• Title/Summary/Keyword: Micro Porosity

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The Effect of Binder Content for the Pore Properties of Fe Foam Fabricated by Slurry Coating Process (슬러리 코팅 공정으로 제조된 Fe 폼의 기공 특성에 미치는 바인더 함량의 영향)

  • Choi, Jin Ho;Yang, Sangsun;Kim, Yang-Do;Yun, Jung-Yeul
    • Journal of Powder Materials
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    • v.20 no.6
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    • pp.439-444
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    • 2013
  • Fe foam with above 90% porosity and 2 millimeter pore size was successfully fabricated by a slurry coating process. In this study, the binder contents were controlled to produce the Fe foam with different pore size, strut thickness and porosity. Firstly, the slurry was prepared by uniform mixing with Fe powders, distilled water and polyvinyl alcohol(PVA) as initial materials. After slurry coating on the polyurethane(PU) foam the sample was dried at $80^{\circ}C$. The PVA and PU foams were then removed by heating at $700^{\circ}C$ for 3 hours. The debinded samples were subsequently sintered at $1250^{\circ}C$ with holding time of 3 hours under hydrogen atmosphere. The three dimensional geometries of the obtained Fe foams with open cell structure were investigated using X-ray micro CT(computed tomography) as well as the pore morphology, size and phase.

Al-7020의 Pulse-GMA용접에 관한 연구 2

  • 김재웅;허장욱;나석주;백운형
    • Journal of Welding and Joining
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    • v.6 no.4
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    • pp.54-62
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    • 1988
  • Major problems in welding Al-7020 include shrinkage, rpopositgy in welds and loss of strength in the heat affected zone. Thus it is important to examine the mechanical properties and reliability of welds. In this study, a series of experiments was carried out to determine the mechanical properties such as micro-hardness distribution, tensile strength, porosity and residual stress distribution of the Al-7020 weldment made by pulse-GMA welding. The resuts of the experiemnts are as folows. 1) The micro-hardness of weld metal and heat affected zone was lower than that of the base metal. 2) The tensile strength of the deposited metal was much lower than that of the base metal. 3) The porrosity in weld metal zone was negligible under the adopted conditsion of experiemnts. 4) The residual stress in the weld metal was lower than that of the heat affected zone, because the weld metal was softened. And the mciro-hardness distribution, the tensile strength and the residual stess distribution of the weldment in the as-welded condition were compared with those of the weldment after heat treatment.

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Study on Permeability Characteristics of Cement Mortar under Carbonation (탄산화 진행에 따른 시멘트 모르타르의 투수특성에 대한 연구)

  • Kwon, Seung-Jun;Song, Ha-Won;Park, Chan-Kyu
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.05b
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    • pp.185-188
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    • 2006
  • During the carbonation process in concrete, the rate of carbonation depends on porosity and moisture content of the concrete. For underground reinforced concrete structures, the interior concrete surface may be exposed to carbonation and the exterior concrete surface exposed to moisture due to wet soil or underground water. In this study, the permeability coefficients in mortar partially carbonated is derived as a function of carbonation depth and porosity of mortar by applying the so-called micro pore structure formation model (MPSFM) which was developed for the modeling of early-aged concrete. The permeability coefficient obtained from the micro-level modeling of carbonated mortar is verified with the results of accelerated carbonation test and water penetration test in cement mortar.

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Characterization of electron beam (EB) welds for SUS310S

  • Kim, Hyun-Suk;Castro, Edward Joseph D.;Lee, Choong-Hun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.360-360
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    • 2011
  • In this work, SUS310S used for valve plate assembly was electron beam (EB) welded to determine the influence of the parametric conditions on the characteristics of the weld and to minimize porosity and micro-fissures among others. The evolution in the weld geometry and microstructure was examined as a function of the process conditions such as beam current and focusing current under a constant welding speed and accelerating voltage. The integrity of the EB welds in SUS310S was examined for defects (e.g. cracking, porosity, etc.), adequate penetration depth, and tolerable weld width deviation for the various welding conditions. Optical microscopy (OM), x-ray photoelectron spectroscopy analysis (XPS), scanning electron microscopy (SEM) and 3D micro-computed tomography (Micro-CT) for the cross section analysis of the electron beam welded SUS310S were utilized. The tensile strength and hardness were analyzed for the mechanical properties of the EB weld. At the 6 kV accelerating voltage, it was determined that a satisfactory penetration depth and desirable weld width deviation requires a beam current of 30 mA and a focusing current of 0.687 A at the welding speed of 25 mm/sec.

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Analysis of Porosity and Distribution of Pores in Rocks by Micro Focus X-Ray CT (미소 초점 X선 CT를 이용한 암석 내 공극의 분포 및 공극률 분석)

  • Jeong, Gyo-Cheol;Takahashi, Manabu
    • The Journal of Engineering Geology
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    • v.20 no.4
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    • pp.461-465
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    • 2010
  • Weathering and permeability in rocks play a very important role in underground disposal of radioactive waste and their long-term management as well as stability security of rock structures. Weathering and permeability of rocks are largely controlled by the characters of inner structures of rocks. In other words, weathering rate can be accelerated depending on the quantity of pore and microcrack in rocks. Quantitative evaluation of inner structures of rocks can serve as a tool that can assess the degree of weathering of rocks. Therefore it can be said that the understanding of three dimensional distribution of the inner structure of rocks is important for long-term management of rock structures. This study was performed to analyze three dimensional distribution of pore in rocks using Micro Focus X-ray CT on fresh granite and weathered granite from Korea. Results of the analysis clearly show distribution of pore and porosity of the inner rock.

Free vibration of imperfect sigmoid and power law functionally graded beams

  • Avcar, Mehmet
    • Steel and Composite Structures
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    • v.30 no.6
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    • pp.603-615
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    • 2019
  • In the present work, free vibration of beams made of imperfect functionally graded materials (FGMs) including porosities is investigated. Because of faults during process of manufacture, micro voids or porosities may arise in the FGMs, and this situation causes imperfection in the structure. Therefore, material properties of the beams are assumed to vary continuously through the thickness direction according to the volume fraction of constituents described with the modified rule of mixture including porosity volume fraction which covers two types of porosity distribution over the cross section, i.e., even and uneven distributions. The governing equations of power law FGM (P-FGM) and sigmoid law FGM (S-FGM) beams are derived within the frame works of classical beam theory (CBT) and first order shear deformation beam theory (FSDBT). The resulting equations are solved using separation of variables technique and assuming FG beams are simply supported at both ends. To validate the results numerous comparisons are carried out with available results of open literature. The effects of types of volume fraction function, beam theory and porosity volume fraction, as well as the variations of volume fraction index, span to depth ratio and porosity volume fraction, on the first three non-dimensional frequencies are examined in detail.

The Effect of Fe and Fe2O3 Powder Mixing Ratios on the Pore Properties of Fe Foam Fabricated by a Slurry Coating Process (슬러리 코팅 공정으로 제조된 Fe 폼의 기공 특성에 미치는 Fe 및 Fe2O3 분말의 혼합 비율의 영향)

  • Choi, Jin Ho;Jeong, Eun-Mi;Park, Dahee;Yang, Sangsun;Hahn, Yoo-Dong;Yun, Jung-Yeul
    • Journal of Powder Materials
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    • v.21 no.4
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    • pp.266-270
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    • 2014
  • Metal foams have a cellular structure consisting of a solid metal containing a large volume fraction of pores. In particular, open, penetrating pores are necessary for industrial applications such as in high temperature filters and as a support for catalysts. In this study, Fe foam with above 90% porosity and 2 millimeter pore size was successfully fabricated by a slurry coating process and the pore properties were characterized. The Fe and $Fe_2O_3$ powder mixing ratios were controlled to produce Fe foams with different pore size and porosity. First, the slurry was prepared by uniform mixing with powders, distilled water and polyvinyl alcohol(PVA). After slurry coating on the polyurethane(PU) foam, the sample was dried at $80^{\circ}C$. The PVA and PU foams were then removed by heating at $700^{\circ}C$ for 3 hours. The debinded samples were subsequently sintered at $1250^{\circ}C$ with a holding time of 3 hours under hydrogen atmosphere. The three dimensional geometries of the obtained Fe foams with an open cell structure were investigated using X-ray micro CT(computed tomography) as well as the pore morphology, size and phase. The coated amount of slurry on the PU foam were increased with $Fe_2O_3$ mixing powder ratio but the shrinkage and porosity of Fe foams were decreased with $Fe_2O_3$ mixing powder ratio.

Bending analysis of porous microbeams based on the modified strain gradient theory including stretching effect

  • Lemya Hanifi Hachemi Amar;Abdelhakim Kaci;Aicha Bessaim;Mohammed Sid Ahmed Houari;Abdelouahed Tounsi
    • Structural Engineering and Mechanics
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    • v.89 no.3
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    • pp.225-238
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    • 2024
  • In this paper, a quasi-3D hyperbolic shear deformation theory for the bending responses of a functionally graded (FG) porous micro-beam is based on a modified couple stress theory requiring only one material length scale parameter that can capture the size influence. The model proposed accounts for both shear and normal deformation effects through an illustrative variation of all displacements across the thickness and satisfies the zero traction boundary conditions on the top and bottom surfaces of the micro-beam. The effective material properties of the functionally graded micro-beam are assumed to vary in the thickness direction and are estimated using the homogenization method of power law distribution, which is modified to approximate the porous material properties with even and uneven distributions of porosity phases. The equilibrium equations are obtained using the virtual work principle and solved using Navier's technique. The validity of the derived formulation is established by comparing it with the ones available in the literature. Numerical examples are presented to investigate the influences of the power law index, material length scale parameter, beam thickness, and shear and normal deformation effects on the mechanical characteristics of the FG micro-beam. The results demonstrate that the inclusion of the size effects increases the microbeams stiffness, which consequently leads to a reduction in deflections. In contrast, the shear and normal deformation effects are just the opposite.

Double bonded Cooper-Naghdi micro sandwich cylindrical shells with porous core and CNTRC face sheets: Wave propagation solution

  • Yazdani, Raziye;Mohammadimehr, Mehdi
    • Computers and Concrete
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    • v.24 no.6
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    • pp.499-511
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    • 2019
  • In this paper, wave propagation of double-bonded Cooper-Naghdi micro sandwich cylindrical shells with porous core and carbon nanotube reinforced composite (CNTRC) face sheets are investigated subjected to multi-physical loadings with temperature dependent material properties. The governing equations of motion are derived by Hamilton's principle. Then, the influences of various parameters such as wave number, CNT volume fraction, temperature change, Skempton coefficient, material length scale parameter, porosity coefficient on the phase velocity of double-bonded micro sandwich shell are taken into account. It is seen that by increasing of Skempton coefficient, the phase velocity decreases for higher wave number and the results become approximately the constant. Also, by increasing of the material length scale parameter, the cut of frequency increases, because the stiffness of micro structure increases. The obtained results for this article can be used to detect, locate and quantify crack.

CHARACTERISTICS OF RESIDUAL CARBON DERIVED FROM THE COMBUSTION OF VACUUM RESIDUE IN A TEST FURNACE

  • Park, Ho-Young;Seo, Sang-Il
    • Environmental Engineering Research
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    • v.12 no.3
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    • pp.109-117
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    • 2007
  • The characteristics of carbonaceous particles collected from the combustion of Vacuum Residue (VR) in a test furnace have been investigated. The physical and chemical characterization includes particle size, scanning electron microscopy of the surface structure, measurement of porosity, surface area and density, EDX/XRD analyses and measurement of chemical composition. The studies show that the carbonaceous VR particles are very porous and spheroidal, and have many blow-holes on the surface. The particles become smaller and more sponge-like as the reaction proceeds. The present porosity of VR particles is similar to that of cenospheres from the combustion of heavy oil, and the majority of pores are distributed in macro-pores above $0.03\;{\mu}m$ in diameter. Measurements of pore distribution and surface area showed that the macro-pores contributed most to total pore volume, whereas the micro-pores contributed to total surface area.