• Journal of Powder Materials
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• v.17 no.1
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• pp.23-28
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• 2010

HDDR treated anisotropic Nd-Fe-B powders have been widely used for the sheet motors and the sunroof motors of hybrid or electric vehicles, due to their excellent magnetic properties. Microstructural alignment of HDDR treated powders are mostly depending on the hydrogen reaction in disproportionation step, so the specific method to control hydrogenation reaction is required for improving magnetic properties. In disproportionation step, hydrogenation pressure and reaction time were controlled in the range of 0.15~1.0 atm for 15~180 min in order to control the micorstructural alignment of $Nd_2Fe_{14}B$ phase and, at the same time, to improve remanence of HDDR treated magnet powders. In this study, we could obtain a well aligned anisotropic Nd-Fe-B-Ga-Nb alloy powder having high remanence of 12 kG by reducing hydrogen pressure down to 0.3 atm in disproportionation step.

• Journal of the Korean Society for Heat Treatment
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• v.29 no.5
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• pp.220-226
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• 2016

The mechanical properties of Ti-6Al-4V can be improved by microstructural control through the heat treatment in ${\alpha}+{\beta}$ region. The heat treatment was carried out with a variety of heat treatment temperatures and holding times to find the optimized heat treatment conditions and it was analyzed by linking the microstructural characteristics and mechanical properties. The part of ${\beta}$ phase with $10{\pm}2wt%$ vanadium was transformed into ${\alpha}^{{\prime}{\prime}}$ martensite phase after quenched, so the hardness and tensile properties were decreased below $900^{\circ}C$. The higher the heat treatment temperature is, the smaller is the vanadium-rich region, which leads to transformation into hcp ${\alpha}^{\prime}$ martensite above $900^{\circ}C$. The hardness and tensile properties were improved due to the hard ${\alpha}^{\prime}$ martensite. As the holding times were longer, the hardness and tensile properties decreased below $900^{\circ}C$ because of the softening effect by the grain growth. When varying the holding times above $900^{\circ}C$, the change of mechanical properties was slight because the softening effect of grain growth and the strengthening effect of ${\alpha}^{\prime}$ phase were counteractive. Therefore, the best conditions of heat treatment, which is in the range of $920{\sim}960^{\circ}C$, 40 min, WQ, can effectively improve the mechanical properties of Ti-6Al-4V.

• Proceedings of the Korean Ceranic Society Conference
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• 2003.04a
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• pp.209.1-209
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• 2003

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2004.11a
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• pp.171-171
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• 2004

• Journal of the Korean Society for Heat Treatment
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• v.13 no.3
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• pp.183-191
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• 2000

• Journal of the Korean Ceramic Society
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• v.29 no.7
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• pp.533-538
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• 1992

Effect of Li2O.4B2O frit on the microstructural and thermal expansion behaviour of $\beta$-spodumene ceramics was investigated. With 4.0~8.0 wt.% frit addition, sintering temperature range was enlarged and densification was enhanced through liquid phase sintering. As the amount of frit addition was increased, thermal expansion coefficient was increased to 1.72$\times$10-6$^{\circ}C$-1 of its highest value, which indicated that the increment of thermal expansion coefficient due to the second phase was constrained.

• The Korean Journal of Ceramics
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• v.1 no.1
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• pp.45-54
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• 1995

Four kinds of silicon nitride based ceramic materials have been hot pressed. Effect of the sintering additives on the phase transformation, microstructural development and mechanical properties was investigated. While sintering under the same condition a big difference among the microstructures of the specimens, they appeared alike if sintered to have a similiar $\alpha$-$\beta$ phase ratio. The specimen of the stoichiometric $\alpha$-$\beta$ sialon composition showed very limited amount of the intergranular glassy phase and a significant degree of the residual stress. It exhibited almost no strength degradation up to $1300^{\circ}C$, and the strength of the specimen degraded more as its composition deviated from the stoichiometry.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1995.06a
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• pp.81-90
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• 1995

Age hardenable aluminum alloys show high specific strength, good thermal and electrical conductivity as well as lightness, and are typical aircraft materials. High fatigue strength and good resistancy against stress corrosion cracking are also important for aircraft aluminum alloys. Al alloy 7050 has been developed to meet the above mentioned requirements and the use of this alloy as forged aircraft part becomes more important. However, forged 7050 parts showed undersirable structures such as severe local grain coarsening in surface area and unproper metal flow that is degrading mechanical properties. In this paper, microstructural aspects of die forging in the Al alloy 7050 are investigated. Also suggested are the optimal forging conditions for microstructural control of Al alloy 7050.

• 연구논문집
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• s.26
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• pp.113-120
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• 1996

Age hardenable aluminium alloys show high specific strength, good thermal and electrical conductivity as well as lightness, and are typical aircraft materials. High fatigue strength and good resistancy against stress corrosion cracking are also important for aircraft aluminium alloys. Al alloy 7050 has been developed to meet the above mentioned requirements and the use of this alloy as forged aircraft part becomes more important. However, forged 7050 parts showed undersiable structures such as severe local grain coarsening in surface area and unproper metal flow that is degrading mechanical properties. In this paper, microstructural aspects of die forging in the Al alloy 7050 are investigated. Also suggested are the optimal forging conditions for microstructural control of Al alloy 7050.

• Journal of the Korean Ceramic Society
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• v.29 no.8
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• pp.646-650
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• 1992

Effect of Li2O.4B2O3 frit addition on microstructural and thermal expansion behaviour of the $\beta$-spodumene ceramics made from kaolinite was investigated. With 2.0~4.0 wt% frit addition, the densification by liquid phase sintering caused low water absorption below 3% and enhancement of beding strength. As the amount of frit addition was increased, thermal expansion coefficient was increased to large scale, but in 2 wt% frit addition, its thermal expansion coefficient was constrained to 1.92$\times$10-6$^{\circ}C$-1.