• Title/Summary/Keyword: Micro-particles

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Micro-morphological Features of Liquid Urea-Formaldehyde Resins during Curing Process at Different Levels of Hardener and Curing Time Assessed by Transmission Electron Microscopy

  • Nuryawan, Arif;Park, Byung-Dae
    • Current Research on Agriculture and Life Sciences
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    • v.32 no.3
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    • pp.125-130
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    • 2014
  • This study used transmission electron microscopy (TEM) to investigate the micro-morphological features of two formaldehyde to urea (F/U) mole ratio liquid urea-formaldehyde (UF) resins with three hardener levels as a function of the curing time. The micro-morphological features of the liquid UF resins were characterized after different curing times. As a result, the TEM examination revealed the presence of globular/nodular structures in both liquid UF resins, while spherical particles were only visible in the low F/U mole ratio resins. The high F/U mole ratio liquid UF resins also showed extensive particle coalescence after adding the hardener, along with the appearance of complex filamentous networks. When the resins were cured with a higher amount of hardener and longer curing time, the spherical particles disappeared. For the low mole UF resins, the particles tended to coalesce with a higher amount of hardener and longer curing time, although discrete spherical particles were still observed in some regions. This is the first report on the distinct features of the crystal structures in low F/U mole ratio UF resins cured with 5% hardener and after 0.5 h of curing time. In conclusion, the present results indicate that the crystal structures of low F/U mole ratio UF resins are formed during the curing process.

Micro- PIV Measurements of Microchannel Flows and Related Problems (마이크로 채널 내부 유동의 Micro-PIV측정과 제반 문제점)

  • Lee Sang-Joon;Kim Guk-bae
    • 한국가시화정보학회:학술대회논문집
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    • 2002.04a
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    • pp.79-84
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    • 2002
  • Most microfluidic devices such as heat sinks for cooling micro-chips, DNA chip, Lab-On-Chip, and micro pumps etc. have microchannels of various size. Therefore, the design of practical microfluidics demands detail information on flow structure inside the microchannels. However, detail velocity field measurements are rare and difficult to carry out. In addition, as the microfluidics expands, accurate understanding of microscale transport phenomena becomes very important. In this research, micro-PIV system was employed to measure the velocity fields of flow inside a micro-channel. We carried out PIV measurements for several microchannels with varying channels width, inlet and outlet shape, filters, CCD camera and ICCD camera, etc. For effective composition of micro-PIV system, first of all, it is essential to understand optics related with micro-imaging of particles and the particle dynamics encountered in micro-scale channel flows. In addition, it is necessary to find the optimal condition for given experimental environment and? micro-scale flow to be investigated. The problems encountered in measuring velocity field of micro-channel flows are discussed in this paper.

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Numerical Analysis Study on Micro-plastic Particle behavior According to the Shape of Cyclone Separator (Cyclone separator의 형상에 따른 미세플라스틱 입자 거동 수치해석 연구)

  • Insun Kang;Wonjun Seo;Dongho Yu;Yeongshik Kim;Hyeungchul Kim;Seokyeon Im
    • Tribology and Lubricants
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    • v.40 no.2
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    • pp.61-66
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    • 2024
  • Micro-plastics are synthetic high-differentiation chemicals of less than 5mm in size, and are deposited not only on the sea surface but also on the coast. If these micro-plastics are not properly separated from the sand, they can threaten marine ecosystems. Thus, in the present study, we aimed to apply cyclone separator to the micro-plastic retrieval in order to predict the movement of particles according to the formation of the cyclone separator by applying the centrifugal force of the particle in accordance with the rotational movement of the air. The cyclone separator has three shapes, the first one is a typical interconnected cyclone separator. The second is the horn form, except for the cylinder in a regular cyclone separator, and the third is a form that increases the horn's height twice in the second. The numerical analysis simulation of the Cyclone separator used the Fluent software package. The output speed of the Cyclone separator was 5 to 13m/s at 1m/s intervals. The simulated particles include sand, Styrofoam, PET, PP, and PU. Sand particles are assigned a fixed diameter of 2mm, while other particles have a diameter of 3mm. As a result of the analysis, the first form was not separated from plastic. The Styrofoam separation efficiency in the second showed its highest efficiency at 72.7% at 7m/s, and the efficiency decreased after 12m/s as the sand particles were mixed into the plastic attachment location. In the third form, the separation efficiency of Styrofoam at 12m/s was highest at 67.9%.

Nano-scale Precision Polishing Characteristics using a Micro Quill and Magnetic Chain Structure (미세공구와 자기체인구조를 이용한 초정밀 폴리싱 특성)

  • 박성준;안병운;이상조
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.8
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    • pp.34-42
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    • 2004
  • A new polishing technique for three dimensional micro/meso-scale parts is suggested using a micro quill and a magnetic chain structure. The principle of this method is to polish the target surface with the collected magnetic brushes at a micro tool by the non-uniform magnetic field generated around the tool. In a typical magnetic abrasive finishing process magnetic particles and abrasive particles are unbonded each other. But, to finish the three dimensional small parts bonded magnetic abrasive have to be used. Bonded magnetic abrasives are made from direct bonding, and their polishing characteristics are also examined. Alumina, silicon carbide and diamond micro powders are used as abrasives. Base metal matrix is carbonyl iron powder. It is found that bonded magnetic abrasives are superior to unbonded one by experiment. finally, the polished surface roughness is evaluated by atomic force microscope.

Surface polishing of Micro channel using Magneto-Rheological fluid (MR유체를 이용한 미세 채널구조물의 표면연마)

  • 이승환;김욱배;민병권;이상조
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.1873-1876
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    • 2003
  • Magneto-rheological polishing is a new technology used in precision polishing. It utilizes magneto-rheological fluid. nonmagnetic polishing abrasive, aqueous carrier fluids in magnetic field to remove material from a part surface. Silicon micro channel as work piece is fixed in the slurry which is made of MR fluid and CeO$_2$(10 vol%) abrasive particles. And permanent magnet rotate in the slurry to transfers magnetic force to abrasive particles by increasing yield strength of MR fluid. so, the obtained bottom surface roughness of micro channel by experiment reduced to Ra 0.010 $\mu\textrm{m}$ Rmax 0.103 $\mu\textrm{m}$ and finwall surface roughness of micro channel reduced to Ra 0.018 $\mu\textrm{m}$ Rmax 0.468 $\mu\textrm{m}$. At optimum conditions of variables, the workpiece as silicon micro channel have about 24 times smaller surface roughness than before polishing.

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Flow Properties of Micro Column Packed with Perfusive Particles (투과성 입자로 이루어진 미세 칼럼의 유동 특성)

  • Kim, Duck-Jong;Hwang, Yun-Wook;Park, Sang-Jin;Heo, Pil-Woo;Yoon, Eui-Soo
    • 유체기계공업학회:학술대회논문집
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    • 2005.12a
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    • pp.89-93
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    • 2005
  • In this work, perfusive particles are used to form a micro column in a microfluidic chip and flow properties of the micro column are investigated. The packing flow velocity and the column/particle size ratio are shown to be important parameters affecting the packing density of the micro column. Experimental results show that the effect of the column/particle size ratio on the flow resistance of the micro column is negligible. This contrasts with previous works on the effect of the column/particle size ratio on the total pressure drop across the column.

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전기 저항법을 이용한 Micro Particle Counter Micro Fluidic Device 개발

  • Lee Jun;Yun Deok-Won;Chae Ho-Cheol;Han Chang-Su
    • Proceedings of the Korean Society Of Semiconductor Equipment Technology
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    • 2005.05a
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    • pp.134-138
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    • 2005
  • Recently many researches related with biotechnology are processed and it is the situation that research about micro fluidic devices is active. Micro fluidic devices has been one of the most widely used devices for the analysis in biotechnology because they have many advantages, flexibility, transparency, thermal and electrical stability, nontoxic, etc. In this study, micro fluidic device with PDMS is developed for particle counter which separates a small quantity of particles, The principle of micro particle counter is electrical-impedance method, and it was also applied hydrodynamic flow focusing. It is more efficient method to analyzing particles furthermore it can be applied to cell count ins for biotechnology.

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Physicochemical Characteristics of Single Asian Dust Storm Particles

  • Ma, Chang-Jin;Mikio kasahara;Hwang, kyung-Chul;Park, Kum-Chan;Park, Seong-Boo;Lee, Jeong-Joo
    • Journal of Korean Society for Atmospheric Environment
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    • v.16 no.E
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    • pp.29-38
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    • 2000
  • For the detailed characterization of atmospheric aerosol, the analysis of single particle is highly valuable. In this study, to investigate the characteristics of single Asian dust storm particles, scanning electron microscope(SEM) coupled with and energy dispersive X-ray microanalyzer(EDX) and micro-PIXE were applied. Sampling was performed at Kyoto University located in Kyoto, Japan, in spring of 1999. Mass concentration during Asian dust storm events was higher roughly 3∼5 times than measured in the season of the highest concentration. Single particles were generally sharp-edged and irregular in shape and contained mostly crustal elements. Significant amount of S in coarse fraction was detected in individual particles. A large particles in coarse fraction existed as the mixture of soil components and S. A good agreement between the result of SEM-EDX analysis and that iof micro-PIXE analysis was obtained in this study.

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Combustion Modeling of Nano/Micro Aluminum Particle Mixture (나노-마이크로 알루미늄 혼합 입자의 공기와의 연소 모델링)

  • Yoon, Shi-Kyung;Shin, Jun-Su;Sung, Hong-Gye
    • Journal of the Korean Society of Propulsion Engineers
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    • v.15 no.6
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    • pp.15-25
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    • 2011
  • One dimensional combustion modeling of aluminum combustion behavior is proposed. Combustion model is assumed that region consists as follows ; preheat, reaction, post reaction region. Flame speed as a function of particle size, equivalence ratio for unitary particles and fraction ratio of micro to nano particle size for binary particles were investigated for lean burn condition at 1 atm. Results were compared with experimental data. For unitary particles, flame speed increase as particle size decreases, but opposite trend with equivalence ratio. For binary particles, flame speed increases proportionally as nano particle fraction increases. For flame structure, separated or overlapping flames are observed, depending on the fraction of nano sized particles.

Interpretation of the Chemical Transformation of Individual Asian Dust Particles Collected on the Western Coast of Korean Peninsula

  • Ma, Chang-Jin;Kim, Jong-Ho;Kim, Ki-Hyun
    • Asian Journal of Atmospheric Environment
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    • v.6 no.1
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    • pp.14-22
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    • 2012
  • This paper is focused on the comprehensive and detailed interpretation for the chemical transformation of individual Asian dust (hereafter called "AD") particles during long-range transport from source regions to receptor area. A multi-stage particle sampler was operated at a ground-based site in Taean, Korea directly exposed to the outflow of air masses from China during AD period in April 2003. Both quantitative and qualitative analyses for size-classified individual particles were carried out by a microbeam X-ray fluorescence (XRF) method and a microbeam Particle Induced X-ray Emission (micro-PIXE), respectively. Among major characteristic elements, the elemental masses of soil derived components, sulfur, and chloride varied as a function of particle size showing the monomodal maximum with a steeply increasing at 3.3-4.7 ${\mu}m$ particle size. Although the details on chemical composition of AD particle collected on a straight line from source area to our ground-based site are needed, a large amount of Cl coexisted in and/or on AD particles suggests that AD particles collected in the present study might be actively engaged in chemical transformation by sea-salt and other Cl containing pollutants emitted from the China's domestic sources. Through the statistical analyses it was possible to classify individual AD particles into six distinct groups. The internally mixed AD particles with Cl, which has various sources (e.g., sea-salt, coal combustion origin HCl, gaseous HCl derived from the adsorption of acids to sea-salt, and Cl containing man-made particles) were thoroughly fractionated by the elemental spectra drivened by the double detector system of micro-PIXE.