• Journal of Powder Materials
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• v.29 no.5
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• pp.399-410
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• 2022

Changes in the mechanical properties and microstructure of an IN 939 W alloy according to the sintering heating rate were evaluated. IN 939 W alloy samples were fabricated by spark plasma sintering. The phase fraction, number density, and mean radius of the IN 939 W alloy were calculated using a thermodynamic calculation. A universal testing machine and micro-Vickers hardness tester were employed to confirm the mechanical properties of the IN 939 W alloy. X-ray diffraction, optical microscopy, field-emission scanning electron microscopy, Cs-corrected-field emission transmission electron microscopy, and energy dispersive X-ray spectrometry were used to evaluate the microstructure of the alloy. The rapid sintering heating rate resulted in a slightly dispersed γ' phase and chromium oxide. It also suppressed the precipitation of the η phase. These helped to reinforce the mechanical properties.

• Journal of the Korean Society for Heat Treatment
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• v.18 no.1
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• pp.12-17
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• 2005

Effects of Zn and Zr additions on the microstructure and mechanical properties of Al-5%Mg-1%Mn alloys were investigated. As Zn content increased in the Al-Mg-Mn-Zn alloys, the tensile strength and ductility of as-cast alloys rather decreased while the tensile strength of the heat-treated alloys significantly increased mainly due to the precipitation of fine $MgZn_2$ phases. Small amount of Zr was added to the 3%Zn alloy to further enhance the mechanical properties, and it appeared to increase the strength and ductility, especially in as-cast state.

• Transactions of Materials Processing
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• v.32 no.3
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• pp.145-152
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• 2023

The Inconel 706 alloy is a nickel-based super alloy and requires a large load for hot forging due to its excellent mechanical properties at high temperature. Rotary forging process is an innovative metal forging process where workpiece is gradually deformed by the revolving conical upper die with an inclination angle. This process allows that the workpiece is partially in contact with an upper die during the process so that the press force is considerably lower compared with the conventional upsetting process. In this study, experiments of rotary forging process and conventional upsetting process for cylindrical parts using Inconel 706 where conducted to investigate the formability of rotary forging process. And microstructure analysis and mechanical properties of Inconel 706 were performed to investigate the effect of rotary forging process on the material property.

• Korean Journal of Materials Research
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• v.33 no.6
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• pp.251-256
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• 2023

This study aims to examine the correlation between microstructures and the mechanical properties of two high-strength API X70 linepipe steels with different specimen directions and Moaddition. The microstructure of the Mo-added steel has an irregularly shaped AF, GB matrix with pearlite because of the relatively large deformation in the non-recrystallization temperature region, while that of the Mo-free steel shows a PF matrix with bainitic microstructure. In the Mo-added steel, the M/A (martensite-austenite) in granular bainite (GB) and pearlite act as crack initiation sites with decreased upper shelf energy and an increased ductile to brittle transition temperature (DBTT). Regardless of Mo addition, all of the steels demonstrate higher strength and lower elongation in the T direction than in the L direction because of the short dislocation glide path and ease of pile-up at grain boundaries. In addition, the impact test specimens with T-L direction had a lower impact absorbed energy and higher DBTT than those with the L-T direction because the former exhibit shorter unit crack path compared to the latter.

• Journal of the Korean Ceramic Society
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• v.41 no.10 s.269
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• pp.723-727
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• 2004

Three kinds of $Si_3N_4$ powders (M-11, SN-ESP, and SN-E10) were gas-pressure sintered at $1700-1900^{\circ}C$ for 2 h under 18 atm $N_2$. Their densification behavior was investigated and compared as well as the mechanical properties and microstructure of the resulting ceramics. SN-ESP and SN-E10 started to reach nearly full densification at $1750^{\circ}C$ and showed almost no decomposition up to $1900^{\circ}C$. In contrast, M-11 was not fully densified until $1800^{\circ}C$ and showed about $3\%$ weigh loss at $1900^{\circ}C$ indicating poor thermal stability. SN-ESP and SN-E10 showed much higher strength both at room temperature and $1200^{\circ}C$ than M-11 when fully densified. Compared with SN-ESP, SN-E10 was not only a little better in strength (both at room temperature and $1200^{\circ}C$) and fracture toughness but also much higher in the Weibull modulus due to more interlocked microstructure by well elongated grains.

• Nuclear Engineering and Technology
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• v.47 no.3
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• pp.323-331
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• 2015

Zirconium alloys are widely used in nuclear reactors as structural materials. During the operation, they are exposed to fast neutrons. Ion irradiation is used to simulate the damage introduced by neutron irradiation. In this article, we briefly review the neutron irradiation damage of zirconium alloys, then summarize the effect of ion irradiation on microstructural evolution, mechanical and corrosion properties, and their relationships. The microstructure components consist of dislocation loops, second phase precipitates, and gas bubbles. The microstructure parameters are also included such as domain size and microstrain determined by X-ray diffraction and the S-parameter determined by positron annihilation. Understanding the relationships of microstructure and properties is necessary for developing new advanced materials with higher irradiation tolerance.

• 연구논문집
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• s.32
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• pp.77-84
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• 2002

A martensitic precipitation hardening stainless steel, 17-4PH has been widely used in the aircraft, chemical and nuclear industries for long time, owing to the excellent mechanical properties with corrosion resistance that can be achieved by simple heat treatment. The microstructure and mechanical properties of the 17-4PH stainless steel cast parts for aircraft, such as impeller, are largely affected by heat treatment condition. But the database of heat treatment has not been clearly established in the domestic investment casting industries because the domestic aerospace, industry lags behind the advanced countries. In this study, the microstructural evolution and mechanical properties of cast 17-4PH stainless steel depending on the heat treatment conditions and aging at $400^{\circ}C$ were investigated.

• Korean Journal of Metals and Materials
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• v.48 no.10
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• pp.942-950
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• 2010

The microstructure and mechanical properties of a Cu-Fe-P copper alloy processed by differential speed rolling (DSR) were investigated in detail. The copper alloy, with a thickness of 3 mm, was rolled to 50% reduction at ambient temperature without lubrication with a differential speed ratio of 2.0:1 and then annealed for 0.5h at various temperatures ranging from 100 to $800^{\circ}C$. Conventional rolling was performed under the same rolling conditions for comparison. The shear strain introduced by the conventional rolling process showed positive values at the positions of the upper roll side and negative values at the positions of the lower roll side. However, the result was zero or positive values at all positions for samples rolled by DSR. The effects of DSR on the microstructure and mechanical properties of the as-rolled and subsequently annealed samples are discussed.

• Journal of Korea Foundry Society
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• v.16 no.6
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• pp.537-549
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• 1996

This study aims at investigating the correlation of microstructure and mechanical properties of the AZ91 Mg/Al borate whisker composites fabricated by squeeze csting technique with a variation of applied pressure. Microstructure observation and in-situ fracture tests were conducted on the composites to identify the microfracture process. Detailed microstructural analyses indicated that the grain refinement could be achieved with applied pressure and the little change in volume fraction on reinforcing whiskers could be carried out. It was also found clearly from in-situ observation of crack initiation and propagation that in the composite processed by the lower applied pressure, microcracks were initiated earily at whisker/matrix interfaces, thereby resulting in the drop in strength. In the composite processed by the higher applied pressure, on the other hand, planar slip lines were well developed in the matrix, and then propagated through whiskers without whisker/matrix decohesion. Thus, the effect of the applied pressure on microstructure and mechanical properties can be explained by grain refinement, increased amounts of reinforcements, and improvement of whisker/matrix interfacial strength as the applied pressure in increased.

• Transactions of Materials Processing
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• v.27 no.1
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• pp.12-17
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• 2018

This paper outlines the research findings on the microstructure and mechanical properties of AZ31 Mg alloy fabricated by differential speed rolling (DSR) with respect to processing variables such as temperature, roll speed ratio (RSR), and deformation route. The resultant microstructure of the sample, deformed by 2-pass DSRs at 473 K, comprised finer grains with more uniform distribution than those at 573 and 623 K. This was due to active recrystallization, which was expected to appear during DSR at temperatures higher than 573 K. When the sample was deformed via DSR with RSR of 1:4 for the upper and lower rolls at 453 K, the values of yield and ultimate tensile strength were observed to be higher than their counterpart with RSR of 1:1. The application of sample rotation around the longitudinal axis would give rise to an excellent combination of tension strength (~330 MPa) and ductility (~20 %) at ambient temperatures. This is discussed based on its uniform fine grained structure and the softening of basal texture.