• 제목/요약/키워드: Micro-sized

검색결과 405건 처리시간 0.029초

수계분산매체에서 나노 $CeO_2$ 입자의 계면전위 거동 (Surface Potential Behavior of Nano $CeO_2$ Particles in Aqueous Media)

  • 이태원;백운규;최성철;이상훈;임형섭;김철진
    • 한국세라믹학회지
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    • 제37권7호
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    • pp.721-725
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    • 2000
  • In this study, the dispersion stability of nano-sized CeO2 particles, synthesized by hydrothermal method in aqueous was evaluated from observing the surface potential behavior of CeO2 particle synthesized by solid state reaction. The isoelectric point(IEP) of nano-sized CeO2 synthesized by hydrothermal synthesis was found to be pH 9 contrary to the isoelectric point of micro-sized CeO2 synthesized by solid state reaction at pH 6.7. IEP was shifted to pH 2.0 as the addition of D-3019 from 0.1 to 1.0 wt%. The surface potential of CeO2 particles synthesized by hydrothermal synthesis was reduced as the addition of B-1001 used as a binder without change of IEP because the absorption of B-1001 polymer on the CeO2 particles shifted the shear plane of CeO2 particles outward away from the surface. This surface potential behavior was well correlated with the dispersion stability of slurry.

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A Simple Prediction Model for PCC Voltage Variation Due to Active Power Fluctuation of a Grid Connected Wind Turbine

  • Kim, Sang-Jin;Seong, Se-Jin
    • Journal of Power Electronics
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    • 제9권1호
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    • pp.85-92
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    • 2009
  • This paper studies the method to predict voltage variation that can be presented in the case of operating a small-sized wind turbine in grid connection to the isolated small-sized power system. In order to do this, it makes up the simplified simulation model of the existing power plant connected to the isolated system, load, transformer, and wind turbine on the basis of PSCAD/EMTDC and compares them with the operating characteristics of the actual established wind turbine. In particular, it suggests a simplified model formed with equivalent impedance of the power system network including the load to analytically predict voltage variation at the connected point. It also confirms that the voltage variation amount calculated by the suggested method accords well with both simulation and actually measured data. The results can be utilized as a tool to ensure security and reliability in the stage of system design and preliminary investigation of a small-sized grid connected wind turbine.

Characteristic X-ray Spectrum Analysis of Micro-Sized SiC

  • Miyoshi, Noriko;Mao, Weiji;Era, Hidenori;Shimozaki, Toshitada;Shinozaki, Nobuya
    • Applied Microscopy
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    • 제46권1호
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    • pp.27-31
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    • 2016
  • It has been investigated what kind of characteristic X-ray in electron probe micro-analyzer (EPMA) is effective for the determination of compounds of Si series materials. After comparing the characteristic X-rays among the primary and secondary lines in $K_{\alpha}$ and $K_{\beta}$ obtained from the Si series standard samples, it was found that the secondary line of $K_{\alpha}$ exhibited the most informative spectrum although the intensity was considerably weak. As a result of analyzing the spectrum shapes of the Si series standard samples, the spectrum shape of the secondary line of $K_{\alpha}$ for SiC was different from those for other Si compounds. To grasp the characteristics of the shape, a line was perpendicularly drawn from the peak top to base line in order to divide a spectrum into two areas. The area ratio of right to left was defined to call as the asymmetry index here. As a result, the asymmetry index value of the SiC was greater than one, while those of other Si compounds were less than one. It was found from the EPMA analysis that identification of SiC became successful to distinguish from other Si compounds and this method was applicable for micro-sized compounds in a practical composite material.

Design and Contact Force Control of a Flip Chip Mounting Head system

  • Kim, Kyoung-Jun;Shim, Jae-Hong
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2003년도 ICCAS
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    • pp.1060-1065
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    • 2003
  • This paper contributes to development of a new chip mounting head system for flip chip. Recently, the LDM(Linear DC Motor) has been widely used, because it has particular merits than the rotary type motors. In this paper, we proposed a macro/micro positioning system for force control of a chip mounting system. In the proposed macro/micro system, the macro actuator provide the system with a gross motion while the micro device yields fine tuned motion to reduce the harmful impact force that occurs between very small sized electronic parts and PCB surface. In order to prove the effectiveness of the proposed macro/micro chip mounting system, we compared the proposed chip mounting head with the conventional chip mounting head equipped with a macro actuator only. A series of experiments were executed under the mounting conditions of various access velocities and PCB stiffness. As a result of this study, a satisfactory voice coil actuator as the micro actuator has been developed, and its performance meet well the specifications desired for the design of the chip mounting head system and show good correspondence between theoretical analysis and experimental results.

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STUDIES FOR THE CHARACTER OF NANO-SIZED $TiO_2$ PARTICLE SYNTHESIZED BY MICRO-EMULSION METHOD AND GOLD-DEPOSITED $TiO_2$ PARTICLE

  • Jhun, Hyun-Pyo;Park, Jae-Kiel;Lee, Kyoung-Chul;Park, Jae-Eon
    • 대한화장품학회지
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    • 제22권2호
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    • pp.52-69
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    • 1996
  • Nano-Sized TiO$_2$ particles with diameter between 2 and 5 nm are synthesized in Water/Triton X-100/n-Hexane microemulsion. Particles show the amorphous structure and partially hydroxide form. The optical absorbance of particles appears at 250nm and band edge at 340nm. Gold metal is deposited on the surface of TiO$_2$ particles by reduction reaction of Au(III) ion with sodium hypophosphite. The size of gold-deposited particles is 20nm, and the optical absorbance appears at 270nm and at 550nm. So particles show the red color. The dense precipitation is formed by aggregation in the TiO$_2$ nano-sized particles of about 5nm size. But the bulky precipitation is formed by agglomeration phenomena in the gold-deposited particles of 20nm size. And also gold-deposited particles is easily dispersed by being re-dispersed in PEG/Water solution. This study has compared those things measuring the SPF characteristics of the cosmetics made of the synthesized particles. If the particle size is controlled appropriately, then the SPF value will be higher, or more colorless cosmetics will be made.

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Stability/instability of the graphene reinforced nano-sized shell employing modified couple stress model

  • Yao, Zhigang;Xie, Hui;Wang, Yulei
    • Wind and Structures
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    • 제32권1호
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    • pp.31-46
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    • 2021
  • The current research deals with, stability/instability and cylindrical composite nano-scaled shell's resonance frequency filled by graphene nanoplatelets (GPLs) under various thermal conditions (linear and nonlinear thermal loadings). The piece-wise GPL-reinforced composites' material properties change through the orientation of cylindrical nano-sized shell's thickness as the temperature changes. Moreover, in order to model all layers' efficient material properties, nanomechanical model of Halpin-Tsai has been applied. A functionally modified couple stress model (FMCS) has been employed to simulate GPLRC nano-sized shell's size dependency. It is firstly investigated that reaching the relative frequency's percentage to 30% would lead to thermal buckling. The current study's originality is in considering the multifarious influences of GPLRC and thermal loading along with FMCS on GPLRC nano-scaled shell's resonance frequencies, relative frequency, dynamic deflection, and thermal buckling. Furthermore, Hamilton's principle is applied to achieve boundary conditions (BCs) and governing motion equations, while the mentioned equations are solved using an analytical approach. The outcomes reveal that a range of distributions in temperature and other mechanical and configurational characteristics have an essential contribution in GPLRC cylindrical nano-scaled shell's relative frequency change, resonance frequency, stability/instability, and dynamic deflection. The current study's outcomes are practical assumptions for materials science designing, nano-mechanical, and micromechanical systems such as micro-sized sensors and actuators.

기능성 나노 제올라이트가 분산된 친수성 복합막 제조 및 탈수 투과증발 특성 연구 (Characteristic of Water Pervaporation Using Hydrophilic Composite Membrane Containing Functional Nano Sized NaA zeolites)

  • 오덕규;이용택
    • Korean Chemical Engineering Research
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    • 제51권1호
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    • pp.98-105
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    • 2013
  • NaA 제올라이트 입자들을 폴리비닐알콜(PVA) 고분자에 분산시키어 복합막을 제조하였다. 나노 크기의 NaA 입자들을 연구실에서 합성하였으며, 그 평균 크기는 대략 60 nm이었다. 제조한 혼합 매트릭스 분리막을 이용하여 0.01 부터 0.05 몰분율 농도 범위의 에탄올 수용액으로부터 물을 선택적으로 분리하고자 공급 수용액의 농도 및 첨가한 제올라이트 함유량을 0 에서 5 wt% 내에서 조절하면서 투과증발 특성을 고찰하였다. 상호 비교 목적으로 평균 $5{\mu}m$ 크기의 NaA 입자들을 분산시킨 복합막의 투과 증발 특성도 함께 조사하였다. 공급된 에탄올 농도가 0.01 몰분율인 실험조건에서 분리막 내의 나노 NaA 입자들의 첨가량이 0 wt%에서 5 wt%로 증가함에 따라 물의 투과플럭스는 $600g/m^2/hr$에서 $2,000g/m^2/hr$로 크게 증가하였으며, 물 선택성은 1.5에서 7.9로 5배 이상 증가함을 알 수 있었다. 또한, 나노 입자들이 분산된 분리막을 통한 물 투과플럭스는 마이크로 입자들이 분산된 분리막을 통한 물 투과플럭스보다 전반적으로 약 15% 이상 증가한 반면, 선택도는 약 5% 정도 증가한 것으로 관찰되었다. 따라서, 마이크로 입자보다는 나노 입자의 혼합으로 인한 투과플럭스나 선택도에 미치는 영향이 매우 크기 때문에 나노 입자가 더 효율적이라고 사료된다.

Comparison of teratogenecity induced by nano- and micro-sized particles of zinc oxide in cultured mouse embryos

  • Jung, A Young;Jung, Ki Youn;Lin, Chunmei;Yon, Jung-Min;Lee, Jong Geol;Lee, Beom Jun;Yun, Young Won;Nam, Sang-Yoon
    • 대한수의학회지
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    • 제55권2호
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    • pp.133-139
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    • 2015
  • The increasing uses of zinc oxide nanoparticles (nZnO) in industrial and personal care products raise possible danger of using nZnO in human. To determine whether ZnO induces size-dependent anomalies during embryonic organogenesis, mouse embryos on embryonic day 8.5 were cultured for 2 days under 50, 100, and $150{\mu}g$ of nZnO (< 100 nm) or micro-sized ZnO (mZnO; $80{\pm}25{\mu}m$), after which the morphological changes, cumulative quantity of Zn particles, and expressions of antioxidant and apoptotic genes were investigated. Although embryos exposed to $50{\mu}g$ of ZnO exhibited no defects on organogenesis, embryos exposed to over $100{\mu}g$ of ZnO showed increasing anomalies. Embryos treated with $150{\mu}g$ of nZnO revealed significant changes in Zn absorption level and morphological parameters including yolk sac diameter, head length, flexion, hindbrain, forebrain, branchial bars, maxillary process, mandibular process, forelimb, and total score compared to the same dose of mZnO-treated embryos. Furthermore, CuZn-superoxide dismutase, cytoplasmic glutathione peroxidase (GPx) and phospholipid hydroperoxidase GPx mRNA levels were significantly decreased, but caspase-3 mRNA level was greatly increased in nZnO-treated embryos as compared to normal control embryos. These findings indicate that nZnO has severer teratogenic effects than mZnO in developing embryos.