• Title/Summary/Keyword: Micro strength

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Effect of Curing Conditions on the Strength of Fly-Ash Based Geopolymer (양생조건이 플라이애쉬 기반 지오폴리머 강도에 미치는 영향)

  • Cho, Young-Keun;Moon, Gyu-Don;La, Jung-Min;Jung, Sang-Hwa
    • Journal of the Korea Concrete Institute
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    • v.26 no.4
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    • pp.449-456
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    • 2014
  • Material properties of geopolymer, whose the reaction is very complicated, have been influenced by chemical compositions and particle size distributions of fly ash, concentrations and types of alkali-activators and curing conditions such as temperatures and time. In this research, experiments with several variables such as curing temperatures, preset prior to the high temperature curing and high temperatures have been conducted in order to evaluate to investigate effects on the compressive strengths of geopolymer caused by curing condition. Experiment results were evaluated with compressive strengths and micro-structures such as SEM and MIP of geopolymer pastes. As a result, as higher curing temperature or longer preset time were applied to the pastes, higher compressive strengths were observed. However, compressive strengths of geopolymer pastes declined due to increases in macropores (>50 nm) under high temperatures elapsed after 24 hours. In this sense, it can be considered that strengths and microstructures of geopolymers depends on curing temperature and time.

Properties of $CaO-P_2O_5-SiO_2$ Glasses ($CaO-P_2O_5-SiO_2$계 유리의 물성)

  • 조정식;김철영
    • Journal of the Korean Ceramic Society
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    • v.30 no.4
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    • pp.289-298
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    • 1993
  • Properties in terms of the variation of the glass compositions, which were density (p), molar volume(Vm), atom/ion packing density (Dp), refractive index (nD), transformation temperature (Tg), dilatometric softening point (Td), thermal expansion coefficient (α), Young's modulus (E), and knoop hardness (KHN) were investigated in CaO-SiO2 glasses and CaO-P2O5-SiO2 glasses containing less than 10mole% of P2O5. Those properties were measured by density measurement kit, Abbe refractometer, dilatometer, ultrasonic pulse echo equipment, and micro hardness tester. When CaO content was increased in CaO-SiO2 glasses, p, Dp, nD, Tg, Td, α, E and KHN were increased, while Vm was decreased. When P2O5 was added to the CaO-SiO2 glasses with constant CaO/SiO2 ratio as 1.07, p, Dp, nD, Tg, Td, α, E and KHN were decreased, while Vm was increased. When the amount of P2O5 in glasses was kept constant, the changes of the properties with variation of CaO content in the CaO-P2O5-SiO2 glasses were very similar to those of CaO-SiO2 glasses. These phenomena could be explained by the structural role of P2O5 in the CaO-P2O5-SiO2 glasses, which was polymerization of siicate structures and resulted in [PO4] monomer structure in glasses. Due to this structural characteristics, the bond strength and packing density were changed with compositions. Proportional relationships between 1) np and Dp, 2) Tg, Td, α and CaO content, 3) E and Vm-1, and 4) KHN and P2O5 content were evaluated in this investigation.

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Study on the Optimal Release Condition of Wafer Level Molding Process using Plasma Surface Treatment Method (플라즈마 표면처리 방법을 이용한 웨이퍼레벨 몰딩 공정용 기판의 최적 이형조건 도출)

  • Yeon, Simo;Park, Jeonho;Lee, Nukkyu;Park, Sukhee;Lee, Hyejin
    • Journal of Institute of Convergence Technology
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    • v.5 no.1
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    • pp.13-17
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    • 2015
  • In wafer level molding progress, the thermal releasing failure phenomenon is shown up as the important problem. This phenomenon can cause the problem including the warpage, crack of the molded wafer. The thermal releasing failure is due to the insufficiency of adhesion strength degradation of the molding tape. To solve this problem, we studied experimental method increasing the release property of the molding tape through the plasma surface treatment on the wafer substrate. In this research, the vacuum plasma treatment system is used for release property improvement of the molding tape and controls the operating condition of the hydrophilic($O_2$, 100kW, 10min) and hydrophobic($C_2F_6$, 200kW, 10min). In order to perform the peeling test for measuring the releasing force precisely, we remodel the micro scale material property evaluation system developed by Korea institute of industrial technology. In case of hydrophilic surface treatment on the wafer substrate, we can figure out the releasing property of molding tape increase. In order to grasp the effect that it reaches to the release property increase when repeating the hydrophilic treatment, we make an experiment with twice treatment and get the result to increase about 12%. We find out the hydrophilic surface treatment method using plasma can improve releasing property of molding tape in the wafer level molding process.

Study on Deformation of Miniature Metal Bellows in Cryocooler Following Temperature Change of Internal Gas (내부 기체의 온도 변화에 따른 극저온 냉각기용 소형 금속 벨로우즈의 변형에 관한 연구)

  • Lee, Seung Ha;Lee, Tae Won
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.4
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    • pp.429-435
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    • 2015
  • A bellows is an important temperature control component in a Joule-Thomson micro-cryocooler. It is designed using a very thin shell, and the inside of the bellows is filled with nitrogen gas. The bellows is made of a nickel-cobalt alloy that maintains its strength and elastic properties in a wide range of temperatures from cryogenic to $300^{\circ}C$. The pressure of the gas and the volume within the bellows vary according to the temperature of the gas. As a result, the bellows contracts or expands in the axial direction like a spring. To explore this phenomenon, the deformation of the bellows and its internal volume must be calculated iteratively under a modified pressure until the state equation of the gas is satisfied at a given temperature. In this paper, the modified Benedict-Webb-Rubin state equation is adopted to describe the temperature-volume-pressure relations of the gas. Experiments were performed to validate the proposed method. The results of a numerical analysis and the experiments showed good agreement.

Research on the technical development by the CAD/CAM System (CAD/CAM시스템을 이용한 기술개발에 대한 연구 (워엄기어 개발을 중심으로))

  • Jeong, Seon-Mo
    • Journal of the Korean Society for Precision Engineering
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    • v.3 no.3
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    • pp.40-71
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    • 1986
  • By developing a computer program for the systematic design of worm gears, the design formulae and tables of AGMA, JGMA, BS and DIN are analized and compared. The computer program can be used on micro-computers. According to the input data of the reduction ratio, the center distance. the driving torque and the material as design parameters, the program calculate the most efficient worm gear dimension. The variation of the design parameters and other empirical coefficients in case of resulting an inadequate design gear dimension can be easily modified throuth the way of interactive method between the user and the monitoring system of computer. A proposal of the standardization of worm gears was made in which a standard module according to the DIN 323 standard series number was applied. For the more exact and effective calculation of the stress concentration and the deformation of gear teeth, a computer program using the boundary element method is also developed. Even the strength of the special gear shape such as Niemann's "Cavex" gear can be calculated in a short CPU-time. The most effort of this study has been layed on the developing a computer program for the correction of a tooth profile and face width which is most important design factor for an exact and wide teeth contacts under loads, especially by great and wide gears. For this purpose were investigated the tooth stiffness, the mesh interferences and the kinematics and the dynamics of gear mesh. The deflection and the deformation of the gear shaft due to the loads acting on gear and shaft were aslo considered. Some examples have shown the sufficient good status of teeth contact in which the correction of the tooth profile and face width were accomplished due to the calculated results.d results.

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Carbon-Nanofiber Reinforced Cu Composites Prepared by Powder Metallurgy

  • Weidmueller, H.;Weissgaerber, T.;Hutsch, T.;Huenert, R.;Schmitt, T.;Mauthner, K.;Schulz-Harder, S.
    • Journal of Powder Materials
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    • v.13 no.5 s.58
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    • pp.321-326
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    • 2006
  • Electronic packaging involves interconnecting, powering, protecting, and cooling of semiconductor circuits fur the use in a variety of microelectronic applications. For microelectronic circuits, the main type of failure is thermal fatigue, owing to the different thermal expansion coefficients of semiconductor chips and packaging materials. Therefore, the search for matched coefficients of thermal expansion (CTE) of packaging materials in combination with a high thermal conductivity is the main task for developments of heat sink materials electronics, and good mechanical properties are also required. The aim of this work is to develop copper matrix composites reinforced with carbon nanofibers. The advantages of carbon nanofibers, especially the good thermal conductivity, are utlized to obtain a composite material having a thermal conductivity higher than 400 W/mK. The main challenge is to obtain a homogeneous dispersion of carbon nanofibers in copper. In this paper, a technology for obtaining a homogeneous mixture of copper and nanofibers will be presented and the microstructure and properties of consolidated samples will be discussed. In order to improve the bonding strength between copper and nanofibers, different alloying elements were added. The microstructure and the properties will be presented and the influence of interface modification will be discussed.

The Effect of Hydrogen on Mechanical Properties of Gas Pipeline Material: I Tensile property (가스배관 재료의 기계적특성에 미치는 수소의 영향: I 인장특성)

  • Kim, Woo-Sik;Jang, Jae-Il
    • Journal of the Korean Institute of Gas
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    • v.15 no.3
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    • pp.67-73
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    • 2011
  • One of the important topics to prepare the up-coming era of so-called ‘hydrogen economy’ is hydrogen transmission. Pipeline is conceivably the most economic way to consistently and safely transport a large amount of hydrogen over a long distance, which may be strongly requested in hydrogen economy era. As a good starting point for the purpose, one might wonder whether conventional API pipeline steels as designed for natural gas transmission can be used as the hydrogen pipeline materials or not. To answer the question, here we performed a series of micro-/nano-indentations together with tensile tests on the hydrogen-charged API X65, X70 and X100 steels having different strength level. In this paper, from the results of tensile tests, the hydrogen effects on the mechanical behavior in the API steels are systematically evaluated.

Methodological Implications of Everyday Life Research in Library and Information Science - With Special Reference to Current Research Trends - (문헌정보학에 있어서 일상생활 연구의 방법론적 함의 - 최근 연구동향을 중심으로 -)

  • Kim Jung-Gun;Chang Durk-Hyun
    • Journal of Korean Library and Information Science Society
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    • v.30 no.2
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    • pp.55-75
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    • 1999
  • Although the importance of research methodoogy in library and information science(LIS) has been widely recognized, LIS has been also criticized that current research methodology in the field maintains only the positivistic orientation. Researchers on the other hand, assert that US should be studied as a human study, a subjective approach based on a phenomenological perspective, since US has very much to do. with the 'human factor,' with subjectivity in the form of librarian, patron, and administrator. In this paper, a review of the published qualitative research in the field which try to generate theories from the subjects in their own everyday life situation, attempts to shed light on the implication of a new terrain of everyday life research to US. Theory of everyday life is generated by the subjects who are involved in the social relationship, using their own language. It is a theory which shows the logic of the real world in which the everyday man recognize, act and communicate. This includes the perceptions, feelings, and meanings members experience as well as the 'small world' they create in process. Everyday life research performed using qualitative research methods which have strength to investigate this micro-structure applied to the field of library and information science, may bring enrichment to the library and information science research.

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Design Validation through Analysis of Concrete Modular Road Behavior under Static Axial Loads (콘크리트 모듈러 도로 축하중 거동 분석을 통한 설계 타당성 검증)

  • Nam, Jeong-Hee;Kim, Woo Seok;Kim, Ki Hyun;Kim, Yeon Bok
    • International Journal of Highway Engineering
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    • v.17 no.6
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    • pp.37-45
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    • 2015
  • PURPOSES : The purpose of this study is to validate the design criteria of the concrete modular road system, which is a new semi-bridge-type concept road, through a comparison of numerical analysis results and actual loading test results under static axial loads. METHODS : To design the semi-bridge-type modular road, both the bridge design code and the concrete structural design code were adopted. The standard truck load (KL-510) was applied as the major traffic vehicle for the design loading condition. The dimension of the modular slab was designed in consideration of self-weight, axial load, environmental load, and combined loads, with ultimate limit state coefficients. The ANSYS APDL (2010) program was used for case studies of center and edge loading, and the analysis results were compared with the actual mock-up test results. RESULTS : A full-scale mock-up test was successfully conducted. The maximum longitudinal steel strains were measured as about 35 and 83.5 micro-strain (within elastic range) at center and edge loading locations, respectively, under a 100 kN dual-wheel loading condition by accelerating pavement tester. CONCLUSIONS : Based on the results of the comparison between the numerical analysis and the full-scale test, the maximum converted stress range at the edge location is 32~51% of the required standard flexural strength under the two times over-weight loading condition. In the case of edge loading, the maximum converted stresses from the Westergaard equation, the ANSYS APDL analysis, and the mock-up test are 1.95, 1.7, and 2.3 times of that of the center loading case, respectively. The primary reason for this difference is related to the assumption of the boundary conditions of the vertical connection between the slab module and the crossbeam module. Even though more research is required to fully define the boundary conditions, the proposed design criteria for the concrete modular road finally seems to be reasonable.

The Influence of W Addition on Cube Textured Ni Substrates for YBCO Coated Conductor (양축 정렬된 Ni 기판의 특성에 미치는 W 첨가의 효과)

  • Kim Kyu Tae;Lim Jun Hyung;Kim Jung Ho;Jang Seok Hern;Kim Ho-Jin;Joo Jinho;Kim Chan-Joong;Song Kyu Jung;Shin Hyung Sub
    • Progress in Superconductivity
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    • v.6 no.1
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    • pp.64-68
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    • 2004
  • We fabricated cube-textured Ni and Ni-W alloy substrates for coated conductors and characterized the effects of W addition on microstructure, mechanical strength, and magnetic properties of the substrate. Pure Ni and Ni-(2, 3, 5at.%)W alloys were prepared by plasma arc melting, heavily cold rolled and then annealed at various temperatures of $600-1300^{\circ}C$. The texture was evaluated by pole-figure and orientation distribution function (ODF) analysis. Mechanical properties were investigated by micro Vickers hardness and tension test. Ferromagnetism of the substrate was measured by physical property measurement system (PPMS). It was observed that Ni-W substrates had sharp cube texture, and the full-width at half-maximums (FWHMs) of in-plane texture was $^{\circ}$-5.57$4.42^{\circ}$, which is better than that of pure Ni substrate. In addition cube texture of Ni-W substrates was retained at higher temperature up to $1300^{\circ}C$. Microstructural observation showed that the Ni-W substrates had fine grain size and higher mechanical properties than the pure Ni substrate. These improvements are probably due to strengthening mechanisms such as solid solution hardening and/or grain size strengthening. PPMS analysis showed that addition of W effectively reduced saturation magnetization in applied magnetic field and Curie temperature.

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