• Title/Summary/Keyword: Micro Powder

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Materials Characterization and the Microstructure of Pure Cu and Cu-3vol%CNT Composite Fabricated From Optimization of SPS Processing Variables (SPS 공정 변수의 최적화에 의한 Pure Cu와 Cu-3vol%CNT composite의 미세구조와 소재특성)

  • Lee, Hee Chang;Kim, Hye Sung
    • Journal of the Korean Society for Heat Treatment
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    • v.33 no.4
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    • pp.185-192
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    • 2020
  • In this study, materials characterization of pure copper and copper based carbon nano-tube composite prepared by powder metallurgy method were investigated. Prior to evaluate materials characterization, spark plasma sintering processing variables such as sintering temperature, pressure, thickness and diameter of compacts was optimized to ensure the microstructure and materials property of pure Cu and Cu-CNT composite. In addition, corrosion behavior of Cu-based CNT composite produced by powder sintering method was investigated. It was confirmed from this study that the corroded surfaces of the composite shows less dissolution compared with pure copper in 3.5 wt% NaCl solution. The measured corrosion current density (Icorr) indicates improved corrosion property of Cu based composite containing small additions of CNTs in chloride containing media. Micro-galvanic activity between Cu and CNT was not observed in given sintering condition.

Wear Patterns and Mechanisms of Cutting Tool in Cutting of Machinable Ceramics (가공성 세라믹 절삭에서 공구의 마멸 패턴과 메카니즘)

  • Jang, Sung-Min;Baek, Seung-Yub
    • Journal of the Korean Society of Safety
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    • v.25 no.5
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    • pp.1-6
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    • 2010
  • When the ceramic material is being machined, micro crack and brittle fracture dominate the process of material removal. Generally, ceramics are very difficult-to-cut materials and machined using conventional method such as grinding and polishing. However, such processes are generally cost-expensive and have low material removal rate. Machinable ceramics used in this study contain BN powder to overcome these problem and for productivity elevation. This paper focuses on machinability evaluation during end mill process with CNC machining center in this study. Experiment for this purpose is performed for tool wear patterns and mechanism.

Processing of Barrier Ribs of PDP Using an UV-curable Paste (광경화성 페이스트를 이용한 PDP 격벽 형성 연구)

  • Kim Yoo-Seong;Koh Tae-Gum;Kim Yong-Seog
    • Journal of Powder Materials
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    • v.13 no.3 s.56
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    • pp.211-216
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    • 2006
  • In an attempt to reduce processing cost and to improve resolution of PDPs, micro mold transfer processing route for barrier ribs of plasma display panel was attempted. In this study, the parameters that may cause defects during the process were identified, which include the shrinkage during UV curing process, stress due to evaporation of organic components, and sintering shrinkage. Considering such parameters, UV curable paste was developed and barrier ribs of PDPs were successfully processed via the process. This work demonstrated the possibility of build-up route in manufacturing barrier ribs of PDP.

Effect of Si/$Si_3N_4$ Ration on the Micro structure and Properties of Porous Silicon Nitride Prepared by SHS Method (규소/질화규소 비가 자전연소합성공정을 이용한 다공질 질화규소 세라믹스의 미세구조와 특성에 미치는 영향)

  • Kim, Dong-Baek;Park, Dong-Su;Han, Byeong-Dong;Jeong, Yeon-Gil
    • 연구논문집
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    • s.34
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    • pp.131-138
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    • 2004
  • Porous silicon nitride ceramics were prepared by Self-propagating High Temperature Synthesis from silicon powder, silicon nitride powder and the pore-forming precursor. The microstructure, porosity and the flexural strength of the porous silicon nitride ceramics were varied according to the Si/$Si_3N_4$ ratio, size and amount of the pore-forming precursors. Some samples exhibited as high flexural strength as $162\pm24$ MPa. The high strength is considered to result from the fine pore size and the strong bonding among the silicon nitrid particles.

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An Experimental Studyon the Durability of Steel Field Reinforced Concrete Using Silica Fume (실리카흄을 혼입한 강섬유보강 콘크리트의 내구성에 관한 실험적연구)

  • 박승범;홍석주;조청휘;김부일
    • Proceedings of the Korea Concrete Institute Conference
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    • 1998.04a
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    • pp.285-291
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    • 1998
  • During recent years, the durability of concrete structures has been considered in concret practice and material research. To preserve the brittleness of concrete as well as energy absorption and impact resistance, amount of fiber usage has greatly increased in the field of public works. Ultra fine powder, silica fume, mixed into concrete, it reduce void of concrete structure. Especially, there's a great effect for strength improvement of concrete by initial pozzolanic reactions. For these reasons, if silica fume mixed into concrete, it decrease the total void by microfilter effect . Pozzolan reaction, between cement particle and silica powder, can elaborate the micro structure of matrix. And so, in this paper, we deal SFRC for the purpose of efficiently using of industrial by-products(silica fume). Also we performed the test for durability such as freeze-thaw resistance and accelerated carbonation of SFRC using silica fume.

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A Nano-particle Deposition System for Ceramic and Metal Coating at Room Temperature and Low Vacuum Conditions

  • Chun, Doo-Man;Kim, Min-Hyeng;Lee, Jae-Chul;Ahn, Sung-Hoon
    • International Journal of Precision Engineering and Manufacturing
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    • v.9 no.1
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    • pp.51-53
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    • 2008
  • A new nano-particle deposition system (NPDS) was developed for a ceramic and metal coating process. Nano- and micro-sized powders were sprayed through a supersonic nozzle at room temperature and low vacuum conditions to create ceramic and metal thin films on metal and polymer substrates without thermal damage. Ceramic titanium dioxide ($TiO_2$) powder was deposited on polyethylene terephthalate substrates and metal tin (Sn) powder was deposited on SUS substrates. Deposition images were obtained and the resulting chemical composition was measured using X-ray photoelectron spectroscopy. The test results demonstrated that the new NPDS provides a noble coating method for ceramic and metal materials.

Comparison of the chlorophyll content analysis methods of micro-algal oil (미세조류의 엽록소 분석법에 따른 함량 비교)

  • Choi, Byoungyun;Kim, Deogkeun
    • 한국신재생에너지학회:학술대회논문집
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    • 2011.11a
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    • pp.113.1-113.1
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    • 2011
  • 미세조류 내의 엽록소는 바이오디젤 전환 반응에서 산 촉매의 활성을 억제 할 뿐만 아니라, 짙은 색상을 띄게하여 바이오디젤 품질규격으로부터 벗어나게 한다. 미세조류의 엽록소 분석은 용매에 의해 엽록소를 추출한 후, 흡광도를 측정하여 그 함량을 계산하는 방법을 널리 사용하고 있다. 건조된 미세조류의 분석은 선택되는 용매에 따라 최대 추출량이 달라지는 것을 제외하고 큰 문제가 없지만 미세조류를 lipid 오일로 변환하면, 용매에 녹지 않아 추출이 되지않는 문제가 발생하여 흡광도 측정을 어렵게 한다. 따라서 미세조류의 형태가 powder일 때와 오일인 경우를 구분하여 용매를 선택해야 하며, 오일 또는 powder 형태 구분 없이 사용할 수 있는 분석법을 적용하여 서로 다른 엽록소 함량을 비교한 후 분석법 간의 상호 장단점을 파악해야한다. 본 연구에서는 메탄올을 용매로 사용하는 분석법(porra et al.)과 아세톤을 용매로 사용하는 분석법(Humphrey and Jeffrey)을 적용하여 엽록소 함량을 비교하였고, AAS(Atomic Absorption Spectrometer)를 통한 Mg 함량 측정을 통해 엽록소 함량을 계산하는 분석법간의 차이를 확인하였다.

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Characteristics of Ti-Ni-(XCu) Shape Memory Alloy Powders made by Gas Atomization Process (가스 분무법으로 제조한 Ti-Ni-XCu 형상기억합금분말의 특성)

  • 징동훈
    • Journal of Powder Materials
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    • v.6 no.2
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    • pp.171-177
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    • 1999
  • Ti-45.2at.%Ni-5at.%Cu and Ti-40.2at.%Ni-10atat.%Cu alloy powders were fabricated by gas atomization process. The microstructures, Shape, hardness and phase transformation behaviors of the powders were investigated by means of optical microscopy, scanning electron microscopy, micro-hardness measurement, x-ray diffraction analyses and differential scanning calorimetry. The hardness of the Ti-Ni-XCu alloy powders decreased as Cu-content increased. The x-ray diffraction analyses were carried out for powders without heat treatment, and those that treated at 85$0^{\circ}C$ for an hour in a vaccum state($10^5$ torr) and then quenched into ice water. The intensity of B$19^t$ phase increased with heat treating. The monoclinic B$19^t$ martensite was formed in the Ti-Ni-XCu alloy powders during cooling.

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Recent Progress on the Application of Atomic Layer Deposition for Lithium Ion Batteries (원자층 증착법을 적용한 리튬 이온 전지 연구 동향)

  • Kim, Dong Ha;Choi, Byung Joon
    • Journal of Powder Materials
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    • v.23 no.2
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    • pp.170-176
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    • 2016
  • Lithium-ion batteries (LIBs) are rapidly improving in capacity and life cycle characteristics to meet the requirements of a wide range of applications, such as portable electronics, electric vehicles, and micro- or nanoelectro-mechanical systems. Recently, atomic layer deposition (ALD), one of the vapor deposition methods, has been explored to expand the capability of LIBs by producing near-atomically flat and uniform coatings on the shell of nanostructured electrodes and membranes for conventional LIBs. In this paper, we introduce various ALD coatings on the anode, cathode, and separator materials to protect them and improve their electrochemical and thermomechanical stability. In addition, we discuss the effects of ALD coatings on the three-dimensional structuring and conduction layer through activation of electrochemical reactions and facilitation of fluent charge collection.

New Frontiers in Hard Materials Testing

  • Gee, Mark;Gant, Andrew;Morrell, Roger;Roebuck, Bryan
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.885-886
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    • 2006
  • Significant advances in mechanical testing for hard materials are discussed in this paper. There are three specific areas that are covered. In the measurement of fracture toughness factors such as the control of slow crack growth to produce strating cracks, and evaluating reproducibility and repeatability of tests have been recently examined. The miniaturization of tests reduces the amount of material that is used in testing, improves the throughput of tests, and also improves cost effectiveness. New techniques such as stepwise testing and micro scratch testing have contributed to significant additions to the knowledge of the wear mechanisms that operate in these materials.

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