ and tan-12. After development the shaded part of the PMMA the tetrahedral mirror remains, The completed mirror shows excellent aspects of mirror-like facets and knife-edges. By controlling the gap between the mask and the substrate the size of mirror easily can be changed. This mirror would be used as a laser beam splitter for the feedback control of the HDD slider.

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고강도 Al-Zn기 다이캐스팅 합금개발에 관한 연구 II: 중력주조, 유동성평가 (A Study on Development of High Strength Al-Zn Based Alloy for Die Casting II: Evaluation of Fluidity and Gravity Casting)

  • 신상수;임영훈;김억수;임경묵
    • 대한금속재료학회지
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    • 제50권7호
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    • pp.531-538
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    • 2012
  • In this study, we evaluated the fluidity of the Al-Zn based alloys which exhibit excellent mechanical properties. We conducted computer simulations of fluid flow using the results of DSC, DTA analysis and Java-based Materials Properties software (J. Mat. Pro). Such computer simulations were then compared with the results obtained from experimental observations. The computer simulation results and the experimental results were very similar in fluidity length. It was found that the fluidity length of Al-Zn alloys is improved by increasing the Zn content while decreasing the solidus temperature of an alloy. In addition, we elucidate the effect of Zn addition on variations in different mechanical properties and the microstructure characteristics of (Al-xZn3Cu0.4Si0.3Fe) x=20, 30, 40, and 45 wt% alloys fabricated by gravity casting.

고강도 Al-Zn기 다이캐스팅 합금개발에 관한 연구 I (A Study of the Development of a High-Strength Al-Zn Based Alloy for Die Casting I)

  • 신상수;염길용;김억수;임경묵
    • 대한금속재료학회지
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    • 제48권10호
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    • pp.936-941
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    • 2010
  • Al-Zn based alloys are the most common types of wrought Al alloys. Although Al-Zn alloys have high strength, they cannot be applied to a conventional casting process. In this study, Al-Zn-based alloys applicable to a die casting process were developed successfully. The developed Al-45 wt% Zn-based alloys showed a fine equiaxed grain structure and high strength. A fine equiaxed grain having an average size of $25{\mu}m$ was obtained by the die casting process. The UTS and elongation of the new alloy are 475 MPa and ~3.5%, respectively. In addition, we elucidate the effect of a Zn addition on variations in different mechanical properties and the microstructure characteristics of (Al96.3-xZnxCu3Si0.4Fe0.3) x=20, 30, 40, and 45 wt% alloys fabricated by a die casting process.

고 Mn계 TWIP 강의 미세조직과 기계적 성질 (Microstructure and Mechanical Properties of High Mn TWIP Steels)

  • 정종구;이오연;박영구;김동은;진광근;김성규;송기홍
    • 대한금속재료학회지
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    • 제46권10호
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    • pp.627-633
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    • 2008
  • The austenitic Fe-Mn alloys have received considerable attention as a possible candidate for the automotive structural materials due to their high strength and high formability with high elongation. This research investigates the effect of alloying elements on the phase transformation, deformation behavior and mechanical properties in high Mn steels for the development of a high strength high ductility steel. The mechanical stability of austenitic phases is very important for high ductility and it depends largely on the composition of carbon, manganese and aluminum. The dominant deformation mode shifts from TRIP to TWIP mode as the amount of C, Mn and Al is increased. Especially, even a small amount of Al addition facilitates significantly TWIP deformation due to the increase of stacking fault energy in Fe-Mn alloys, this leads to increase the ductility and also decrease the crack sensitivity.

Effect of CNT Addition on the Hydriding and Dehydriding Rates of Mg-Ni-Fe2O3 Alloy

  • Song, Myoung Youp;Kwak, Young Jun;Lee, Byung-Soo;Park, Hye Ryoung;Kim, Byoung-Goan
    • 대한금속재료학회지
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    • 제49권12호
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    • pp.989-994
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    • 2011
  • Samples with compositions of 80 wt% Mg-14 wt% Ni-6 wt% $Fe_2O_3$ (named $Mg-Ni-Fe_2O_3$), and 78 wt% Mg-14 wt% Ni-6 wt% $Fe_2O_3-2$ wt% CNT (named $Mg-Ni-Fe_2O_3-CNT$ ) were prepared by reactive mechanical grinding. Hydriding and dehydriding properties and effects of CNT addition on the hydriding and dehydriding rates of $Mg-Ni-Fe_2O_3$ were then investigated. Activation of the $Mg-14Ni-6Fe_2O_3$ sample was completed after three hydriding (under 12 bar $H_2$)-dehydriding (under 1.0 bar $H_2$) cycles at 573 K. The addition of CNT to the $Mg-14Ni-6Fe_2O_3$ sample made the activation process unnecessary, with a small decrease in the hydrogen-storage capacity.