• Title/Summary/Keyword: Micro strength

Search Result 1,212, Processing Time 0.036 seconds

DIFFERENCE IN BOND STRENGTH ACCORDING TO FILLING TECHNIQUES AND CAVITY WALLS IN BOX-TYPE OCCLUSAL COMPOSITE RESIN RESTORATION (박스 형태의 복합레진 수복시 충전법 및 와동벽에 따른 결합력 차이에 관한 연구)

  • Ko, Eun-Joo;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
    • /
    • v.34 no.4
    • /
    • pp.350-355
    • /
    • 2009
  • Bond strength depends on characteristics of bonding surface and restorative technique. The majority of studies dealing with dentin bond strength were carried out on flat bonding surface, therefore, difference of bond strength between axial wall and pulpal wall is not clear yet. This study evaluated bonding difference between cavity walls in class I composite resin restoration with different filling techniques. Twenty extracted caries-free human third molars were used. Cavities were prepared in 6 ${\times}$4 ${\times}$3 mm box-type and divided into four groups according to filling technique and bonding surface: Group I; bulk filling - pulpal wall, Group II; bulk filling - axial wall, Group III; incremental filling - pulpal wall, Group IV; incremental filling - axial wall. Cavities were filled with Filtek $Z250^{(R)}$(3M/ESPE., USA) and Clearfill SE $bond^{(R)}$(Kuraray, Japan). After 24 hour-storage in $37^{\circ}C$water, the resin bonded teeth were sectioned bucco-lingualy at the center of cavity. Specimens were vertically sectioned into 1.0 ${\times}$1.0 mm thick serial sticks perpendicular to the bond surface using a low-speed diamond saw (Accutom 50, Struers, Copenhagen, Denmark) under water cooling. The trimmed specimens were then attached to the testing device and in turn, was placed in a universal testing machine (EZ test, Shimadzu Co., Kyoto, Japan) for micro-tensile testing at a cross-head speed of 1 mm/min. The results obtained were statistically analyzed using 2-way ANOVA and t-test at a significance level of 95%. The results were as follows: 1. There was no significant difference between bulk filling and incremental filling. 2. There was no significant difference between pulpal wall and axial wall, either. Within the limit of this study, it was concluded that microtensile bond strength was not affected by the filling technique and the site of cavity walls.

Study of Solidification by Using Portland and MSG(micro silica grouting) Cements for Metal Mine Tailing Treatment (금속 광미 처리를 위한 포틀랜드 시멘트와 MSG(micro silica grouting) 시멘트 고형화 실증 실험 연구)

  • Jeon, Ji-Hye;Kim, In-Su;Lee, Min-Hee;Jang, Yun-Young
    • Economic and Environmental Geology
    • /
    • v.39 no.6 s.181
    • /
    • pp.699-710
    • /
    • 2006
  • Batch scale experiments to investigate the efficiency of the solidification process for metal mine tailing treatment were performed. Portland and MSG (micro silica pouting) cements were used as solidifier and three kinds of mine tailings (located at Gishi, Daeryang, and Aujeon mine) were mixed with cements to paste solidified matrices. Single axis com-pressible strengths of solidified matrices were measured and their heavy metal extraction ratios were calculated to investigate the solidification efficiency of solidified matrices created in experiments. Solidified matrices ($5cm{\times}5cm{\times}5cm$) were molded from the paste of tailing and cements at various conditions such as different tailing/cement ratio, cement/water ratio, and different cement or tailing types. Compressible strengths of solidified matrices after 7, 14, and 28 day cementation were measured and their strengths ranged from 1 to $2kgf/mm^2$, which were higher than Korean limit of compressible strength for the inside wall of the isolated landfill facility ($0.21kgf/mm^2$). Heavy metal extractions from intact tailings and powdered matrices by using the weak acidic solution were performed. As concentration of extraction solution for the powdered solidified matrix (Portland cement + Gishi tailing at 1:1 w.t. ratio) decreased down to 9.7 mg/L, which was one fifth of As extraction concentration for intact Gishi tailings. Pb extraction concentration of the solidified matrix also decreased to lower than one fourth of intact tailing extraction concentration. Heavy metal extraction batch experiments by using various pH conditions of solution were also performed to investigate the solidification efficiency reducing heavy metal extraction rate from the solidified matrix. With pH 1 and 13 of solution, Zn and Pb concentration of solution were over the groundwater tolerance limit, but at pH $1{\sim}13$ of solution, heavy metal concentrations dramatically decreased and were lower than the groundwater tolerance limit. While the solidified matrix was immerged Into very acidic or basic solution (pH 1 and 13), pH of solution changed to $9{\sim}10$ because of the buffering effect of the matrix. It was suggested that the continuous extraction of heavy metals from the solidified matrix is limited even in the extremely high or low pH of contact water. Results of experiments suggested that the solidification process by using Portland and MSG cements has a great possibility to treat heavy metal contaminated mine tailing.

Evaluation of Shear Zone in Direct Shear Test Using Elastic, Electromagnetic Waves and Cone Tip Resistance (전단파, 전자기파 및 콘 관입저항력을 이용한 직접전단실험시 전단영역 특성 평가)

  • Byun, Yong-Hoon;Truong, Q. Hung;Tran, M. Khoa;Lee, Jong-Sub
    • Journal of the Korean Geotechnical Society
    • /
    • v.27 no.2
    • /
    • pp.43-52
    • /
    • 2011
  • The characteristics of shear zone in granular soils largely affect the stability of geo-structures. The goal of this study is to evaluate shear zone in a direct shear test using shear wave, electrical resistivity, and cone tip resistance. Bender elements and electrical resistivity probe are embedded into the wall of a direct shear box made of transparent acrylic material to estimate the shear wave velocities and the electrical resistivity at shear and non-shear zones. At the point of peak and residual strength, micro cone penetration test which can be available to measure tip resistance has been performed. Experimental results show that the shear wave velocities at upper shear zone increase during shearing while the values remain constant at bottom and lower shear zone. Also, resistivities at lower shear zone depend on relative density while resistivities at bottom remain constant. The results of cone penetration test demonstrate the correlation of the cone tip resistance and small strain shear modulus at shear zone. This study suggests that the application of the modified direct shear box including shear wave, electrical resistivity and the micro cone tip resistance may become effective tools for analyzing the characteristics of a shear zone.

A Study about The Global Trend of Neo-Grouting Technology (최신 그라우팅 기술의 세계적인 동향에 관한 연구)

  • Kim, Jin-Chun;Kim, Sang-Gyun;Yoo, Byung-Sun;Kang, Hee-Jin
    • Journal of Korean Society of Disaster and Security
    • /
    • v.7 no.2
    • /
    • pp.25-34
    • /
    • 2014
  • This study researches on global technology trend in each of composing technology, such as grouting material, grouting equipment, and construction management technology, which grouting technology has been founded upon to improve relatively inadequate domestic grouting technology and to establish the global standard for overseas expansion in the future. As far as grouting material is concerned, while High-Penetration and High-Strength micro cement ($1.5{\mu}m$) has been developed in 2000's in Japan, JinChun Kim et al. (2014) has been developing hybrid type micro cement grouting material and examining specifications of different kinds of projects and countries to analyze the trend of grouting equipment development. The specification contains detailed requisite specification for materials, mixers, pumps, agitators, and packers and it has to satisfy the standard of different countries to win global contracts. Grouting management technology can be divided into four different generations and Scandinavian countries, such as Sweden, Norway, and Finland, Japan, and South Korea are recently doing vigorous researches on the Fourth generation which merges grouting technology with ICT.

Effect of Fine Particle Cement and Recycled Aggregates as Alkali Activator on the Engineering Properties and Micro-Structure of High Volume Blast Furnace Slag Concrete (알칼리 자극제로서 미분시멘트와 순환골재가 고로슬래그 다량치환 콘크리트의 공학적 특성 및 미세구조에 미치는 영향)

  • Han, Min-Cheol;Lee, Hyang-Jae;Han, Cheon-Goo
    • Journal of the Korea Institute of Building Construction
    • /
    • v.13 no.6
    • /
    • pp.602-608
    • /
    • 2013
  • The aim of this study is to investigate experimentally the effect of the combination of fine particle cement with high Blaine fineness (FC) and recycled aggregates on the engineering properties and micro structure of high volume blast furnace slag (BS) concrete with 75% BS and 21 MPa. FC manufactured by particle classification at the plant with Blaine fineness of more than $7000cm^2/g$ was used as additional alkali activator for high volume blast furnace slag concrete made with recycled fine and coarse aggregates. FC was replaced by 15, 20 and 25% OPC. Test results showed that the incorporation of FC resulted in an increase in the compressive strength compared to BS concrete without FC by as much as 30% due to accelerated hydration and associated latent hydraulic reaction. It was found that the use of FC and recycled aggregates played an important role in activating BS for high volume BS concrete by offering sufficient alkali.

An Experimental Study on Mechanical Properties of Hybrid Fiber Reinforced Concrete Pavement (하이브리드 섬유로 보강된 콘크리트 포장의 역학적 특성 실험연구)

  • Park, Jong-Sup;Choi, Sung-Yong;Jung, Woo-Tai;Park, Young-Hwan
    • Journal of the Korea Concrete Institute
    • /
    • v.25 no.1
    • /
    • pp.11-18
    • /
    • 2013
  • Cement concrete pavement offers long-term service life and excellent applicability for heavy traffic. It is easier to purchase and more durable and economical than the asphalt pavement. However, it is difficult to repair and rehabilitate compared to the asphalt pavement when it comes to the maintenance problem. Since the crack is the main reason of the damage of concrete pavement, it is necessary to control the early and long-term crack in the concrete pavement. In this experimental study, the basic performance tests have been carried out to investigate the effect of hybrid fibers which were composed of micro fibers with small diameter and high aspect ratio and macro fibers with large diameter and low aspect ratio on the concrete pavement, in which lower water ratio and larger aggregates were used compared to the general concrete mixture. The test results showed that the flexural strength and toughness of concrete pavement mixture have been increased with the use of hybrid fibers in the concrete pavement mixture, even though they were less effective compared to the normal concrete mixture. It was found that the hybrid fibers were effective to control the early shrinkage of the concrete pavement which is one of the main reasons of the damage in the concrete pavement.

Mechanical and Electrical Properties of Electrospun CNT/PVDF Nanofiber for Micro-Actuator (미세-작동기를 위한 전기방사 CNT/PVDF 나노섬유 기반의 탄소 복합재의 기계적 및 전기적 특성 평가)

  • Gu, Ga-Young;Wang, Zuo-Jia;Kwon, Dong-Jun;Park, Joung-Man
    • Composites Research
    • /
    • v.26 no.1
    • /
    • pp.14-20
    • /
    • 2013
  • The electrospun PVDF containing CNT was made for fabricating materials of the actuator. The electrochemical and their actuating movement were evaluated for the actuator performance in the electrochemical environment. The actuator (which was fabricated by electrospinning) had some advantages, i.e., good dispersion and flexible properties. In the electrospinning process, the final product would have different forms based on different essential factors. In this work, electrospun nanofibers were aligned by using the drum-type collector, and the morphology was identified via the field emission-scanning electron microscope (FE-SEM). The uniform dispersion of CNT in PVDF nanofiber was observed by electron probe X-ray micro-analysis (EPMA) test. The results of tensile strength and electrical resistivity provided the aligned state. The electrospun CNT/PVDF nanofiber sheet on the aligned direction showed better mechanical and electrical properties than the case of the vertically-aligned direction. The efficiency and electrical capacities of electrospun CNT/PVDF nanofiber sheets were compared with the cast PVDF sheet for actuator application. Electrospun CNT/PVDF nanofiber sheet exhibited much better the case of actuator performance than cast neat PVDF actuator, due to the excellent electrical connecting areas.

Characteristic Evaluation of SCR catalyst using Aluminum dross (알루미늄 폐드로스를 활용한 SCR 탈질촉매 제조 및 특성평가)

  • Bae, Min A;Kim, Hong Dae;Lee, Man Sig
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.14 no.10
    • /
    • pp.4672-4678
    • /
    • 2013
  • Aluminum dross is formation at the surface of the molten metal as the latter reacts with the furnace atmosphere and it was an unavoidable by-product of the aluminum production process. However aluminum dross was usually landfilled or disposed without treatment, causing much environmental damage. The purpose of this study is to investigate the possibility of ceramic catalyst support using recycled Al dross. The recycled Al dross was made into SCR catalyst by mixing with $WO_3$, $V_2O_5$ and $TiO_2$. The $V_2O_5-WO_3/TiO_2-Al_2O_3$ SCR catalyst was observed with XRF, XRD and BET. $V_2O_5-WO_3/TiO_2-Al_2O_3$ SCR strength was measured by Universal Testing Machine(UTM). As the added $Al_2O_3$, streagth is increased. And the NOx removal activity was observed by MR(Micro-Reactor). The temperatures ranging from $350^{\circ}C$ and $400^{\circ}C$, $V_2O_5-WO_3/TiO_2-Al_2O_3$ SCR catalyst De-NOx performance result of showed excellent activity over 90% at application condition.

Study on the Development of Putty According to Epoxy Resin Hardener (Epoxy 수지 경화제에 따른 Putty 개발에 관한 연구)

  • Oh, Seung-Jun;Cheong, Da-Som;Park, Gi-Jung;Wi, Koang-Chul
    • Journal of Conservation Science
    • /
    • v.31 no.2
    • /
    • pp.105-114
    • /
    • 2015
  • In this study, an advanced epoxy putty which was as a multi-purpose restoration material being used to restore missing parts in the artifact preservation treatment process was developed. For the purpose of addressing the issues including the workability issue resulting from high strength, the drooping issue resulting from long hardening time during work process and the issue of contaminating the surface of artifact resulting from stained material on tools or gloves, a property comparison was conducted with existing materials to examine the properties of restoration materials in the form of epoxy putty currently being frequently used. For the purpose of addressing the issues of existing materials and allowing the developed epoxy putty to have similar properties, two types of hardeners with different properties were selected to conduct property experiments. As for the hardeners, mercaptan type hardener and aliphatic amine type hardeners in the total of two types were selected for the development. The result showed that the two types were both in the form of paste and their hardening time of 5-10 minutes were about 3-10 times shorter than that of existing materials, thereby improving the work convenience. In terms of abrasion rate to increase workability, it was improved by about 3 times to allow effective and convenient use. As for the issue of contaminating the artifact surface during the process, white micro-balloon was added as filler to address the issue to reduce the oil ingredient to develop multi-purpose restoration material with low shrinkage & high workability in coloring, light weight and cutting force.

Study on the Development and Property of Epoxy Putty with Excellent Low Shrinkage and Cutting Force Using Mercaptan Type and Diamine Type (Mercaptan계와 Diamine계를 이용한 저수축·절삭력이 우수한 Epoxy Putty의 개발 및 물성에 관한 연구)

  • Oh, Seung-Jun;Wi, Koang-Chul
    • Journal of Adhesion and Interface
    • /
    • v.16 no.4
    • /
    • pp.137-145
    • /
    • 2015
  • This study aimed to develop epoxy putty as a multi-purpose connection and restoration material that can be used for material-specific restoration work such as metal, wood, ceramics, earthenware and stone artifacts by replacing synthetic resins currently being used for preservation treatment of cultural assets. Existing synthetic resins have the issue of cutting force resulting from high strength, deflection resulting from long hardening time, contaminating the surface of artifacts through staining on tools or gloves and need for re-treatment resulting from material discoloration. Accordingly, paste type restoration material most widely being used in the field of cultural assets preservation treatment was selected and examined the property to select it as an object of comparison. Based on such process, epoxy putty was developed according to the kind of agent, hardener and filler. For the purpose of solving the issues of existing material and allowing the epoxy putty developed to have similar property, property experiments were conducted by selecting agents and hardeners with different characteristics and conditions. The study findings showed that both kinds are paste type that improved work convenience and deflection issue as a result of their work time of within 5~10 minutes that are about 3~10 times shorter than that of existing material. In regards to wear rate for increasing cutting force, it improved by about 3 times, thereby allowing easy molding. For the purpose of improving the issue of surface contamination that occurs during work process, talc and micro-ballon were added as filler to reduce the issue of stickiness and staining on hand. Furthermore, a multi-purpose restoration material with low shrinkage, low discoloration and high cutting force was developed with excellent coloring, lightweight and cutting force features.